汞化

2 The analysis step by 25.0mL sample lixivium, moved in the direction of arsenic in the bottle, plus 10 ml of hydrochloric acid and 10 ml of potassium iodide solution and 5 drop acid stannochlor solution, shake the place 10min, together with 2 g of arsenic-free zinc metal, immediately mounted a good lead acetate paper turns red cotton and mercury bromide from log that arsenic tube placed in the 25-38, f μh of the dark side, remove the test strip and standard mercury bromide a color not deeper than standard.

7.2 分析步骤取25.0mL样品浸泡液，移入测砷瓶中，加5mL盐酸、5mL碘化钾溶液及5滴酸性氯化亚锡溶液，摇匀后放置10min，加2g无砷金属锌，立即将已装好乙酸铅棉花及溴化汞试纸的测砷管装上，放置于25～30℃的暗处1h，取出溴化汞试纸和标准比较，其色斑不得深于标准。

Reaction conditions are studied, and the result shows that it is better to adopt mercuric oxide or mercuric fluoride as fluorination catalyst with reaction temperature -20~-10℃.

结果表明，采用氧化汞或氟化汞作氟化催化剂、氟化氢作溶剂较好，适宜的反应温度为－20~-10℃，较长的反应时间(48 h)和增加氟化氢和催化剂的量有利于氟化。2-氯－5-三氯甲基吡啶的转化率和选择率均可达到97%以上。

Methods The mercury in urine, which is the total amount of inorganic mercury in urine, including those produced from organic mercury after treated by potassium bromate and potassium bromide, is determined by atomic absorption spectrophotometer after reduction into mercury atom with sodium borohydride.

方法］尿样中汞（尿中无机汞和经溴酸钾－溴化钾处理尿中有机汞生成的无机汞之和）以硼氢化钠还原生成汞原子蒸气，用原子吸收光谱仪测定其汞的含量。

The high-pressure mercury vapor lamp according to the invention is remarkable in that germanium and oxygen are added in small quantities to the mercury and/or the mercury halides.

根据本发明的高压汞蒸气灯的显著之处在于给汞和/或卤化汞添加少量的锗和氧。

Lower mercury methylation was expected in these two reservoirs.With the development of reservoir,it is possible that the methylmercury concentrations will increase due to autochthonous and extraneous organic materials,and methylmercury may be released due to thermal stratification.But this was not confirmed.

通过研究发现目前库区环境汞的甲基化率低，但随着水库生态系统的不断演化，内源和外源营养物的输入及水体在温度分层其间自身甲基汞的形成，导致水体甲基汞含量的逐渐增加，但仍需进一步的研究证实。

Several attempts on epoxidation, oxymercuration and dihydroxylation of this bicyclic system were turn out to be unsuccessful.

尝试了环氧化、羟汞化等方法，但没有能够成功将C8-端烯转化成对应的叔醇。

Total mercury and methyl mercury concentrations were analyzed by cold vapor atomic fluorescence spectrometry and aqueous phase ethylation,GC separation,and CVAFS detection.

2006年1~12月，每月采集乌江流域梯级水库入出库河流水样，用两次金汞齐-冷原子荧光光谱法和蒸馏-乙基化结合GCCVAFS法测定了水中总汞和甲基汞的浓度。

Under a light and rapid hand, the glass is pushed straight forward and drives before it the surplus of the metal; and the mercury, shut in between the tin and the glass, spreads out, adheres, and amalgamates in a few minutes.

用手将玻璃迅速向前轻推，把多余的汞朝前挤；夹在锡箔和玻璃之间的汞几分钟之内就散开，胶着，齐化了。不过玻璃必须在重压下干燥近 8 天，贴锡的工序才算完成。

The influences of environmental factors on the abiotic methylation were studied. The biggest production of methylmercury was found after 2 days of incubation in presence of FA. The rate of production of methylmercury depends upon temperature. In presence of FA from sediment, the biggest production of methylmercury was found under 40℃. In presence of FA from soil, production rate increases with temperature. The biggest production of methylmercury was found when solution pH was 2 and 4 in presence of FA from sediment and soil, respectively. Increase in concentrations of inorganic mercury and FA solution causes an increase in the production of methylmercury. Under irradiation with ultraviolet ray, blacklight lamp as well as natural light, methylation is stimulated, especial for irradiation of ultraviolet light.

环境条件对汞甲基化作用的影响研究得出，在底泥和土壤FA体系中甲基汞产量均在反应2天后达到最大值；在底泥FA体系中汞的甲基化在反应温度为40℃时产量最大，而在土壤FA体系中，甲基汞产量在10～60℃之间随反应温度升高而增加；底泥和土壤FA体系中汞的甲基化分别在pH值为2和4时最大；甲基汞产量均随无机汞浓度和腐殖质浓度的增加而增加；紫外线、黑光灯和自然光照射都可促进甲基汞的生成，紫外线的作用尤其明显。

The titrant is a mixture of EDTA and sodium fluoride, both mercury film electrode and fluorinion selective electrode are inserted in the titration solution. In a process of titration, both the added volume of titrant and the concentration of mercury ion at each titration point can be obtained simultaneously from the potentials of two electrodes, and then the concentration of each component in the alloy can be obtained from the titration curves by multivariate calibration.

用ED-TA与氟化钠的混合溶液作为滴定剂，被滴定液中同时插入了汞膜电极和氟离子选择电极，在滴定过程中的任一滴定点，溶液中汞离子的浓度和滴定剂的加入体积可由两个电极的电位测定值同时获得，从而可应用多元校正法由相应的滴定曲线求得混合金属中每一种组分的含量。

I can not make it blossom and suits me

我不能让树为我开花

When temperatures are above approximately 80 °C discolouration of the raceways or rolling elements is a frequent feature.

当温度高于 80 °C 左右时，滚道或滚动元件褪色是很常见的特征。