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In this work, a series of layered silver-long chain alkylamine complex has been synthesized in the alcohol/water system for the first time, and such compound possesses the special sponge-like macroporous structure.

在本工作中,系列银-不同碳链长度的有机胺的配合物首次在醇-水体系中被合成获得,且该化合物具有特征性的海绵形貌中空结构。

Apparent partition coefficient in octanol-water and binding percentage to BSA of ~(153)Sm-NTMP,~(153)Sm-HEDTMP,~(153)Sm-DCTMP,~(153)Sm-EDTMP,~(153)Sm-DTPMP,~(113,117) Sn~m-EDTMP,~(113,117) Sn~m-HEDTMP,~(113,117) Sn~m-DTPMP are measured. The results show that there is a linear relationship between the relative magnitude of the apparent partition coefficient in octanol-watetr and the relative magnitude of the binding percentage to BSA of these ~(153)Sm~(113,117Sn~m complexes.

测定了NTMP,HEDTMPN (羟乙基乙二胺基三亚甲基膦酸,DCTMP(1,2 环己二胺四亚甲基膦酸),EDTMP(乙基二胺基四亚甲基膦酸),DTPMP(二乙基三胺基五亚甲基膦酸)的153Sm配合物以及HEDTMP,EDTMP,DTPMP的113,117Snm配合物在正辛醇水中的表观脂水分配系数和在0 5%牛血清白蛋白水溶液中与BSA的结合率。

In order to investigate the influence of magnetic field on the vapor-liquid equilibrium of binary azeotrope,the vapor-liquid equilibrium of n-butanol-water system was studied under magnetic field with different magnetic induction intensity.

为探讨磁场对二元共沸物系汽液平衡的影响,在不同磁感应强度的磁场中,研究了正丁醇-水物系的汽液平衡。

Result The number of diarrhea in each group administered bayberry extracts was reduced, with the effect of the ethanol extract being stronger than that of water extract.

结果 灌胃杨梅果实提取物的小鼠的腹泻次数均有明显的下降,且醇提物的作用效果要好于水提物。

The result of drip test (The height is 20 cm) was that the bibulous speed was 4 to 5 seconds.

先用4公升实验室的管道自来水,与40克洛醇配成水溶液,剪一块30 x 50 cm 的布料,以手工操作,30分钟后,再换4公升新配的水溶液,30分钟后,再换4公升新配的水溶液,30分钟后烘乾,经检查,棉子売清除达98%,滴水测试结果是(高度20 cm )吸水速度4 -5秒,白度接近6。

The effects of sodium laurylsulfonate and butanol on upper critical solution temperature s for water-phenol were studied by means of cloud point.

浊点法研究了十二烷基磺酸钠和正丁醇对水-苯酚系统上临界溶解温度的影响,结果发现在试验的浓度范围内,该系统的上临界溶解温度随十二烷基磺酸钠质量分数的增大而线性下降。

The optimum conditions were determined as follows:the molar ratio of butyraldehyde to glycol was 1∶1.6,the mass ratio of catalyst to reactants was 0.4%,the volume of cyclohexane as the water-carrying agent was 10 mL,and the reaction time was 60 min.

结果表明,磷钨钼杂多酸对合成丁醛乙二醇缩醛有较好的催化活性,适宜的反应条件如下:n∶n=1∶1.6、催化剂用量为反应物料总质量的0.4%、带水剂环己烷用量为10 mL、反应时间为60 min。

The results showed that new-type solid ferric potassium alum was a good catalyst for the synthesis of ethyl decanoate and the optimum conditions were as follows: molar ratio of acid to alcohol was 1∶2, the use level of catalyst was 0.6 g/0.05 mol capric acid, water-taking reagent benzene was...

结果表明,新型固体酸铁钾矾是合成癸酸乙酯的良好催化剂,在酸醇物质的量比为1∶2,催化剂用量为0.6g(0.05mol癸酸),带水剂苯为15mL,反应时间为2.5h的条件下,癸酸乙酯的酯化率可达98%。

The results showed that new-type solid ferric potassium alum was a good catalyst for the synthesis of ethyl decanoate and the optimum conditions were as follows: molar ratio of acid to alcohol was 1:2, the use level of catalyst was 0.6g/0.05 mol capric acid, water-taking reagent benzene was 15 mL, reaction time was 2.5 h and the yield of ethyl decanoate could reach 98%.

结果表明,新型固体酸铁钾矾是合成葵酸乙酯的良好催化剂,在酸醇物质的量比为1:2,催化剂用量为0.69(0.05 mol癸酸),带水剂苯为15mL,反应时间为2.5h的条件下,癸酸乙酯的酯化率可达98%。

The effects of the length of alkyl-chain,the polar group and the number of carboxyl group on rust-inhibiting properties and solubility were investigated in systematically.

合成并研究了水溶性有机羧酸醇铵盐类防锈剂,系统地考察了烷链的长度、极性基团、羧基的个数对防锈性能和溶解度的影响。

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