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Meanwhile, several physicochemical descriptors of xanthone molecules were calculated by using quantum chemistry method.

同时,运用量子化学计算了山酮分子的物化参数,并选择相互作用能、疏水常数(log P;其中P为正辛醇-水分配系数)和山酮分子总能量作为分析结构-电泳迁移定量关系的物化参数,用以研究分离机制及在毛细管区带电泳分离中山酮类化合物与β-CD 和磺酸化β-CD间的分子识别过程。

Meanwhile, several physicochemical descriptors of xanthone molecules were calculated by using quantum chemistry method. Among the physicochemical parameters, interaction energy, the logarithms of octanol-water partition coefficient and total energy of xanthone molecules were selected to investigate the separation mechanism and describe molecular recognition process between the xanthones and the CDs in CZE by means of quantitative structure-electromigration relationships.

同时,运用量子化学计算了山酮分子的物化参数,并选择相互作用能、疏水常数(log P;其中P为正辛醇-水分配系数)和山酮分子总能量作为分析结构-电泳迁移定量关系的物化参数,用以研究分离机制及在毛细管区带电泳分离中山酮类化合物与β-CD 和磺酸化β-CD间的分子识别过程。

The results show that the dehydration efficiency improves with the increase of the amount of butanol during the continuous distillation dehydration process;the first four coordinated water molecules in bischofite can be more easily taken away than the last two coordinated water molecules,especially the last one;the ultrasonic pretreatment of the bischofite bu...

研究结果表明:在连续蒸馏法脱水过程中,水氯镁石的脱水率随着丁醇用量的增加而提高;水氯镁石最初4个结晶水分子较容易脱除,后2个结晶水特别是最后1个结晶水难以脱除。

Pyruvaldehyde was synthesized with acetone or 1,2 propanediol as starting material respectively.With n∶n=1 00∶0 79,3 0-4 0 g potassium chlorate as catalyst,and water and glacial acetic acid as solvent,refluxing on water bath of 60-75 ℃ for 4 h,bromoacetone was obtained in 63 5% yield.

分别用丙酮和 1,2 丙二醇做原料合成了丙酮醛。n∶n =1 0 0∶0 79,加入 3 0~4 0g氯酸钾做催化剂,水和冰醋酸做溶剂,水浴温度为 6 0~ 75℃,回流 4h ,制得产率为 6 3 5 %的溴丙酮。V∶V =11 9∶1 0 ,通入空气,在 6 5~ 70℃反应 5~ 8h ,制得产率为 5 9 6 %的丙酮醛。

Not only could the ethanol decoction reserve the characters of the water decoction, reducing the carene and pinene, but also it enriched the terpenes and reduced the fatty acids in the water decoction.

YL2000醇提制剂保留了水煎降低蒎烯和蒈烯含量的特点,而且进一步富集了水煎剂中的萜类有效成分,降低了脂肪酸类成分。

The aim of this study was to examine the possible antioxidant and antiproliferative activities of the ethanol and water extracts of four Hydrocotyle species from Taiwan. ABTS radical monocation scavenging, FRAP method, DPPH radical scavenging, reducing power method, total polyphenol content, total The results showed that the water extracts of all the samples had higher antioxidant and antiproliferative activities than the ethanol extracts.

本实验针对台湾产四种天胡荽属植物之水萃取物及乙醇萃取物进行抗氧化及抗增生活性研究,分析方法包括ABTS自由基的清除、FRAP方法、DPPH自由基的清除、还原力、总多酚类含量、总类黄酮类含量、总黄酮醇类含量以及癌细胞增生之抑制,结果显示所有样品的水萃取物之抗氧化及抗增生活性皆大於乙醇萃取物,但在抗氧化活性方面,所有受测样品活性皆小於正对照组。

The samples of free amino acids were prepared from bee-collected pollens of codo-nopsis pilosula, brassica campestris, typha angustifilia and papaver, through extraction with ethanol-water solution and further purified by ion-exchange chromatographic columns.

本文以党参、油菜、水烛及罂粟等4种植物的蜂集花粉进行醇—水提取,经离子交换柱后得到游离氨基酸样品,提取后的花粉残渣以6ml/l盐酸封管水解制得结合氨基酸样品。

Benzyl acetate was synthesized from acetic acid and benzyl alcohol as raw materials with phosphotungstic acid as catalyst.

介绍了以冰乙酸和苯甲醇为原料,采用磷钨酸作催化剂合成乙酸苄酯的方法,考察了反应物醇酸摩尔比、催化剂用量、带水剂用量、反应时间、带水剂品种、催化剂重复使用对酯化率的影响。

The steady state kinetics of the lignin peroxidase catalyzed oxidation of veratryl alcohol by H2O2 in a sodium bis(2-ethylhexyl) sulfosuccinate/isooctane/toluene/water reverse micellar medium was studied and a comparison with the corresponding aqueous medium was made to understand the effect of the reverse micellar medium on the catalytic mechanism and kinetic parameters.

为了理解木素过氧化物酶在反胶束介质中的催化性能与动力学行为,本文以LiP催化过氧化氢氧化藜芦醇反应为模型反应,研究了2-乙基己基琥珀酸磺酸钠/异辛烷/甲苯/水反胶束中上述模型反应的稳态动力学并与水介质做了比较。

Based on " Green" chemistry , this paper mainly reviewed the latest research advance of the hydrotalcite-like materials and their derived composite oxides as an excellent solid base catalyst used in aldol condensation, Knoevenagel condensation, Michael addition, transesterification reactions and so on.

以绿色化学为基础,综述了类水滑石及其以类水滑石为前驱体衍生的复合氧化物作为一类优异的固体碱催化剂应用于醇醛缩合、克诺文诺盖尔缩合、麦克尔加成以及酯交换等反应的最新研究进展。

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