水醇的

TEM shows that drying by direct heating might result in hard aggregation of the tourmaline powder, while hard aggregation might be avoided by azeotropic distillation. Raman spectroscopy reveals that there are O_H and C_H on the surfaces of the tourmaline powder obtained by azeotropic distillation, which indicates that butoxy is chemically adsorbed on the surfaces of tourmaline particles, but not adsorbed on those formed by direct drying. X_ray powder diffraction shows that the intensity of diffraction peaks decreases after grinding. There is no damage to the tourmaline crystal lattice in the process of direct heating, azeotropic distillation, or ultrafine grinding.

透射电镜分析结果表明，直接加热脱去水或正丁醇会使电气石超细颗粒发生硬团聚，而共沸蒸馏法则可有效防止硬团聚的产生；拉曼光谱结果表明，共沸蒸馏法制备的电气石粉末表面存在O—H和C—H键，说明正丁醇在颗粒表面为化学吸附，而直接干燥法得到的电气石粉末表面则没有；X射线粉晶衍射结果表明，研磨过程降低了粉末衍射峰的强度，但直接加热干燥和共沸蒸馏干燥均未破坏电气石的晶格结构。

A method for the preparation of microcellular elastomeric polyurethane foams from a reaction mixture comprising a polyisocyanate component containing at least 85% by weight of 4,4'-diphenylmethane diisocyanate or a variant thereof, a polyol composition comprising at least one polyoxyalkylene polyol having an average nominal hydroxyl functionality of from 2 to 6, an average hydroxyl equivalent weight of at least 1300 and an average oxyethylene content of between 50 and 85% by weight, water, a chain extender having an average hydroxyl equivalent weight of from 15 to 250 and optionally a crosslinking agent, the hardblock-content being more than 45% by weight.

本发明是有关一种制备微孔弹性聚氨基甲酸酯泡沫体的方法，其反应混合物包括：一种含至少85重量％的4，4′－二苯甲烷二异氰酸酯或其变体的聚异氰酸酯组分，一种多元醇组合物，其包含至少一种平均标称羟基官能度从2至6、平均羟基当量至少1300且平均氧乙烯含量介于50至85重量％之间的聚氧亚烷基多元醇，水，一种平均羟基当量为15至250之增链剂，以及视需要使用的交联剂，该硬性嵌段－含量（hardblock-content）大于45重量％。

Moreover, taking the adsorption process from oven-dry state to the equilibrium state in 20℃,60%RH environment as an example, the dielectric relaxation based on the reorientation of adsorbed water molecules was separated out from that based on the methylol groups in the amorphous region of wood cell wall.

以绝干状态→20℃，60%RH 平衡态的吸湿过程为例，将基于吸着水分子回转取向运动的介电弛豫与基于木材无定形区中伯醇羟基回转取向运动的介电弛豫进行分离，并在 Eyring 的绝对速度反应论的基础上，求得了与吸着水分子进行回转取向运动相关连的热力学量，得到了在吸着过程中吸着水分子与木材吸着点之间的氢键结合随着水分吸着进程的变化情况。

Nevertheless, the yield of pinacol was also strongly affected by the steric environment surrounding the carbonyl group. The pinacol coupling of aromatic aldehydes has been achieved with high yields under such a condition. However, the diastereose-lectivities of pinacols were not satisfying. Unfortunately, the ketones and most aliphatic aldehydes appeared inert under the same reaction conditions.

然而， 呐偶合反应的产率受到羰基周围环境的立体位阻影响较大，在此条件下，锌粉能有效地促进芳香族醛类化合物进行水相呐偶合反应，得到的呐醇产率高，但非对映异构体选择性差，而脂肪族醛类化合物得到的呐醇产率较低，在同样的条件下，酮类化合物不能顺利进行呐偶合反应。

The effect of silicon atom in substrate on the reaction rate and the stereoselectivity of enzymatic reactions was revealed by comparison of horse liver alcohol dehydrogenase-catalyzed stereoselective dehydrogenation of the three isomers of acetyltrimethyl propanone and their carbon analogues in aqueous/organic biphasic systems.

本项目通过对比在水－有机溶剂两相系统中，马肝醇脱氢酶催化三甲基硅烷丙酮的三个异构体及其碳类似物的光学选择性脱氢反应，揭示了底物中的硅原子对酶反应速度、立体选择性的影响规律，成功地合成了高对映体纯度的手性有机硅醇，并实现了辅酶的再生。

Two 0.5-ml volumes of an isobutanol internal standard (10 mg/ml water; pipette 12.4 ml of isobutanol and dilute to 1 liter with water) are pipetted into two different 2-dram (7.4-ml) shell vials, one market "known."and the other "unknown."

将两份0.5毫升的异丁醇内标物(浓度为10mg/ml水，其配制法为：用吸量管吸取12.4ml 异丁醇用水稀释至1L )，用吸量管分别吸入两个不同的2-打兰(7.4毫升)的壳型小瓶中，一个标为&已知&，另一个标为&未知&。

The effect of hydrocarbon chain of co-surfactant,chlorpyrifos solution content,chlorpyrifos content in oil,temperature,and water hardness were investigated by surfactant/cosurfactent/oil/water pseudo-ternary phase diagram to evaluate the factor effect in forming chlorpyrifos microemulsion.

为考察各因素对毒死蜱微乳液形成规律的影响，系统研究了助表面活性剂直链醇碳链长度、毒死蜱溶液含量、油相中毒死蜱的含量、温度及水质对表面活性剂/直链醇/毒死蜱溶液/水体系拟三元相图的影响规律。

The trace amount of impurities,namely C5,tert-butyl alcohol,di-secondary butyl ether,methyl ethyl ketone and secondary butyl alcohol,in C4 hydrocarbon from butylene hydration tail gas were analysed by means of gas chromatograph with a column packed with sebaconitrile and polyethylene glycol-20M,and liquid-phase admission valve.

2m×4mm为填充柱，采用液相进样阀液态直接进样的填充柱气相色谱法分析了丁烯水合尾气C4烃中的C5、叔丁醇、二仲丁醚、甲乙酮及仲丁醇等微量杂质的含量。

Propanediol phenyl ether was synthesized from phenol and propylene oxide in the presence of a series of solid-based catalysts derived from hydrotalcite-like compounds. The effects of the composition and structure of the catalysts, and the reaction conditions on the synthesis of propanediol phenyl ether were studied.

以不同类水滑石化合物为前驱体制得的复合氧化物作为合成丙二醇苯醚反应的固体碱催化剂，考察了催化剂组成、结构及反应条件对催化合成丙二醇苯醚反应的影响。

In the paper, adsorption equilibrium and kinetics of water in the solvents of benzene series and low-carbon alcohol on 3A zeolite molecular sieve were studied including effective pore size of zeolite, adsorbate concentration and temperature. The mechanism and characteristics of water adsorption in such systems, the effect of solvents to adsorption equilibrium and kinetics of water were discussed, and diffusivities of water under different conditions were obtained.

论文研究了苯系列物质—水体系、低碳醇—水体系中水在3A沸石上的吸附动力学，考察了沸石晶格窗口大小、吸附质浓度、温度等因素对吸附动力学的影响规律；分析了吸附机理以及两类体系的特点；通过数学模型对实验数据的拟合，求取了各种条件下的动力学参数；研究了两类体系的溶剂对吸附平衡和动力学的影响。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。