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The aliquot was determined and confirmed by gas chromatography-negative chemical ionization mass spectrometry using external standard method.

样品中三唑醇残留物由正己烷饱和的乙腈(含1%冰醋酸)提取,加入无水硫酸镁与无水醋酸钠振荡促使提取液分层后进行固相分散萃取净化,用气相色谱-负化学离子源质谱法进行测定与确证,外标法定量。

The effects of anhydrous alcohol,dispersant and water on the quality and storage stability of the No.

试验研究了无水乙醇、分散剂和水对含醇汽油质量及贮存稳定性的影响。

A kind of water-soluble adhesive was made by mixed modified rosin with Polyvinyl butyral .

用丙烯酸对松香改性制得水溶性的改性松香增粘剂,再与聚乙烯醇缩丁醛共聚制得水溶性胶粘剂。

With the application of Partial Least Square technique and the input need of only 2-D molecular structure, it overcomes the difficulty of conformer alignment for 3D-QSAR techniques and avoids the multiple collinearity for traditional Multiple Linear Regression.

本文应用基于分子全息的QSAR技术研究了联苯以及209种氯代同系物的水溶解度、正辛醇水分配系数、总分子表面积、水活度系数和亨利常数等5种与生物累积性有关的理化性质以及气相色谱相对保留时间,建立了一批具有高度预测性的QSAR模型。

Based on the market demands,the trend of pine chemicals'developmet and our own foundation of technology and economy,we developed this series products, includ hydrogenated rosin、high-hydrogenated rosin、water-white hydrogenated rosin、water-white rosin、glycerol ester of hydrogenated rosin、pentaerythritol ester of hydrogenated rosin、methanol ester of hydrogenated rosin etc.

本公司基于市场需求、国内外发展趋势以及自身的技术和经济基础,开发了氢化松香系列产品,包括氢化松香、高度氢化松香、水白氢化松香、水白松香、氢化松香甘油酯、氢化松香季戊四醇酯、食品级氢化松香甘油酯、氢化松香甲酯等。

The optimal conditions for extraction of saponins PD from Akebia trifoliate were as follows: 80 ml of 70% ethanol, 90 min action duration, then extractived by n-butyl alcohol for 3 times, hydrolyzed with 36% hydrochloric acid for 4 h at 70%, and extractived by chloroform.

结论]三叶木通中常春藤皂苷的最佳提取工艺为:70%甲醇溶液80 ml超声提取90 min,水饱和正丁醇萃取3次,36%盐酸4 ml,70℃水浴回流水解4 h,氯仿萃取2次,合并氯仿层,旋转蒸干后甲醇溶解定容。

Its structure was characterized by FT-IR, 1H NMR and MS. Solubility data of betulin and 3, 28-di-O-glutaryl-betulin in acetone, ethanol, water and phosphate-buffered saline (PBS, pH value 7.4) were determined by equilibrium method.

采用FT-IR、1H NMR和MS对产物进行结构表征,并且选用平衡法测定了桦木醇和桦木醇戊二酸酯在丙酮、无水乙醇、水和磷酸盐缓冲溶液(PBS, pH值7.4,)等不同溶剂中的溶解度。

Cyclopentanol was synthesized from cyclopentene and water through hydration reaction using HNb3O8·H2O/SiO2 as main catalyst and tris(dioxa-3,6-heptyl)amine (TDA-1) as cocatalyst.

在以硅胶负载铌酸为主催化剂、三(3,6-二氧杂庚基)胺为助催化剂的作用下,以环戊烯和水为原料,通过水合加成反应合成了环戊醇。

Five Co-B amorphous alloy catalysts were prepared by chemical reduction in different media, including pure water and pure ethanol as well as the mixture of ethanol and water with variable ethanol content. Their catalytic properties were evaluated using liquid phase furfural hydrogenation to furfuryl alcohol as the probe reaction.

采用化学还原法在不同介质中制备了5种Co-B非晶态合金催化剂,反应介质包括水、乙醇以及不同乙醇含量的乙醇-水混合溶液,并以液相糠醛加氢制备糠醇为探针反应考察了其催化性能。

Esterification of sorbitan and oleic acid can be carried out by lipase CAL in nonaqueous phase under mild conditions.

失水山梨醇单油酸酯作为一种重要的非离子表面活性剂,可利用脂肪酶在非水相中合成[1] 。

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