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A novel type of amphiphilic tri-block copolymers with both pH and temperature sensitiveness: poly-poly (dimethylamino ethyl methacrylate)-poly (ε-caprolactone)(PEG-PDMAEMA-PCL) was synthesized via sequential oxyanionic polymerization of macro-molecular: PEG, with a hydroxyl at one end, and dimethylamino ethyl methacrylate andε-caprolactone, with the potassium naphthalene as the initiator.

在本文中,报道了一类新型的兼具pH和温度敏感的双亲性嵌段共聚物:聚乙二醇-聚甲基丙烯酸N,N-二甲氨基乙酯-聚己内酯(PEG-PDMAEMA-PCL)及聚甲基丙烯酸N,N-二甲氨基乙酯-聚己内酯(PDMAEMA-PCL)的制备;并利用动态光散射和氢核磁共振光谱(~1H NMR)对该嵌段共聚物的水溶液性质进行研究;在此研究结果的基础上,初步探讨了其在仿生物矿化中的应用。

The influence on the diffraction efficiency and the noise of diffusion was discussed when use dimethylbenzene and saturated sucrose solution as matching liquid. And the angular excursion of the reconstructed light beam caused by the two kinds of matching liquid was discussed in this paper.

对使用二甲苯及饱和蔗糖水溶液作为匹配液对漫射噪声及衍射效率的影响,以及带来的再现光角度的偏移进行了讨论。

The main contents as following:1 Phase separation ability of dipotassium hydrogen phosphate solution was investigated on the conditions of different solvent, different temperature, different pH value and little additional sodium chloride.

实验结果表明:在相同条件下,异丙醇的分相能力大于乙醇;温度对磷酸氢二钾+乙醇/异丙醇+水体系分相能力的影响很小;磷酸氢二钾水溶液的pH值对体系的分相能力影响较大,当pH值较小时,体系不能形成两相,当pH值>6时,随着pH值的升高,分相能力逐渐增强;外加少量无机盐NaCl,对体系的分相能力影响不大。

Influence of oxygen content of IEP and dispersity of silicon carbide fine powder and mechanism for its dispersity were studied.

摘 要 研究了氧含量对碳化硅微粉的等电点和分散性的影响,同时讨论了SiC粉料在水溶液中的分散机制。

This paper mainly studied the synthesis and characterization of some dissymmetric bis-quaternary ammonium gemini surfactants, then determined the surface tensions of their water solutions, finally calculated their critical micelle concentrations and build a surface tension-concentration model.

本文主要研究了非对称型季铵盐双子表面活性剂的合成与表征,测定了其水溶液的表面张力,并计算出其临界胶束浓度。

The antimicrobial test and researched was done on wide distillation of different solvents on Terpenoid, polarity separation of ethanol distillable substance, thin layer chromatography of different polarities and distillation of amylase. The results showed that the active substance distilled by 95% ethanol and V methanol: toluene=3:1 had stronger antimicrobial activity on Agaricus blazei Murrill. The antimicrobial activity of ethyl acetate was stronger than wide distilling substance with ethanol, but the water part has not antimicrobial effect. Two straps of ethyl acetate phase(Rf0.57、Rf0.63)(0.1g/ml)had stronger antimicrobial activity on Agaricus blazei Murrill, the antimicrobial zone on Pseudomonas was 19.3mm. The bacteriostatic activity of chromatography strap of water phase was rather weaker, the water solution (0.5g/g) of amylase had better effect on pathogenic fungus of Agaricus blazei Murrill, its antimicrobial zone on Aspergillus niger, Citrinin, Trichoderma viride were 10.8 mm, 7.9 mm, 5.3 mm.

通过对日本凹顶藻以不同溶剂的粗提、乙醇提取物的极性分离、不同极性的薄层层析和多糖的提取,进行抗菌试验的研究,发现95%乙醇和V甲醇:甲苯为3∶1的提取的活性物质具有较强的抗姬松茸的病原细菌活性,乙酸乙酯相对病原细菌的抑菌强于乙醇的粗提物,而水相基本无抑菌效果,乙酸乙酯相的两个带(Rf0.57、Rf0.63)浓度为0.1g/ml具有较强抗姬松茸病原细菌的活性,对假单孢杆菌抑菌圈达到19.3mm,水相层析带的抑菌活性较弱,多糖的粗提物配成0.25g/g的水溶液对姬松茸病原真菌有较好的抑菌效果对黑曲霉、桔青霉和绿色木霉的抑菌圈分别达到10.8 mm、7.9 mm、5.3 mm。

The mechanism of dioxygen oxidation of 4-nitrotoluene-2-sulfonic acid to 4,4'-dinitrostilbene-2,2'-disulfonic acid in alkali solution under mild condition was investigated.

探讨了在温和条件下在碱的水溶液中氧气液相氧化 4-硝基甲苯- 2 -磺酸制取 4,4'-二硝基二苯乙烯- 2 ,2 '-二磺酸的反应机理,发现 4-硝基甲苯- 2 -磺酸在碱作用下发生离子化生成 4-硝基- 2 -磺酸基苄基阴离子,然后被活化的分子氧氧化成 4-硝基- 2 -磺酸基苄基自由基是反应的关键步骤。

The product is in the pore structure on the graft copolymer of styrene divinyl benzene [-N amines (CH 3) 2 The ion exchange resin], the less alkaline, in the acidic, neutral and effective exchange of inorganic acid medium. and the larger size can be adsorbed molecules in aqueous solution and the use of anion.

本产品是在大孔结构的苯乙烯二乙烯苯共聚体上接枝叔胺基[-N(CH3)2]的离子交换树脂,其碱性较弱,能在酸性、近中性介质中有效地交换无机酸,并能吸附分子尺寸较大的阴离子以及在非水溶液中使用。

The extraction equilibrium constants of Nd , Eu , Am in the system of seven monoacidic organophosphorus compounds dodecane 1. 0mol/l NO〓are reported. The dependency of the extractability on the PO〓function group、bonding charactor、metallic ion species and the structure of substitute has been examined.

给出了七个烷基磷酸的正十二烷熔液从1.0mol/lNO〓水溶液中萃取Nd、Eu、Am的平衡分配常数Kex,考察了萃取剂PO〓官能团、萃合物成键特性、金属离子及取代基结构与萃取性能间的关系,发现了:(1)可运用取代基自由能加和模型预测辛基膦酸辛基酯对La、Eu、Nd、Am等三价离子的平衡分配数据。

It indicates that the absorption amount and rate of Cd2+ in eichhornia crassipes solution enhanced with an increase of reaction time.

水葫芦在含5 mg/L Cd2+的水溶液中能继续生长,其对Cd2+的吸收量及吸收率随时间的延长而增加。

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This paper analyzes the compound attractor structure of a new three-dimensional autonomous chaotic system.

分析了一种新的三维自治混沌系统吸引子的复合结构。

ON shut rivals out of their transmission systems and shy away from reinvesting their profits in network improvements.

ON将竞争者挡在了其输送体系之后,并不愿将其收益再投资于网络改建工作。

Objective: Elucidate the medicinal licorice species circumscription in order to develop licorice resources in China and select new cultivars.

目的:阐明中国药用甘草物种之间的界限,为甘草资源开发和优良品种选育奠定基础。