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A two-fold penetration coordination polymer n (1)(bpy=4,4'-bipyridyl) has been synthesized through hydrothermal reaction and structurally characterized by single crystal X-ray diffraction method.

利用水热反应,合成了一个具有二重穿插结构的一价铜配位聚合物n(1)(bpy=4,4'-联吡啶),并利用元素分析,X射线单晶衍射,红外光谱以及热重分析等手段对标题化合物进行了表征。

The dehydration technology of bischofite by butanol complexation distillation was studied by such methods as X-ray diffraction and elementary analysis.

摘 要:采用X射线衍射及元素分析方法研究了水氯镁石的丁醇络合蒸馏脱水工艺。

A novel planar chiral diferrocenylimine-diols 6 was synthesized by the condensation of R, S(subscript p-1-(2-diphenyl hydroxyl methyl) ferrocenylethylamine [R, S(subscript p-4] with phthaldehyde in anhydrous ethanol, and was crystallographically characterized.

通过R,S(下标 p-1-(2-二苯基羟甲基)二茂铁乙胺[R,S(下标 p-4]和对苯二甲醛在无水乙醇中的缩合反应合成了一种新型平面手性双二茂铁亚胺二醇化合物6,并经X-射线衍射分析它的晶体结构。

FT-IR spectra shows that the polyaniline is present primarily in the emeraldine salt form, and the polymeric chains interact with inorganic framework, most likely via V=O…HN hydrogen bonding. XRD,TG and DSC indicate that the lamellar structure of the V_2O_5 is preserved, PAn chains eliminate water form the interlamellar region and are partially inserted between the layers, and exist with extended-chain conformation owing to the confined environment.Electrochemical investigation in the range of 1.8~3.8V vs.

红外光谱表明复合物中PAn主要以导电聚苯胺盐的形式存在,PAn链与V_2O_5晶格之间可能形成了V=O…HN氢键。X射线衍射、热重和差示扫描量热证实了PAn/V_2O_5复合物保持了较规整的层间排列结构,PAn取代了V_2O_5干凝胶中的层间水而部分嵌入其片层间,由于受空间的限制,PAn分子链以比较伸展的链构象存在。

Hot corrosion behavior of Na2SO_4 coated B-1900 alloy was studied in air at 827 and 750℃.Corrosion kinetics of the coated alloy was gravimetrically measured,and contents of water soluble ions in the reaction products were chemically analyzed.X-ray diffraction and EMP techniques were employed to determine the components and morphology of the corrosion product scale.

用涂 Na_2SO_4盐膜法研究高温合金 B-1900在827℃和750℃于空气中的热腐蚀行为,测定其腐蚀动力学曲线,用 X -射线衍射和电子探针元素面扫描方法分析腐蚀产物的相组成和成份,还对其中的水溶性离子进行化学定量分析。

One theory was that rifle fire from the Housatonic had put a hole in the Hunley, flooding it.

有种说法趁,从HOUSATONIC号发散出来的火焰射穿了杭力号,使其进水。

The mechanisms of phosphate sorption on hydrotalcite and its calcined product are different, which has been confirmed by X-ray diffraction examination.

水滑石及其焙烧产物对磷的吸附具有不同的机理,并得到了X射线衍射的证实。

Based on the theory of radio-freqency impendence, the dielectric constant of water is much greater than that of oil, so they show different properties in the respect of radio impedance.

水的介电常数远大于油的介电常数,因而两者呈现不同的射频阻抗是油品含水量测量的理论依据。

The total of 36 compounds were characterized by X-ray single crystal diffraction, EA, TG, IR, luminescence, adsorption, XPS, powder XRD, M〓ssbauer spectra, EPR, magnetical measurements.

本论文利用水热法,成功设计和合成出三个系列Ln-M(M=Mn〓,Fe〓,Ag〓)共23个未见文献报道的稀土—过渡混合金属配位聚合物,同时也得到了结构新颖的仅含稀土或两种不同过渡金属的从一维到三维的聚合物13个,并对它们进行了结构、元素分析、热重分析、红外光谱、荧光、吸附、磁性、光电子能谱、粉末衍射和M〓ssbauer谱等表征。

Single-crystalline cerium orthovanadate (CeVO4) nanorods are synthesized successfully by Na2EDTA-assisted hydrothermal method. The products are characterized using X-ray diffraction, transmission electron microscopy, high-resolution transmission electron microscopy and superconducting quantum interference device.

以Na2EDTA为模板导向剂,利用水热法成功合成了单晶CeVO4纳米棒,使用X射线衍射仪、透射电镜、高分辨透射电镜和超导量子磁强计等对产物的结构和磁学性能进行了表征。

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