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In other part stood one who at the Forge Labouring, two massie clods of Iron and Brass [ 565 ] Had melted (whether found where casual fire Had wasted woods on Mountain or in Vale, Down to the veins of Earth, thence gliding hot To som Caves mouth, or whether washt by stream From underground) the liquid Ore he dreind [ 570 ] Into fit moulds prepar'd; from which he formd First his own Tooles; then, what might else be wrought Fusil or grav'n in mettle.

他们那飞快的弹拨,通过高低音阶的协和,得心应手地奏出奔腾浩荡回环激荡,余音袅袅的旋律。另一方,一个把铁在熔炉旁劳动和青铜熔合的汉子。那流动的矿水被注进备好的模子里。从模子里,他们首先造出自己的劳动工具,其次,铸造或雕刻其他各种金属物品。

The method comprises:(1) weighing lead acetate hexahydrate and thioacetamide, and preparing aqueous solutions respectively, so that the concentration ratio of Pd2+ to S is 1:(1-4);(2) adding acetic acid into thioacetamide solution to adjust the pH value to 2-4;(3) adding poly surfactant into lead acetate solution, ultrasonicating to mix uniformly and obtain a colorless and transparent sol;(4) mixing the sol and thioacetamide solution;(5) placing the mixed solution in a sealed container, irradiating by 2.5 MeV and 40 mA electron accelerator with irradiation dose of 25-40 Mrad;(6) washing the product, centrifuging for separation, and drying to obtain black PdS nanoparticles.

本发明方法的工艺过程如下:首先称取一定量的六水合醋酸铅和硫代乙酰胺,各自配制成水溶液,其浓度比为使其中的铅离子浓度与硫原子浓度的比例为1∶1~1∶4;在硫代乙酰胺溶液中加入适量醋酸调节其pH值至2~4;醋酸铅溶液中加入少量表面活性剂聚乙烯醇,然后超声振荡,混合均匀,制成无色透明溶胶;随后将溶胶与上述的硫代乙酰胺溶液混合;将该混合液置于密闭容器中,并将其放置于2.5MeV、40mA的电子加速器产生的电子束辐照下进行辐照处理,其辐照剂量为25~40Mrad;然后将反应生成物清洗,并用高速离心机离心分离,然后干燥,最终得到黑色纳米硫化铅颗粒。

The effects of different factors on the laser-induced graft polymerization on the PET surface were analyzed, and the mechanisms were discussed. The factors were: 1 Monomers with smaller molecules resulted in better modification than polymeric monomers. Acrylamide monomer was chosen as hydrophilic modifier finally; 2 Higher concentration of the monomer solution favored the graft reaction; 3 With the increasing laser fluence, the surface hydrophilicity of PET films increased at first, then decreased. More laser pulses led to a more hydrophilic surface; 4 Benzophenone as a photosensitizer hindered the graft polymerization; 5 The homopolymer retardant of ammonium iron sulfate hexahydrate in a proper concentration retarded the formation of homopolymers and promotes the graft copolymerization; 6 The solvent of monomer solution also affected the graft reaction. Different solvents functioned in different ways. Ethanol can promote the graft reaction because of the activity of hydrogen in its structure; 7 pH value of the monomer solution affects the polymerization rate, and a lower pH value was favorable to the graft reaction.

这些影响因素的作用分别为:1小分子单体的表面改性效果好,确定以丙烯酰胺为亲水性改性单体;2较高的单体溶液浓度有利于接枝反应;3激光能量密度增大,薄膜表面亲水性先显著增强,后又减弱;激光脉冲次数越多,改性后表面亲水性越强;4光敏剂BP对PET表面接枝聚合反应有阻碍作用;5适当浓度的均聚物抑制剂六水合硫酸铁铵能减少单体均聚物的生成,促进接枝聚合;6单体溶液的溶剂也影响接枝聚合的反应进程,不同溶剂的影响作用原理不同,含较活泼氢的乙醇能促进接枝反应;7溶液pH值影响单体聚合速率,pH值较低有利于接枝反应。

Meanwhile with increasing the total amount of leaching water (250mL~750mL), the gross of 5Zr in leaching water changed indistinctively, which indicated that once 95Zr was absorbed by soils, it was very difficult to unbind by water.

刁。4cm土层范围内,红黄壤和海泥则分别为%。02%一97.16%和95.94%~98.01%;(3)随淋溶水盐度的增加,表层土(0一0.2cm)中952:的量明显提高,表明水体盐度增加有助于提高土壤对952:的吸附率。3、研究了卿鱼对952:的吸收和在其体内的分布动态以及95Zr在水生生态系统中的行为特性,并运用非线性拟合方法建立其数学模型。

Then, the quasi-overconsolidation ratio is introduced to consider the effect of super pore pressure; and the fitting formulation is applied to consider the influence of shearing strain. The degenerated formulation of undrained strength of saturated loess is deduced at last; and its reasonableness is proved by the test results.

在此基础上,引入似超固结比的概念来考虑超孔隙水压力的影响,应用拟合公式来考虑剪切变形的影响,最终推导出了饱和黄土不排水强度的退化公式,与试验结果的对比证明了理论公式预测结果的合理性。

The chemistry behavior research of wollastonite indicated that the silicon-potassium fertilizer has a chemical active in organic acid.The factors affecting manurial effect of silicon-potassium fertilizer are not only soil pH and desilicification,but also content and type of organ in the soil.Wollastonite chemistry behavior indicates that silicic acid can be dissolved out from silicon-potassium fertilizer in chlorhydric acid solution if pH of solution is not smaller than 2. The drop of apparent density,increase of DBP sorptive rate and specific surface for leavings indicate that hydrated silicon oxide is polyporous,and those mineralogic feature presignify that silicon-potassium fertilizer has a role of conservation of both Moisture and Fertility and improving soil structure.After active ingredient releasing,silicon-potassium fertilizer leaves half the substance (non-active ingredient)in soil.

熟料单矿物在酸溶液中的化学行为研究表明,硅钾肥矿物在有机弱酸中的化学活性较好,影响硅钾肥肥效发挥的因素是土壤pH值和土壤的去硅化程度,还有土壤有机质的含量与种类;硅灰石在盐酸溶液中化学行为表明,在反应体系pH不小于2的情况下,硅钾肥矿物大量溶出硅酸根组分;溶解残余物表观密度降低、DBP吸着率和比表面积增加表明水合二氧化硅是以多孔形式存在,为硅钾肥具有保水保肥、改良土壤结构的提供了矿物学依据。

Based on the deterioration mechanism of corrosive medium, a lot of polymer such as ternary-polymer, adding-felt addition, hydrophobe and polypropylene fiber were added to enhance the performance of anti-corrosion, anti-penetration, conglutination and anti-cracking of original cementious material. The microstrure of cementious material was changed from the simplex hydration product of cement to the superposition structure of the hydrolysate of polymer and the hydration product of cement. A lot of the corrosive ions were prevented from the interior of concrete by this stable structure. The results of tryout indicated that the mending material has the good effect at the corrosion form of corrosive medium.

根据介质腐蚀形式的劣化机理,该文以提高修补材料耐腐蚀性能、抗渗透性能、粘结性能和抗裂性能为出发点,采用添加有机硅改性三元共聚物、增粘剂、孔隙憎水剂等多种聚合物和聚丙烯纤维对原水泥基材料进行改性,使得修补材料的内部微观结构从单纯的水泥水化产物转变成聚合物和水泥水化产物叠合的空间网状结构,这种稳定的结构能有效抵抗各种介质离子的侵蚀,在实际工程上的试用也显示出新修补材料良好的使用效果。

We have presented a practical method for the preparation of propargylic alcohols from terminal alkynes and carbonyl compounds promoted by KOH in the presence of 18-crown-6,and subsequent efficient cyclizations of propargylic alcohols with 2-naphthol catalyzed by InCl_3·4H_2O under the solvent-free ball-milling conditions.Ball milling exhibits its superiority over the reported methods in the preparation of propargylic alcohols and naphthopyran derivatives.

采用机械研磨方法进行了连续的两步固相化学反应的研究:首先,在氢氧化钾和18-冠-6的作用下,端基炔和羰基化合物在机械研磨条件下反应可以高效地生成相应的炔醇化合物;其次,在四水合三氯化铟的催化作用下,生成的炔醇化合物和2-萘酚在机械研磨条件下环加成生成相应的萘并吡喃产物。

The result indicated that MgO and α- methacrylic acid can together thicken epoxy, and the speed of thickening epoxy become quickly with the increasing content of MgO; when the ratio of MgO and α- methacrylic acid is 3:1, thickening epoxy have a better effect; the thickening mechanism: the terminal corboxyl group of α- methacrylic acid react with MgO, and it accompany with large numbers of heat, the heat can accelerate the reaction between the terminal corboxyl group with the secondary hydroxyl groups of epoxy, intermolecular hydrogen bonding which the water of above-mentioned formation result in and complex compound which format the metal atoms and carbonyl group complexing collective increase the viscosity of epoxy resin.

结果表明:MgO和α-甲基丙烯酸配合可增稠环氧树脂,随着MgO加入量的增加,环氧树脂增稠的速度加快;MgO与α-甲基丙烯酸为3:1时,增稠环氧树脂的效果较好;推测环氧树脂的增稠机理是α-甲基丙烯酸中的端羧基与氧化镁反应,放出热量促使其端羧基与环氧树脂中的仲羟基反应,上述反应生成水产生的氢键和羰基与氧化镁中的金属原子形成络合物共同导致环氧树脂的粘度增加。

On base of liquid synthesis, the influence of various adulterations on calcination of hydrous titanium dioxide is investigated and the connection of various calcination programs and performance of titanium white is explored.

在液相合成的基础上,实验研究了不同掺杂条件对水合二氧化钛煅烧过程的影响,探索了不同煅烧程序与钛白性能之间的关系,制备出了性能优良的钛白原料,可供进一步加工成化纤钛白。

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By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候,里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色,卵在发育96h后卵基本全部孵化。

There was a conflict between plebs and patricians in ancient Rome in 494BC.

在公元前494年,罗马发生了一次平民反对贵族的斗争。