水凝胶

The Diels-Alder cycloadditions of [60] fullerene for preparation of optical limitingmaterials are discussed in chapter 3 and 6. Soluble cycloaddition derivatives of 〓aresynthesized by the reaction of 〓 with indene,1,1'-biindene andcyclopentadiene derivatives.〓Particular, the Diels-Alder cycloaddition of 〓 with1,1'-biindene under controlled conditions affords the stable monoadduct 〓〓of novel structure, which was confirmed by HPLC, FTIR, FD-MS,〓NMR,〓 NMR, HMQC and HMBC spectra, Its two bridgehead cage carbons resonate at70.91ppm, The 〓 NMR spectra showed 38 lines consistent with the 〓 symmetryassociated with [6,6] addition. The 〓 shows similar optical limitingproperties to that of 〓 in toluene for 8ns laser at wave length 532nm. Moreover, thehigh solubility of this adduct in polar solvents such as THF, acetone enables itsincorporation into sol-gel glass matrix. The thin films prepared via the sol-gel methodshow improved OL behaviour compared to those of 〓. The langmuir-Blodgett filmformation and uv-visible absorption of 〓 are also investigated. LBmonolayer of this compound is prepared on the air-water interface at 〓 mol/l. In chapter 4, three water-soluble derivatives of [60] fullerene: fullerol(1), theaddition product (2)of fullerol (1)with polyvinylpyrrolidone and fumaric acidderivative of 〓(3) are synthesized and characterized.

通过Diels-Alder环加成反应，用茚〓和1，1'-联茚〓及取代茂合成了一系列可溶性的〓环加成衍生物，发现可控制反应条件，使1，1'-联茚与〓反应，并高产率地得到具有新颖结构的单加成物，用HPLC、FTIR、FD-MS 及〓、HMQC、HMBC等多种波谱技术对其结构进行表征，测得它的两个〓杂化的桥头碳的化学位移为〓ppm，证明生成的衍生物为6∶6闭式环加成，〓NMR谱中共给出38个信号，表明〓联茚衍生物分子具有〓对称性；在波长532nm，脉冲宽度8ns的激光下，〓联茚衍生物的甲苯溶液的光限幅性能与〓的甲苯溶液相近，由于〓联茚单加成衍生物熱稳定性好，在四氢呋喃，丙酮等极性溶剂中溶解性好，能分别均匀地掺入溶胶-凝胶中，已发现它的溶胶(so1)光限幅性能优于纯〓的光限幅性能；使用Langmuir-Blodgett技术将〓联茚衍生物在空气和水的界面进行了LB单层膜和多层膜实验以及UV-Vis吸收谱研究，通过等温压缩曲线测试，证明浓度为〓〓时，〓联茚衍生物能够形成单层膜。

It is a topical intravaginal gel which is water soluble but has the property of remaining in the vagina for extended periods of time.

其为一种见水即溶的局部阴道内凝胶，但是具有能在阴道内保留较长时间的特点。

The standard data for mathematical model establishment come from the figure such as water content by Microcoulomb equipment, solid content by loss of weight of Volatilization and PTMEG relative molecular mass by Gel Chromatography.

建立校正模型的标准数据采用微库仑法测定水含量，挥发失重法测定固含量，凝胶色谱法测定PTMEG的数均相对分子质量。

The fermentation characteristics of W39 is as follows: it can yield in the liquid the insoluble gel-like cellulose only with the existence of oxygen. The forming of nata needs uncovered surface of static liquid.

研究了该菌在椰子水培养基上的发酵特性：经液态发酵产生不溶性的凝胶纤维素，且只在有氧生长时才合成纤维素；对无机盐和生长因子的要求复杂；用于纳塔生产时必须静置培养并保证液面与空气接触。

PES/NMP were used as the model membrane-forming system, H〓, 1butanol, and diethylene glycol (as well as isopropanol and ethylene glycol) was selected as nonsolvent additives.

本文选取PES/NMP为制膜体系，研究NSA——水、正丁醇、一缩二乙二醇在浸入凝胶成膜过程中的作用。

Organic substances (diethylene glycol, glycol methyl ether and methyl ethyl ketone) were used as nonsolvent additives and N-methyl-2-pyrrolidone used as a solvent in membrane preparation. The effects of PPESK concentration, the type of additives and the NSA concentration in casting solution on the morphology and performance of the PPESK hollow fiber ultrafiltration membrane were systematically investigated.

以PPESK为膜材料，NMP为溶剂，水为凝胶剂，选用乙二醇甲醚、一缩二乙二醇和丁酮为非溶剂添加剂，系统研究了聚合物浓度、添加剂种类和含量对PPESK中空纤维超滤膜结构和性能的影响，制备了一系列具有不同孔径和通量的中空纤维超滤膜。

METHODS: Using Gel chromotography, onionskin analysis and alcohol precipitant method to separate between protein and amino acid in liquor extract of Lingyangjiao Sai.

用凝胶色谱法，透析法和乙醇沉淀法对羚羊角塞水提液中蛋白质、氨基酸等进行分离。

Apple Pectin is a source of water soluble fiber which has a gel-forming effect when mixed with water.

苹果果胶是一种水溶性纤维，当与水分混合时具有形成凝胶的特性。

When A〓 is divinyl sulfone , and BB'〓 is 1-(2-aminoethyl) piperazine, no gelation was observed in water or organic solvents.

当A〓为二乙烯基砜，BB'〓为1-（2-胺乙基）哌嗪时反应在水和有机溶剂中都不会凝胶。

Optical and electrical properties of the pyrite films prepared in this way indicate the superiority of this combined method.

制备出的FeS_2薄膜的光学和电学性质表明了这种凝胶-溶胶水热法结合EPD沉积技术制备FeS_2薄膜方法的优越性。

It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发，分析对称连杆曲线上鲍尔点的产生条件，提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品，年生产总值3000万美元，产品价廉物美、选料上乘、质量保证，深受国内外客户的青睐