氯酸酯

Tris cyanurate as an excellent additional retardant was synthesized by using cyanuric chloride and 2,4,6-tribromophenol as starting materials in the presence of acid accepter.

本文以三溴苯酚和三聚氯氰为原料，在缚酸剂的存在下，合成了一种性能优良的添加型阻燃剂三三聚氰酸酯。

In the presence of NaH and in DMF, the acyclic crown ethers 1a and 1b were synthesized by the reaction of di-or triethyleneglycol ditosylate and o-methoxymethoxybenzyl alcohol, which was obtained from salicylaldehyde via the protection of the hydroxyl group with chloromethyl methyl ether followed by the reduction of the formyl group with NaBH4. The hydrolysis of 1a and 1b with dilute hydrochloric acid provided the diphenolic type acyclic crown ethers 2a and 2b respectively in good yield.

将水杨醛与碱和氯甲基甲基醚反应，再经过NaBH4还原，即制得邻苯甲醇，然后将其在DMF中与NaH和二甘醇二对甲苯磺酸酯反应，得开链冠醚1a和1b.1a和1b经稀酸水解，即脱保护而分别生成新的酚型开链冠醚2a和2b。

DFerric Perchloric acid method was used to determine the content of ester-series alkaloid, and acid dye colorimetry was used to determine the content of total alkaloid in Complex Prescription Monkshood plaster.

方法分别采用改良异羟肟酸铁－高氯酸铁法及酸性染料比色法测定制剂中的酯型生物碱及乌头类总生物碱的含量。

MethodsFerric Hydroxamic acid―Ferric Perchloric acid method was used to determine the content of ester-series alkaloid, and acid dye colorimetry was used to determine the content of total alkaloid in Complex Prescription Monkshood plaster.

方法分别采用改良异羟肟酸铁－高氯酸铁法及酸性染料比色法测定制剂中的酯型生物碱及乌头类总生物碱的含量。

Eight novel N,N′-naphthalene acyl substituted aromatic acylamino thiocarbamide s(Ⅱ1~Ⅱ8) were synthesized from aryl acylhydrazine and α-naphthalene acyl isothiocyanate, which was obtained by the reaction of potassium thiocyanate with α-naphthalene acyl chloride obtained from 2-naphthylacetic acid and thionyl chloride in anhydrous benzene.

通过α-萘乙酸和SOCl2在无水苯中反应制得α-萘乙酰氯，与硫氰酸钾反应生成α-萘乙酰基异硫氰酸酯，再与芳基酰肼进行加成反应，合成8种新型N，N′-萘乙酰基取代芳乙酰胺基硫脲类化合物(Ⅱ1～Ⅱ8)。

In this research, liposoluble chlorogenic laurate was synthesized by acylation with lauroyl chloride in the presence of triethylamine in non-water phase.

本研究对CGA进行了分子修饰，即在非水相中，以三乙胺为催化剂，对其进行月桂酰氯酰化，制备了脂溶性的绿原酸月桂酸酯。

Eight novel N,N′-naphthalene acyl substituted aromatic acylamino thiocarbamides(Ⅱ1~Ⅱ8) were synthesized from aryl acylhydrazine and α-naphthalene acyl isothiocyanate, which was obtained by the reaction of potassium thiocyanate with α-naphthalene acyl chloride obtained from 2-naphthylacetic acid and thionyl chloride in anhydrous benzene.

通过α-萘乙酸和SOCl2在无水苯中反应制得α-萘乙酰氯，与硫氰酸钾反应生成α-萘乙酰基异硫氰酸酯，再与芳基酰肼进行加成反应，合成8种新型N，N′-萘乙酰基取代芳乙酰胺基硫脲类化合物(Ⅱ1～Ⅱ8)。

Furfuryl propionate was synthesized from furfuryl alcohol and propionyl chloride using hexahydropyridine as catalyst and anhydrous sodium bicarbonate as acid-caputor.

以α呋喃甲醇和丙酰氯为原料，以六氢吡啶为催化剂，无水碳酸氢钠为缚酸剂合成了α呋喃甲醇丙酸酯。

Flame—retardant resin was prepared by the condensation and polymerization of phosphoric acid, trihydroxy methyl propane and epoxy chloropropane,the resin was then reacted with hexane diacid and diglycol under certain condition ,resulting in polyol containing 1.5% P and 17— 18% polyester polyol, which was foamed with polyisocyanate, water and catalyst by one— step method, producing fire...

通过磷酸、三羟甲基丙烷和环氧氯丙烷的缩合和聚合反应制得阻燃树脂，然后将它与己二酸、一缩二乙二醇在一定条件下反应制得含P1.5%和含Cl17～18%的聚酯多元醇，再将它与多异氰酸酯、水、催化剂等组分采用一步法发泡工艺制得阻燃聚氨酯软泡塑料。

In order to get the safe, non-leak, minitype and superthin capacitor, electric double layer capacitors of PAN-based gel polymer electrolytes by in-situ polymerization were prepared. In this EDLC, PC and EC were used as plasticizer, LiClO4 was used as the supporting electrolyte and activated carbons with the specific surface areas of 1000m2/g and 2600m2/g, respectively, as the electrode materials.

为了得到安全、无泄漏、微型、超薄型的双电层电容器，采用内聚合方法制得聚丙烯腈基凝胶聚合物电解质双电层电容器，电解质的增塑剂为碳酸丙烯酯和碳酸乙烯酯，支持电解质为高氯酸锂，电极材料分别为比表面积1000m2/g 和2600m2/g 的活性炭。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。