氯酸

The guaiacol methods of synthesizing vanillin mainly includes: nitroso group method, Glyoxalic acid method, formaldehyde method, Reimer-Tiemann method, Trichloroacetaldehyde acetochloralb method, electrolytic oxidation method.

愈创木酚法合成香兰素的方法主要有亚硝基法、乙醛酸法、甲醛法、Reimer-Tiemann法、三氯乙醛法、电解氧化法，本文综述了愈创木酚法合成香兰素的研究进展，并对愈创木酚法合成香兰素提出了展望。

Glyoxylic acid was prepared by reaction of sodium hydroxide surplus with methyl dichloroacetate in methanol solution via neutralization of filtrate with 50 percentage sulfuric acid to pH 2～3 and hydrolyzation after separation of salts.

二氯乙酸甲酯和过量的氢氧化钠在甲醇溶液中反应，滤出氯化钠后，直接加入适量的 5 0 %的硫酸调 pH值为 2～ 3，滤出硫酸钠，蒸馏回收甲醇，水解、浓缩，得到不含乙二醛的 4 0 %乙醛酸溶液。

Our results have shown that the analgesic effect of morphine administered to nucleus accumbens was blocked by intra-habenula injection of naloxone or ME antiserum, whereas the analgesic effect of morphine injected into habenula was attenuated by intra-PAG administration of naloxone or muscimol, and enhanced by bicuculline methochoride (BMC, an antagonist of GABA receptor).

本工作实验结果表明，在伏核内注射吗啡产生的镇痛作用可被缰核内注射NX或ME抗体所大部阻断，而缰核内注射吗啡产生的镇痛作用又可被PAG内注射NX或γ-氨基丁酸受体激动剂异鹅羔胺所削弱，被GABA受体阻断剂氯甲基荷包牡丹碱所增强。

This paperindicated that it was good for condensation reaction when benzene-ring bearingelectron-attaching groups. It also showed that and the 6-hydroxyl group could bereacted with acyl halide, haloid ether and halo alkene, but not with halo alkane. It wasnot only the first time to find that the reaction product of D-mannitol and aromaticaldehyde is tri-condensation derivatives, but also the first time to obtain thep-phthaldehyde-sorbitol derivatives containing eight hydroxyl groups.

研究发现：苯环上有吸电子基团时对缩合反应有利；多元醇缩醛衍生物6-羟基除与酰氯反应外，也能和卤代酸酯、溴代烯反应，但不与卤代烷反应；首次发现D-甘露醇与醛反应主要得到三缩合物；首次合成了含有8个羟基的对苯二甲醛和山梨醇的缩合物。

The method comprises following steps: reacting hydroxylation carbon nano-tube successively with reagent containing halogen and hydrosulphide to prepare sulfhydryl carbon nano-tube; reflowing the sulfhydryl carbon nano-tube and platinum salts in polyatomic alcohol, processing in hydrogen atmpsphere to obtain sulfhydryl anchoring platinum / carbon nano-tube catalyst; reflowing the sulfhydryl carbon nano-tube successively with the hydrochloroauric acid and the platinum salts in polyatomic alcohol, processing in hydrogen atmpsphere to obtain sulfhydryl anchoring platinum-gold / carbon nano-tube catalyst.

本发明将市售羟基化碳纳米管先后与含卤试剂和氢硫化物反应得到巯基化碳纳米管。再将巯基化碳纳米管与铂盐在多元醇中回流，氢气氛中处理得到巯基锚固铂/碳纳米管催化剂。将巯基化碳纳米管依次与氯金酸和铂盐在多元醇中回流，氢气氛中处理得到巯基锚固铂-金/碳纳米管催化剂。

Every patient received 2 mL of the mixture injection qd, intramuscularly for a course of 5 d.

进口双氯芬酸钠利多卡因注射液组67例。2组药物均为2mL，肌内注射，qd，疗程5d。

In searching for novel and high active fungicides with pyridyl moiety, with Dimethomorph as a model compound and isonicotinic acid as the main starting material, twenty-seven title compounds were designed and synthesized through chlorination, Friedel-Crafts acylation, Wittig-Horner reaction and other steps. All the target structures were confirmed via 1H NMR and elementary analysis.

为了寻找具有高活性的含吡啶杂环杀菌剂，以烯酸吗啉为模板化合物，以异烟酸为起始原料，通过卤代反应、Friedel-Crafts酰基化反应、Wittig-Homer反应等，将吡啶－4-基或2-氯吡啶－4-基引入到模板结构中，设计合成了27个4-［3-（吡啶－4-基）－3-取代苯基丙烯酰］吗啉类化合物，其结构通过1H NMR和元素分析确证。

In the presence of laurate inhibitor, positive excess charges would be carried on both stainless steel and carbon steel.

在加有月桂酸盐缓蚀剂的饱和CO_2的含氯离子介质中，不锈钢和碳钢表面均带有过剩正电荷。

Sodium laurate is not effective for carbon steel corrosion in CO_2-saturated solution containing Cl-, but it is effective for galvanic corrosion of galvanic couple (stainless steel/carbon steel).

月桂酸盐对碳钢在饱和CO_2的含氯离子介质中的腐蚀抑制效果较差，但对碳钢/不锈钢偶对的电偶腐蚀抑制效果较好。

A key intermediate of abacavir, named N-(2-amino-4,6-dichloro-5-pyrimidinyl) formamide was synthesized from diethyl malonate and guanidine hydrochloride. This method suits to industry for large scale. The materials are easy to get and very cheap.

2-氨基-4，6-二氯-5-甲酰氨基嘧啶是合成阿巴卡韦的关键中间体，本文拟以丙二酸二乙酯和盐酸胍为起始原料合成这一关键中间体，具有原料来源广，适合大规模生产等优点。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。