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By using the a device being similar to water segregator and by controlling the temperature, cyclization of the intermediate product in chloroform reduced carbonization and gave 2-dodecaneanthraquinane in 68.1% yielding.

以十二烷基苯和苯酐为起始原料,经酰基化、关环和磺化三步反应合成了3-十二烷基蒽醌磺酸;并进一步改进和优化了合成工艺条件:即在催化剂三氯化铝过量50%并有三乙胺存在的条件下,中间体2-(4-十二烷基苯甲酰基)苯甲酸收率为72.45%;关环反应采用氯仿作溶剂,利用类似分水器的装置有效控制反应温度以减少碳化,2-十二烷基蒽醌的收率为68.1%。

Western blot was used to measure HSP70 of ischemia and non-ischemia myocardium and the expression of HSP70 was analyzed semiquantitatively.

采用蛋白质免疫印迹法检测各组缺血区和非缺血区心肌组织HSP70含量,并检测血清一氧化氯、丙二醛含量及总超氧化物歧化酶、肌酸激酶活性变化。

Mainly engaged in fine chemicals, chemical reagents precious metals, silver nitrate, the acid chloride, potassium cyanide-gold, Sulfite the salt, molecular Silver, silver, industrial ethanol, chemical reagents sulfuric acid, hydrochloric acid, nitric acid, ethanol and 95 percent ethanol and chemical reagents and other electronic products research and production.

主要从事精细化工,贵金属化学试剂,硝酸银,氯金酸,氰化亚金钾,亚硫酸金盐,分子银浆,银粉,工业无水乙醇,化学试剂硫酸,盐酸,硝酸,无水乙醇,95%乙醇等电子和化学试剂产品研究与生产。

ShTat1.3 and ShTat1.5 are two variable antigen types of a cloning Anhui strain of Trypanosoma evansi.Total RNA of the two variable antigen types were extracted by acid guanidinium thiocyanate-phenol-chlorform single step method.

应用异硫氰酸胍一酚一氯仿一步法分离伊氏锥虫安徽株克隆虫体ShTatl的二个抗原变异体ShTat1.3和ShTat1.5总RNA,在含有甲醛的琼脂糖凝胶电泳后,转印到硝酸纤维膜上。

Methods The lymphocytes of rats were isolated from the peripheral blood and cultured with sodium arsenite under 37 ℃.The ROS content was detected by DCFH-DA;The content of LPO was detected by fluoresce method.

体外分离大鼠外周血淋巴细胞后,施加处理因素,在37℃条件下恒温培养,用2'7'-二乙酰二氯荧光素染色法检测细胞内的ROS水平,用硫代巴比妥酸荧光法测定细胞内LPO含量。

Platinum nanoparticles with average diameter of 1.3 nm were prepared by reduction of its salt with sodium citrate.

以柠檬酸钠直接还原氯铂酸制备出了平均粒径为1.3nm的纳米铂微粒。

Results Twain-80 can increase the solubility. The dimethylsulfoxide, the sorbic acid and acetic acid chlorine can strengthen its bacteriostasis effect. To choice suitable antiseptic temperature and control antiseptic time may enhance furacilin liquid preparation stability. On the contrary, it may reduce the stability when mixing the antioxidants agents such as the sodium hyposulfite and the sodium bisulfite.

结果 吐温-80可增溶;二甲基亚砜、山梨酸和醋酸氯己定可增强其抑菌效果;选择适宜灭菌温度、控制灭菌时间可提高呋喃西林液体制剂的稳定性;加入硫代硫酸钠和亚硫酸氢钠做抗氧化剂则使其稳定性降低。

The use of pre-processing of silicon and chlorine reaction of acid solution obtained with different surface structure of gold nanoparticles.

利用预处理的硅片与氯金酸溶液反应的方法获得了具有不同表面形貌的金纳米结构。

Aim: To establish a new method for determination the content of diclofenac acid-choline by atomic absorption spectrometry.

目的:建立了原子吸收法测定双氯芬酸胆碱含量的分析方法。

AIM: To evaluate the efficacy and safety of diclofenac sodium/lidocaine injection in treatment of ankylosing spondylitis.

目的:评价国产双氯芬酸钠利多卡因注射液治疗强直性脊柱炎的有效性和安全性。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。