氯酸

A method based on capillary electrophoresis with electrochemical detection has been developed for the separation and determination of epicatechin, kaempferol, chlorogenic acid, 4-hydroxybenzoic acid, quercetin and protocatechuic acid in hawthorn for the first time.

首次采用毛细管电泳—电化学检测法同时测定山楂中的6种活性成分：表儿茶素，山奈酚，氯原酸，4-羟基苯甲酸，槲皮素和原儿茶酸的含量。

Flame—retardant resin was prepared by the condensation and polymerization of phosphoric acid, trihydroxy methyl propane and epoxy chloropropane,the resin was then reacted with hexane diacid and diglycol under certain condition ,resulting in polyol containing 1.5% P and 17— 18% polyester polyol, which was foamed with polyisocyanate, water and catalyst by one— step method, producing fire...

通过磷酸、三羟甲基丙烷和环氧氯丙烷的缩合和聚合反应制得阻燃树脂，然后将它与己二酸、一缩二乙二醇在一定条件下反应制得含P1.5%和含Cl17～18%的聚酯多元醇，再将它与多异氰酸酯、水、催化剂等组分采用一步法发泡工艺制得阻燃聚氨酯软泡塑料。

Flame— retardant resin was prepared by the condensation and polymerization of phosphoric acid, trihydroxy methyl propane and epoxy chloropropane,the resin was then reacted with hexane diacid and diglycol under certain condition ,resulting in polyol containing 1.5% P and 17— 18% polyester polyol, which was foamed with polyisocyanate, water and catalyst by one— step method, producing fire—resistant PU soft foam.

通过磷酸、三羟甲基丙烷和环氧氯丙烷的缩合和聚合反应制得阻燃树脂，然后将它与己二酸、一缩二乙二醇在一定条件下反应制得含P1.5%和含Cl17～18%的聚酯多元醇，再将它与多异氰酸酯、水、催化剂等组分采用一步法发泡工艺制得阻燃聚氨酯软泡塑料。

Based on the experimental evidence, Usnic acid soluble in chloroform and acetone, and Usnic acid with KOH react show yellow in Lichens＇s color reaction; Usnic acid add the mixture of KOH and NaCl react show dark-yellow.

据实验证明，松萝酸易溶于氯仿及丙酮，且在地衣显色反应中，松萝酸与KOH反应显黄色；与KOH和NaCl混合液反应显深黄色。

The preparing method comprises the following steps: adjusting material; washing material; washing; beating; fluffing; blending; removing impurities; washing; preparing acid; preparing chlorine; bleaching; proceeding acid disposal; removing impurities; washing; filtering.

复合纤维素新型浆粕由木材、竹材组合所制成。制造步骤是：调料、洗料、洗涤、打浆疏解、混合、除杂洗涤、预酸、预氯、漂白、酸处理、除杂洗涤、抄造。

The preparing method comprises the following steps: adjusting material; washing material; washing; beating; fluffing; blending; removing impurities; washing; preparing acid; preparing chlorine; bleaching; proceeding acid disposal; removing impurities; washing; filtering.

复合纤维素新型浆粕由棉绒、木材、麻、竹材之任意两种或者两种以上的原材料的任意组合所制成。制造步骤是：调料、洗料、洗涤、打浆疏解、混合、除杂洗涤、预酸、预氯、漂白、酸处理、除杂洗涤、抄造。

Lithium perfluoroalkylphosphonate was synthesized by LiF and perfluoroalkylphosphonate acid obtained by electrochemically fluorinating chlorodiisopropylphosphine. Some properties of a kind of electrolyte that was made from dissolving the lithium perfluoroalkylphosphonate in the mixed solvent with ethylene carbonate and dimethyl carbonate mass ratio 1∶1 were investigated, such as conductivity, stability toward hydrolysis and oxidative decomposition potential, and so on.

选取氯代二异丙基膦(C6H14PCl)为原料，利用电化学氟化方法，得到全氟烷基膦酸[(C3F7)2PF3]，(C3F7)2PF3与氟化锂反应得到全氟烷基膦酸锂Li[(C3F72PF4]，将其溶于碳酸乙烯酯和碳酸二甲酯质量比为1∶1的混合溶剂中得到电解液，考察电解液的电导率、抗水性及氧化分解电位。

The present invention adopts ammonium salt solution as leach, and adopts the liquid-phase oxidation activating agent formed from surfactant sodium ligno-sulfonate or sodium dodecyl sulfonate, liquir phase oxidation catalyst Cu(2+) and sulfur-extracting agent tetrachloroethylene to implement quick leaching process of sulkfide mineral in gas-liquid-solid three-phase reactor, all the sulfurs contained sulfide in mineral powder can be converted into elementary sulfur and sulfuric acid radical, the contained zinc, copper, nickel, cobalt, lead, cadmium and silver can be changed into soluble salt, and fed into leach or remained in the leaching out slag.

本发明涉及的有色金属硫化矿的铵盐液相氧化直接浸出方法，其特征在于：采用铵盐溶液作浸出剂，采用由表面活化剂木质磺酸钠或十二烷基磺酸钠，液相氧化催化剂Cu2+、萃硫剂四氯乙烯组成的液相氧化活化剂，在气液固三相反应器内，实现硫化矿的快速浸出过程，矿粉中各种硫化物所含的硫转变为单质硫和硫酸根，所含的锌、铜、镍、钴、铅、镉、银等变成可溶性盐类进入浸出液中或留在浸出渣中，消除传统流程中二氧化硫，硫化氢，氮氧化物及含砷含汞含铅等有毒烟气的排放。

Besides, n-butyl and sec-butyl tosylate that are difficult for oxidative addition can react with phenylmagnesium bromide to form corresponding cross-coupling products. Primary alkyl halide which contains β-hydrogen and is relatively hard to undergo the reaction , n-butyl chloride for instance, can react with aryl Grignard reagents in the presence of NiB alloy as well.

此外，难以进行氧化加成的对甲苯磺酸正丁酯和对甲苯磺酸仲丁酯可以与苯基溴化镁作用生成相应的交叉偶联产物；反应相对困难的含β-H的伯卤烷，如：正氯丁烷也可以在NiB催化下与芳基格氏试剂发生偶联。

Benzoyl chloride was treated with potassium selenocyanate in dichioromethane by using polyethylene glycal-400 as the solid-liquid phase transfer catalyst to yield the corresponding benzoyl isoselenocyanate. This intermediate did not need to be isolated and directly reacted with arylamines, affording the N-benzoyl-N'-arylselenoureas 2a~2p. These compounds were characterized by IR, 1H NMR spectra and elemental analysis and the single crystal structure of 2k has been confirmed by X-ray crystallographic analysis.

以PEG-400为固液相转移催化剂，通过苯甲酰氯与硒氰酸钾反应合成了中间体苯甲酰基异硒氰酸酯，该中间体不需分离，直接与芳胺反应，得到N-苯甲酰基－N'-芳基硒脲(2a~2p)，这些化合物用1H NMR，IR及元素分析进行了表徵，并用X射线单晶衍射确定了化合物2k的单晶结构。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。