氯酸

With the yield of methyl monochloroacetate as evaluating standard,the synthesized condition of methyl chloroacetate was optimized through orthogonal experiment.

以氯乙酸母液和甲醇为基本原料，固载磷钨酸为催化剂，通过连续酯化的方法制备了氯乙酸甲酯；以氯乙酸甲酯的质量收率为基准，采用三因素三水平正交实验的方法对酯合成的条件进行了优化。

The hydrosilylation was also improved a lot by the catalyst composed of chloroplatinic acid and triethylamine.

在合成γ-氯丙基甲基二氯硅烷的工艺中，选用助催化效果最好的三乙胺作助催化剂与氯铂酸络合形成催化体系，并通过正交试验法优选出该反应的最佳工艺条件，其反应时间大大缩短，产率高达85%，远远高于以往文献报道的产率。

The optimum reaction conditions were: at present of acetic anhydride, a stoichiometric quantity of nitric acid, at room temperature for 40 minutes. Nitration of chlorobenzene gave a,50% yield of mononitro compounds, and an ortho-para isomer ratio 0.20 in product distribution of chlorobenzene mononitration.

结果表明：硅钨酸催化性能较好，催化剂载体以纳米二氧化硅最好，反应条件中醋酸酐用量是主要影响因素；SiW_(12)O_(40)~(4-)／纳米SiO_2催化剂具有强对位选择性：在醋酸酐存在下，氯苯与等当量的硝酸室温下反应40分钟，氯苯一硝化产物中邻／对硝基氯苯异构体的质量比达0.2，产率可达50％。

Chloride by the acid and inorganic acid chloride, such as phosphorus trichloride, phosphorus pentachloride, thionyl acyl chloride (SOCl2) the role of the system was.

酰氯可由羧酸与无机酸的酰氯，如三氯化磷，五氯化磷，亚硫酰氯（SOCl2）作用制得。

Cycloserine was produced using L-serine methyl ester hydrochloride as raw material. L-serine methyl ester hydrochloride was chloridized with phosphorus pentachloride to afford 2-amino-3-chloride propanic acid methyl ester hydrochloride, which was cyclized with hydroxylamine in the presence of alkali to give cycloserine.

以L-丝氨酸甲酯盐酸盐为原料制备了环丝氨酸。L-丝氨酸甲酯盐酸盐和五氯化磷在氯仿溶剂中进行氯代反应生成2-氨基-3-氯丙氨酸甲酯盐酸盐，后者和羟胺在碱性溶液中发生环合反应得到环丝氨酸。

The famciclovir was synthesized from purine by a series of steps by Acylation, Decarboxylation, Reduction ,and so on; Derivatives of these intermediates is described from the 6-chloro- 9H- purin-2-amine as raw materials in different conditions when the iodine and bromide were synthesized with the addition of two intermediate 6-bromo-9H-purin-2-amine and 6-iodo-9H-purin-2-amine; There is elaborated from the main part of a acetophenone, urineaminohydrochloride, phenylhydrazine, ethyl acetoacetate as raw material through a series of reactions to synthetic 3-phenyl-4-formylphenyl pyrazole and 5-chloro-3-methyl-1-phenyl-1H-pyrazole-4-aldehyde two pyrazole aldehyde, and then with 2-amino-6-chlorine-9-(2-methicillin-oxo-co-methyl-4-yl) purine reaction of the two new pyrazole purine Schiff bases.

本论文主是采用以鸟嘌呤为原料，经过一系列的酰基化，脱羧，还原等反应作用下最终得到了产物2-氨基-9-(4-乙酰氧基-3-乙酰氧基甲基丁基)嘌呤；其中的中间体衍生物主要是阐述从以2-氨基-6-氯鸟嘌呤为原料通过在不同的条件下进行溴代与碘代分别合成了另外两种中间体2-氨基-6-溴鸟嘌呤及2-氨基-6-碘鸟嘌呤；还有一部分主要是阐述从以苯乙酮，盐酸氨基脲，苯肼，乙酰乙酸乙酯为原料通过一系列的反应先合成3-苯基-4-醛基吡唑及5-氯-3-甲基-1-苯基-1H-吡唑-4-甲醛这两个吡唑醛，然后再与2-氨基-6-氯-9-(2-甲氧羰基丁酸甲酯-4-基)嘌呤反应得到了两个新型的吡唑嘌呤席夫碱

We studied some new colour reactions for the first time. Amino-Gacid chlorophosphonazo, sulphonic acid amide chlorophosphonazo and phippuric acid chlorophosphonazo were used to establish flow injection spectrophotometric methods of Pd in ores.

我们首次探索了一些前人未研究过的新显色体系，使用氨基G酸偶氮氯膦，磺胺偶氮氯膦，对马尿酸偶氮氯膦建立了测定矿石中Pd的流动注射分光光度法。

The optimal reaction conditions were as follows:chloroform was used as the reaction solvent,3,5-propionyl acid 0.02 mol,sulphoxide diloride 0.054 mol,the reaction temperature 50℃ and the reaction time 5 h. Under these conditions,the yield of product was 98.9%.

对酰氯合成条件进行了研究，得出优惠反应条件为：以氯仿作溶剂、β-（3，5-二叔丁基-4-羟基苯基）丙酸0.02 mol、二氯亚砜0.054 mol、反应温度50℃、反应时间5 h，优惠条件下产品的收率为98.9％。

It deliberated that magnesium sulphate and epichlorohydrin affecting on synthetization of starch xanthate, mass ratio of synthetic starch xanthate and Magnesium sulphate was...

研究了MgSO_4和环氧氯丙烷对DX合成的影响，得出淀粉和MgSO_4的重量比为8：1，淀粉和环氧氯丙烷的重量比为10：1，MgSO_4和环氧氯丙烷对黄原酸化程度没有影响，但能增强交联程度和不溶性。

It deliberated that magnesium sulphate and epichlorohydrin affecting on synthetization of starch xanthate, mass ratio of synthetic starch xanthate and Magnesium sulphate was 8: 1, Mass ratio of synthetic starch xanthate and epichlorohydrin was 10 : 1, Magnesium sulphate and epichlorohydrin didn't affect sulphonating extent of synthetic starch xanthate, but did enhance cross extent and nature of insoluble.

研究了MgSO_4和环氧氯丙烷对DX合成的影响，得出淀粉和MgSO_4的重量比为8：1，淀粉和环氧氯丙烷的重量比为10：1，MgSO_4和环氧氯丙烷对黄原酸化程度没有影响，但能增强交联程度和不溶性。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。