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氯苯乙酮

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Results: Using of handy infrared gas spectrometer, the ammonia, sulphur dioxide, acetone, butanone, ethyl acetate, chloroform, benzene, toluene, methyl alcohol, ethyl alcohol, isopropanol, and other harmful gases can be carried out quickly Online Testing. The arsine, hydrogen chloride, hydrogen cyanide, hydrogen sulfide can not be detected online.

结果:可利用便携式红外气体分析仪对氨、二氧化硫、丙酮、丁酮、乙酸乙酯、氯仿、苯、甲苯、甲醇、乙醇、异丙醇等有害气体可进行快速的在线检测,不能对砷化氢、氯化氢、氰化氢、硫化氢进行快速在线检测。

The reducing-coupling reaction of benzoyl chloride under Dy/n-BuBr was complex. Besides diphenyl diketone, benzoin and ring-opening product of THF were also obtained.

苯甲酰氯在Dy/n-BuBr作用下的还原偶联反应较为复杂,除得到二苯基乙二酮外,还得到四氢呋喃开环产物以及安息香。

Aniline compounds are used as raw material and reacted with anthranilic acid and then phenyl iodide as alkylating agents to give alkylating products followed by cyclizing with concentrated sulphuric acid to give a N-phenyl-acridone(or 3-ethoxyl-N-phenylacridone).The structure of intermediate and target compound are determined by IR and MS.

以苯胺类化合物为原料,先后以邻氯苯甲酸和碘苯为烷基化试剂进行了N 烷基化反应,再用浓硫酸使其环化制得N-苯基吖啶酮和3-乙氧基-N-苯基吖啶酮,并用红外光谱及质谱仪检测了各中间体及目标产物的结构。

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