氯甲烷

The idea of investigating plants as methane emitters grew out of research we had been conducting on chloromethane, a chlorinated gas that destroys ozone and was thought to come mainly from the oceans and forest fires.

把植物视为甲烷排放源的研究念头，萌生自我们对氯甲烷所进行的研究。

Objective: To establish a method for determination of dichloromethane, 1,1-dichloroethylene and 1,2-dichloroethylene in drinking water with headspace gas chromatography.

目的：探讨生活饮用水中二氯甲烷、1，1二氯乙烯和1，2二氯乙烯的顶空气相色谱测定方法。

The results showed as follows: 1 Extraction of gelsemium total alkaloids. Total alkaloids were extracted with 95 per cent ethanol. The extract rate was 0.519 per cent and the extract purity were 88.02 per cent and 87.38 per cent; Total alkaloids were extracted with chloroform .The extract rate was 0.416 per cent and the extract purity were 89.02 per cent and 94.52 per cent. 2 Isolation of gelsemium total alkaloids with TLC. Total alkaloids contained five or more alkaloids. The optimal developing agent was chloroform :methanol :ethyl acetate(9:l:0.3),the optimal eluent was methylene chloride:methanol(92:8). 3 Isolation of total alkaloids with column chromatography. Alkaloid A and alkaloid B were obtained, alkaloid B was identified as koumine.

研究结果如下：1、钩吻总碱的提取：用95％的乙醇提取钩吻生物碱提取率为0.519％，其提取物纯度为88.02％、87.35％；用氯仿提取钩吻生物碱提取率为0.416％，其提取物纯度为89.02％、94.52％。2、钩吻总碱的薄层层析分离：总碱中含有5种或5种已上的生物碱；氯仿：甲醇：乙酸乙酯(9：1：0.3)是最佳薄层层析的展开剂；二氯甲烷：甲醇(92：8)是柱层析的最佳洗脱剂。3、钩吻总碱的柱层析分离：共得到两种钩吻生物碱单体成分碱A和碱B，碱B为钩吻素子，碱A可能是钩吻素甲。4、钩吻总碱的急性毒性试验：钩吻总碱小鼠腹腔注射的半数致死量LD_(50是：7.38mg／kg，95％的可信限范围为：6.67mg／kg～7.94mg／kg。

China mainly natural gas used in the production of nitrogen, followed by the production of methanol, formaldehyde, acetylene, methylene chloride, carbon tetrachloride, carbon disulfide, nitromethane, hydrocyanic acid and extraction of helium and carbon black. Since the 70s, has built more than natural gas and oil field associated gas as raw materials for large-scale ammonia plant, as well as a number of small and medium-sized ammonia plant, so that the national structure of the synthetic ammonia production of raw materials, natural gas share of about 30%; also be built at the same time A system of acetylene gas plant to manufacture Vinylon and vinyl acetate, acetylene gas used in the production of methanol.

中国天然气主要用于生产氮肥，其次是生产甲醇、甲醛、乙炔、二氯甲烷、四氯化碳、二硫化碳、硝基甲烷、氢氰酸和炭黑以及提取氦气。70年代以来，已兴建多座天然气和油田伴生气为原料的大型合成氨厂，以及一批中、小型合成氨厂，使全国合成氨生产原料结构中，天然气所占的比例约达到30％；同时还兴建了天然气制乙炔工厂，以制造维尼纶和醋酸乙烯酯，乙炔尾气用于生产甲醇。

Major procurement of goods: a three-chlorosilanes, dichloromethane, AE activity ester, 3-iodine Silane, special acid, pentyl chloride, triethylamine, thiadiazole, tetrazolylazo acid, 2 - Acetamide, tetrahydrofuran, the four-guanidine, isopropanol, five phosphorus trichloride, sodium vary bitter, acid, sodium phenylacetate, 6-2 silicon n-amine, Ethylacetoacetate , Methyl isobutyl ketone, potassium dihydrogen phosphate, aluminium oxide, DL methionine, N, N-dimethylaniline, NN-diethyl aniline, 4 sodium EDTA, Anhydrous sodium sulfate, ammonium sulfate, potassium sulfate, sodium acetate, sodium carbonate, DMC, formic acid, sodium chloride medicinal, oxalate, protopine, acetone, alcohol, acetic acid, vinegar Ethyl, butyl acetate, methanol, ethanol (anhydrous, industrial, medicinal), formaldehyde, Ye Jian (30%), hydrochloride (industrial-grade, refined grade, reagent level), sulfate (98%), Ammonia, calcium carbonate, chlorine dioxide, 6 - APA ,7-ACA ,7-ADCA ,7-ANCA, sulbactam, ceftazidime activity ester, Deng salt (hydroxymethyl-K, acid precursors Potassium, sodium dihydrogen methyl), resin, the enzyme, water treatment agent, Xiao Mo agent, demulsifier, flocculants, activated carbon, all kinds of medicinal materials, All kinds of additives

三甲基一氯硅烷、二氯甲烷、AE活性酯、三甲基碘硅烷、特戊酸、特戊酰氯、三乙胺、噻二唑、四氮唑乙酸、二甲基乙酰胺、四氢呋喃、四甲基胍、异丙醇、五氯化磷、异辛酸钠、苯乙酸、苯乙酸钠、六甲基二硅胺烷、乙酰乙酸乙酯、甲基异丁酮、磷酸二氢钾、三氧化二铝、DL蛋氨酸、N，N-二甲基苯胺、NN-二乙基苯胺、乙二胺四乙酸四钠、无水硫酸钠、硫酸铵、硫酸钾、醋酸钠、碳酸钠、碳酸二甲酯、甲酸、药用氯化钠、草酸、片碱、丙酮、正丁醇、冰醋酸、醋酸乙酯、醋酸丁酯、甲醇、乙醇、甲醛、液碱（30％）、盐酸（工业级、精制级、试剂级）、硫酸（98％）、氨水、碳酸钙、二氧化氯、6－APA、7－ACA、7－ADCA 、7－ANCA、舒巴坦、头孢他啶活性酯、邓盐(羟甲基钾、前体酸钾、二氢甲基钠)、树脂、生物酶、水处理剂、消沫剂、破乳剂、絮凝剂、活性碳、各种药用辅料、各种添加剂

Moreover, evaluating the effects of different factors such as laying up unaffectedly, temperature.

此外，又评价了自然放置不同时间和不同温度对自来水中氯仿、三氯乙烯、二溴一氯甲烷等存在的影响。

The eight VOCs were acetophenone, phenol, benzotrichloride, 1, 3-butadiene, chlorobenzene, methanol, methyl chloroform and methylene chloride. They were mixed together with very low concentrations.

所测定的八种VOCs为苯乙酮，苯酚，三氯甲苯，1，3丁二烯，氯苯，甲醇，三氯代乙烷和二氯甲烷。

A Product main business categories: chemical solvents white oil, toluene, xylene, durene, valitin water, acetate, D resin, acetone, butanone, cyclohexanone , anti-white water, dichloromethane, trichloroethane, trichlorethylene, loose water-saving washing network water, open water, wash water, and days that water, rust agent, to water-logging, washing machine water, decontamination water, n-butyl alcohol, isopropyl alcohol, ethanol, industrial alcohol, car-washing water, washing machine water, clean lines of water, cleaning machine water, fire water, paint remover, fungicides, antifreeze water, chloroform, grinding fluid , diluent, release agent, dehydration agent substantial industrial solvents.

主要经营产品 A类：化工溶剂白电油、甲苯、二甲苯、四甲苯、凡立水、乙脂、丁脂、丙酮、丁酮、环己酮、防白水、二氯甲烷、三氯乙烷、三氯乙烯、松节水、洗网水、开油水、洗面水、天那水、除锈剂、去渍水、洗枪水、去污水、正丁醇、异丙醇、乙醇、工业酒精、洗车水、洗机水、抹线水、抹机水、火水、脱漆剂、杀菌剂、防冻水、哥罗仿、研磨液、稀释剂、脱模剂、脱水剂等大量工业溶剂。

Under catalysis of AlCl3, trans-1-chloro-3-phenyl-1-propen-3-one was first prepared using benzoyl chloride and acetylene in CH2Cl2 at 20~25℃, which the yield is 7% higher than that in CCl4 at 40~45℃.

通过对其反应条件的研究，首次用苯甲酰氯和乙炔在三氯化铝作用下合成出反－3-苯基－1-氯－1-丙烯－3-酮；并发现用二氯甲烷作介质在20~25℃下的反应产率，比用四氯化碳作介质在40~45℃下的反应产率约高7%。

Chloroacetic acid,chloromethyl ether,acetone,mphenylenediamine,butyl acetate,ethyl acetate,methylene chloride,ethylene dichloride,dioxane.

氯乙酸，氯甲醚，丙酮，间苯二胺，醋酸丁酯，醋酸乙酯，二氯甲烷，二氯乙烷，二氧六环。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。