氯化硫

By using conditional experiment,an optimum processing for preparation of sulfur dichloride was reached.

以工业硫磺和液氯为主要原料，一步法直接制备二氯化硫。

In the presence of the combination of sulphuric and phosphoric acid, with sodium diphenylamine sulfonate as the indicator, standard solution of potassium dichromate was used to titrate total iron value.

试样以盐酸溶解后，在酸性介质中，先以氯化亚锡将三价铁大部分还原为二价，然后在钨酸钠指示下，再以三氯化钛将剩余的三价铁还原为二价，过量的三氯化钛以重铬酸钾氧化消除干扰，在硫磷混合酸存在下，以二苯胺磺酸钠为指示剂，用重铬酸钾标准溶液滴定全铁量。

It is a rubber-like product made by reacting rape-seed oil from the Dutch East Indies with sulfur chloride.

看起来像橡胶一样的东西，是由荷兰东印度群岛出产的菜籽油跟氯化硫进行化学反应制造出来的。

The physics-chemistry properties,synthesis of sul phur monochloride and its application in organic reactions are introduced briefl y.

简要介绍了一氯化硫的理化性质、合成方法及其在有机反应中的应用。

Diallyl trisulfide was synthesized with a yield of 76.4% based on sodium thiosulfate, allyl bromide and sodium sulfide. And diallyl tetrasulfide was synthesized by the reaction of sulfur monochloride with ally1 mercaptan with a yield of 81.0%.

以硫代硫酸钠、烯丙基澳和硫化钠为原料，合成了二烯丙基三硫，产率为76.4%；以一氯化硫和烯丙硫醇为原料合成了二烯丙基四硫，产率为81.0%。

A process for preparing the olefine sulfide includes addition reaction between sulfur monochloride and C3-C12 olefine under existance of low-carbon alcohol as catalyst to obtain addition compound, mixing it with C1-C15 haloalkane, sulfide of alkali metal, sulfur powder, and aqueous solution of emtrol, sulfurizing, dechlorinating, and refining.

一种硫化烯烃的制备方法，包括：(1)使一氯化硫和C 3 ～C 12 烯烃在低碳醇催化剂的存在下进行加合反应，生成加合物；(2)将(1)步的加合物与C 1 ～C 15 卤代烷、碱金属硫化物、硫磺粉、脂肪醇水溶液混合，进行硫化脱氯反应后，精制处理，得到硫化烯烃产品。

1A series ofω-alkylmercapo acid were synthesized by two methods:one involved the reaction of the appropriateω-bromoalkyl acid with mercaptide under the presence of base;the other method was used only for the long alkyl compound by the reaction ofω-alkenyl acid and alkanethiol in the presence of AIBN.

正是基于以上考虑，本论文探索了合成下沿带有硫醚官能团，而上沿带有偶氮官能团的杯[4]芳烃衍生物的方法，进行了以下研究： 1采用ω-溴代羧酸和烃基硫醇在碱性条件下发生反应，或由ω-烯基羧酸和硫醇在AIBN的存在下反应，得到了ω-硫醚羧酸，使用氯化亚砜将羧酸转化为酰氯。

Through Friedel-Crafts reaction, We have prepared highly purified triphenylphosphine sulfide by using benzene, phosphorus trichloride, sulfur, and aluminum trichloride, which is desulfurized with metal powder to produce triphenylphosphine.

实验方法为以苯、三氯化磷、硫和三氯化铝为原料，利用Friedel-Crafts反应，合成三苯基硫膦，收率为79.4％；然后用金属将三苯基硫膦还原制得三苯基膦，收率为80％。

Wedgeplug O-Seal plug valves with their positive, no-leak features are not only recommended as the best general purpose valves for handling hydrocarbons, vegetable oils, solvents, etc., but are ideal for such tough service as butane, propane, butadiene, acetone, ethyl alcohol, ammonia, anhydrous ammonia, benzene, vinyl chloride, dry chlorine, Dowtherm, ethane, ethylene, hydrogen chloride, napthalene, oxygen, hydrogen, phthalic anhydride, dry phosgene, phosphoric acid, potassium carbonate, styrene, molten sulphur, sulphur dichloride and related services within a temperature range from -300oF to + 450oF within pressure limits of the valves.

楔塞O形密封旋塞阀具有积极的、无泄漏特性，不但是最好的通用的阀门，用于处理碳化氢，植物油，溶剂等，还特别适用于严酷的应用环境，如丁烷，丙烷，丁二烯，丙酮，乙醇，氨，无水氨，苯，氯乙烯，干氯，道氏热载体，乙烷，乙烯，氯化氢，萘，氧，氢，邻苯二甲酸酐，干碳酰氯，磷酸，碳酸钾，苯乙烯，融化硫，二氯化硫，以及温度在-184oC至232oC之间，压力在阀门额定压力等级范围内的有关应用。

They are hydrogen peroxide, ammonium persulfate, sodium persulfate, chlorinated polypropylene, chloridized EVA, garox mek, carbon dioxide, hydrogen, sodium carboxymethyl cellulose, carboxymethyl amylum sodium, feed additive, auric salt and silver salt series, tin salt series, tin dichloride, silver nitrate, fireworks raw materials, spheroid form nickel hydroxide, refined sulfuric acid, battery sulfuric acid, ultramicro fine powder, compound fertilizer, 40% multiple sulfur suspending agent, 40% sulfur-tricyclazole suspending agent, 40% sulfur-multiple-trideflocculant, 20% pemiro-dichlor suspending agent, high panniculus adiposus and so on.

主要产品有：过氧化氢、过硫酸铵、过硫酸钠、氯化聚丙烯、氯化EVA 、过氧化甲乙酮、二氧化碳、氢气、羧甲基纤维素钠、羧甲基淀粉钠、饲料添加剂、金、银盐系列、锡盐系列、氯化亚锡、硝酸银、烟花原料、球形氢氧化镍、精制硫酸、电池硫酸、超微细粉体、复合肥、40%多硫悬浮剂、40%硫·三环唑悬浮剂、40%硫·多·三悬浮剂、20%吡嘧·二氯悬浮剂、高脂膜等10个系列百多个品种、规格产品。

It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发，分析对称连杆曲线上鲍尔点的产生条件，提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品，年生产总值3000万美元，产品价廉物美、选料上乘、质量保证，深受国内外客户的青睐