氯化器

First, the preparation of l,2-dichloro-4-nitrobenzene, which l-chloro-4-nitrobenzene reacted with chlorine in a self-designed chlorinator, in presence of Lewis acid catalyst,.was investigated. By means of the Orthogonal Experiments design and single factor experiments, the influence of several reaction variables on the yield were examined and the optimum reaction conditions under the intervallic operation were obtained, the yield of l,2-diehloro-4-nitrobenzene was 83.26%.

为此，本文首先在自行设计的塔式氯化器中，以对硝基氯苯为原料，路易氏酸作催化剂，分子氯氯化合成3，4-二氯硝基苯(合成3-氯-4-氟-硝基苯的原料)，根据该氯化过程特征，利用正交试验设计方法结合单因素实验考察了有关因素对氯化过程的影响，优化得到了最佳的氯化工艺条件，3，4—二氯硝基苯的收率可达83.26％。

The chlorinating tube ,bower plater ,tower sections cond ensers .tower contain condenser and tower contain ,etc.

氯化塔由塔顶冷凝器、塔节、氯分配器、溢流管、塔板、塔节冷凝器，塔釜冷凝器、塔釜等组成。

By using the a device being similar to water segregator and by controlling the temperature, cyclization of the intermediate product in chloroform reduced carbonization and gave 2-dodecaneanthraquinane in 68.1% yielding.

以十二烷基苯和苯酐为起始原料，经酰基化、关环和磺化三步反应合成了3-十二烷基蒽醌磺酸；并进一步改进和优化了合成工艺条件：即在催化剂三氯化铝过量50%并有三乙胺存在的条件下，中间体2-（4-十二烷基苯甲酰基）苯甲酸收率为72.45%；关环反应采用氯仿作溶剂，利用类似分水器的装置有效控制反应温度以减少碳化，2-十二烷基蒽醌的收率为68.1%。

This paper has studied preparation of Grignard reagents under phonochemistry and optimum technologic conditions is: the power of ultrasonic is 500W and frequency is 250KHZ, having twelve energy conversion devices, water bath temperature being 20C, solvent being THF,unstirred.

本文探讨了超声波合成格利雅试剂的机理，研究了声化学法制备格利雅试剂氯化苄基镁的最佳工艺条件为：在超声波的功率为500W，频率为25KHZ，有12个换能器的条件下，水浴温度为20℃，以THF为溶剂，不搅拌。

The influence of the inlet solution concentration, solution flow rate, inlet air flow rate and temperature, air humidity on the absorbed process were studied for different liquid desiccants (calcium chloride, lithium chloride and calcium chloride mixture), and the dehumidifying effects of various mixture ratios on lithium chloride and calcium chloride mixture were also analyzed. The results show that the CELD (Cost-Effective Liquid Desiccant, the mixture ratio is 1:1) is more economical than pure lithium chloride solution, while its dehumidifying performance is better than calcium chloride solution.

针对不同的实验工质：氯化钙溶液、不同混合比的氯化钙和氯化锂混合溶液，研究了除湿器入口溶液浓度、入口空气流量、溶液流量及空气入口温度、湿度变化对除湿器除湿量的影响；以及氯化钙和氯化锂的混合质量比分别为1：1.5、1：1、1.5：1时的除湿效果；实验结果表明：用氯化钙和氯化锂混合质量比为1：1时的除湿溶液代替氯化锂溶液能节省费用，同时也改善了用纯氯化钙浓溶液作除湿剂时的除湿性能。

The main products: large acid-base tank, stainless steel fermentation tank, concentrated liquor cans, seeds, cans, nitrogen tank, condensate, water, automatic air pressure to water tanks, Jinqi cans, vacuum furnace, distillation columns, vacuum tower, the reactor , Condenser, deaerator, air filters, buffers, water collection and bellows heat exchanger, U-tube heat exchanger, such as titanium tetrachloride heater.

主要产品：大型酸碱贮罐、不锈钢发酵罐、母液浓缩罐、种子罐、氮气贮罐、凝水罐、自动气压给水罐、浸漆罐、真空炉、精馏塔、减压塔、反应器、冷凝器、除氧器、空气过滤器、缓冲器、集水器及波纹管换热器、U型管换热器、四氯化钛加热器等。

PTFE referred to F4, because of its excellent dielectric properties and corrosion-resistant chemical (high temperature of the molten fluoride elements and the state of alkali metal), non-absorbent, non-stick, not conductive, low coefficient of friction and not Ageing properties, and is widely used in chemical, petroleum, textile pharmaceutical, metallurgy, machinery, electronics, electrical appliances, electricity, food and aviation, military and scientific research in all walks of life, I plant the development of metal bellows, compensation , PTFE bellows F4 tetrafluoroethane compensator, F4 metal composite compensation, anti-corrosion steel liner tetrafluoroethane pipe, steel-lined tetrafluoroethane three links, elbow, Stone, the reaction tower, tower chloride, lining tetrafluoroethane valve Doors, tetrafluoroethane pads and steel-lined polypropylene pipes and accessories, and earnestly solve the user in the production process by the various anti-corrosion problems.

聚四氟乙烯简称F4，由于其优异的介电性能与耐化学腐蚀性(高温下的氟元素和熔融状态下的碱金属外)，不吸水、不粘、不导电、摩擦系数低及不老化等性能，而被广泛应用于化工、石油、轻纺制药、冶金、机械、电子、电器、电力、食品及航空、军用与科研等各行各业中，我厂开发的金属波纹管、补偿器，四氟波纹管F4四氟补偿器、F4金属复合补偿器，钢衬四氟防腐管件，钢衬四氟三通、弯头、四通、反应塔、氯化塔、衬四氟阀门，四氟垫片以及钢衬聚丙稀管道及配件，切实解决了用户在生产过程中所遇到的各种防腐问题。

After dryness, silica powder is put into chlorinated furnace in fluid bed and reacts with dried hydrogen chloride gas in the environment of 340℃ to form crude trichlorosilane. The crude trichlorosilane , through hydroscrubber and pipe bundle condenser to extract silicon tetrachloride in distillation column produces trichlorosilane gas out of the d istillation column , which can be made into the finished product of trichlorosilane by condensation .

硅粉经干燥后加入氯化沸腾炉，与通入炉中的干燥氯化氢气体在340o C进行反应，生成的粗三氯氢硅经湿法除尘器、列管冷凝器去蒸馏塔分离匹氯化硅，由蒸馏塔出来的三氯氢硅气体经冷凝，制得三氯氢硅成品。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。