氯乙醇

The chloroform layer and the aqueous layer were separated by multiple column chromatography including macroporous resin, silica gel and polyamide column and preparative HPLC. The compounds obtained were identified by mass spectra and NMR data.

大青叶乙醇提取物，用氯仿萃取后得到氯仿层和水层，各层再分别采用硅胶柱、大孔树脂柱、聚酰胺柱、制备液相、葡聚糖凝胶柱层析及重结晶等分离手段进行分离、纯化，并应用化学性质和质谱、波谱法（1H-NMR、13C-NMR、HMBC）鉴定其化学结构。

Properties White powder, inodorous, non-toxic, soluble in dilute alkali solution, carbon disulfide, benzene, acetone, dichloromethane and a little soluble in chloroform, insoluble in alcohol, carbon tetrachloride and ethyl acetate.

性质 白色粉末。无毒、无味。溶于稀碱、二硫化碳、苯、丙酮和二氯甲烷，微溶于氯仿，难溶于乙醇、四氯化碳、醋酸乙酯。

Properties: colorless needle-like crystals, melting point 105 ~ 106 ℃, optical rotation +51 °(c = 0.978, chloroform), other reports shows that by ethanol recrystallization the melting point 104 ~ 105 ℃, methanol re - the formation of solvate crystal melting point 84 ℃.it is Soluble in acetone, chloroform, insoluble in ether, petroleum ether, insoluble in water.

性质：无色针状结晶，熔点105～106℃，旋光度+51°（ c=0.978，氯仿），还有报道经乙醇重结晶熔点104～105℃，经甲醇重结晶形成的溶剂化物熔点84℃。易溶于丙酮、氯仿，难溶于乙醚、石油醚，不溶于水。

Project Background and Conditions: The company started research new chemical products in 1998. After two years of efforts, a series of pharmaceutical intermediate sulfathiazole leave instructions, including : 3- methyl sulfathiazole leave instructions, 2- sulfathiazole leave instructions ethanoic acid, 2- acetyl sulfathiazole leave instructions, 2-thiofuran amino ethane ,2-thiofuran acetic, 3,4,5- tighter nitrobenzene have been successfully developed. 2-thiofuran amino ethane are the precursors raw materials of series antibiotic analgesic.

二、项目建设背景及条件：1998年公司开始研究开发高新精细化工产品，经过两年的努力，已成功研制出噻吩系列医药中间体，包括：3-甲基噻吩、2-噻吩乙酸、2-乙酰噻吩、2-噻吩乙胺、2-噻吩乙醇、3，4，5-三氯硝基苯等。2-噻吩乙胺系列噻吩产品使用于血小板及血栓有关的心脏血管病及消炎镇痛等如氯吡格雷、兴孢噻吩钠、兴孢西丁、噻吩洛酸等十几种新药的前体原料，是国家政策鼓励发展和有自主知识产权的项目。

Pt-inserted nanotube titanic acid was prepared as follows: H_2PtCl_6 ethanol solution was filled into the titanic acid nanotubes and then annealed in air at 673 K for 3 h.X-ray photoelectron spectroscopy showed that H_2PtCl_6 has been converted to Pt~0 and PtO.The result of electron spin resonance revealed that there are single-electron-trapped oxygen vacancies to be formed in PNTA after heat treatment in air.

通过在真空条件下将氯铂酸的乙醇溶液引入到钛酸纳米管内，再经过热处理制备了镶嵌铂的纳米管钛酸。X射线光电子能谱表明氯铂酸大部分转变成Pt0和PtO，顺磁共振谱表明在PNTA中生成了束缚单电子的氧空位，在紫外-可见扩散漫散射谱谱上表现出对可见光有吸收能力。

Chloro-2-hydroxypropyl trimethylammonium chloride was synthesized by using trimethylamine hydrochloride and epichlorohydrin as the raw materials and anhydrous as solvent.

以无水乙醇作溶剂、三甲胺盐酸盐和环氧氯丙烷为原料合成了3-氯-2-羟丙基三甲基氯化铵，探索出最佳合成条件为：n∶n为0.95∶1，反应温度为40~50℃，反应时间为30m in，所得产品质量分数大于98%，收率达90%。

Purified water, euphorbia cerifera wax, glyceryl stearate, ammonium acrylates copolymer, butylene glycol, copernica cerifera wax, stearic acid, sucrose acetate isobutyrate, acrylates copolymer, bentonite, tromethamine, hexylene glycol, silk amino acids, cholesterol, glycine, synthetic wax, ethylhexyl glycerin, alanine, PEG-9 dimethicone, nylon-6, lecithin, silica, simethicone, caprylyl glycol, xanthan gum, propylene glycol, isostearic acid, sodium laureth-12 slfate, ceteareth-20, polyvinyl alcohol, sodium chloride, sodium acetate, disodium EDTA, benzyl alcohol, chlorphenesin, phenoxyethanol, methylparaben, ethylparaben, propylparaben, butylparaben, isobutylparaben, may contain /- mica, iron oxides (CI 77491, CI 77492, CI 77499), titanium dioxide (CI 77891), ferric ferrocyanide (CI 77150), ultramarines (CI 77007), blue 1 lake (CI 42090), bronze powder (CI 77400), aluminum powder (CI 77000), bismuth oxychloride (CI 77163), carmine (CI 75740), chromium hydroxide green (CI 77289), chromium oxide greens (CI 77288), yellow 5 lake CI 19140

水，小烛树蜡，硬脂酸甘油酯，丙烯酸铵共聚物，1，3-丁二醇，巴西棕榈蜡，硬脂酸，异丁酸醋酸蔗糖酯，丙烯酸酯共聚物，蒙脱土，二吡喃乙酸乙酯胺，已烯醇，丝氨酸，胆固醇，甘油，合成蜡，异丁基甘油，丙胺酸，PEG-9二甲基硅油，尼龙-6，卵磷酯，硅粉，硅氧烷，癸酰基乙二醇，汉生胶，丙二醇，异硬脂酸，月桂基醚-12硫酸钠，十六十八醇醚-20，聚乙烯醇，氯化钠，醋酸钠，EDTA二钠，苯氧乙醇，氯代苯酚，卞醇，尼泊金甲酯，尼泊金乙酯，尼泊金丙酯，尼泊金丁酯，尼泊金异丁酯，[可能还含有云母，铁黑(CI 77491， CI 77492， CI 77499)，钛白粉(CI 77891)，氰化亚铁(CI 77150)，靛蓝(CI 77007)，蓝1号(CI 42090)，青铜粉(CI 77400)，铝粉(CI 77000)，氯氧化铋(CI 77163)，洋红色素(CI 75740)，氢氧化铬绿(CI 77289)，氧化铬绿(CI 77288)，黄5号(CI 19140)]文章来自网络，不代表本网站立场，版权归原作者所有，转载请注明出处！

Our company is mainly engaged in chemical raw materials trading, the company mainly engaged in: toluene, xylene, mesitylene, durene, 6 # 120 # 200 # solvent, ethyl acetate, butyl acetate, acetone, butanone, cyclohexanone, isophorone, MIBK, isopropyl alcohol, isobutyl alcohol, butanol, mixed alcohols, methanol, ethanol, ethylene glycol, diethylene glycol, diacetone alcohol, Anti-White Water, CAC, n-hexane, dichloromethane, trichloro-B, DMF, 5 # 10 # 15 # white mineral oil, lubricating oil, sewing machine oil, as well as high-pressure polyethylene, linear polyethylene, low-pressure polyethylene, polypropylene, rubber and other chemical raw materials.

我公司主要从事化工原料贸易，公司主要经营：甲苯、二甲苯、三甲苯、四甲苯、6# 120# 200#溶剂、醋酸乙酯、醋酸丁酯、丙酮、丁酮、环已酮、异佛尔酮、MIBK、异丙醇、异丁醇、正丁醇、混丙醇、甲醇、乙醇、乙二醇、二甘醇、二丙酮醇、防白水、CAC、正已烷、二氯甲烷、三氯乙、DMF、5# 10# 15#白矿油、润滑油、针车油以及高压聚乙烯、线性聚乙烯、低压聚乙烯、聚丙烯、橡胶等各种化工原料。

A GC headspace injection method for the determination of residual organic solvents such as methanol, ethanol, acetonitrile, dichloromethane, ethylacetate, 4 methyl 2 pentanone, toluene, DMF, chloroform and tetrahydrofuran in tazobactam was established.

建立了气相色谱顶空进样法测定三唑巴坦中甲醇、乙醇、乙腈、二氯甲烷、乙酸乙酯、甲基异丁基酮、甲苯、N ，N′-二甲基甲酰胺、氯仿和四氢呋喃等有机溶剂的残留量。

Diethylthiophosphoryl chloride was synthesized by reacting phosphorus thiochloride with anhydrous alcohol in the presence of NaOH, and then a novel phosphorus-nitrogen- and sulfur-containing flame retardant, 1, 4-di(O,O-diethyl thiophosphoryl imine) benzene, was synthesized via the reaction of diethylthiophosphoryl chloride with p-phenylenediamine.

以三氯硫磷与无水乙醇在NaOH存在下合成了二乙基硫代磷酰氯，然后再与对苯二胺反应合成了新型的含磷、氮、硫的膨胀型阻燃剂：1，4-二（O，O-二乙基硫代磷酰亚胺基）苯。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。