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氯乙醇

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After extraction by ethanol and purification by cationic ion-exchange column, a method of using reversed-phase high-performance liquid chromatography and precolumn derivatization with o-phthalaldehyde and 9-fiuorenylmethylchloroformate is employed for determination of free amino acids in tobacco . This method assures that amino acids with amino and imino groups can be determined simultaneously. The results of duplication experiment and recovery experiment are acceptable.

本试验用乙醇提取烟叶中的游离氨基酸,并用阳离子交换树脂纯化,再用邻苯二甲醛、氯甲酸芴甲酯联合柱前衍生、反相高效液相色谱分析测定了烟叶中的游离氨基酸,该方法能同时测定烟叶中的带氨基和亚氨基基团的氨基酸,并且分析方法的重现性和回收率均令人满意。

Then, the whole herb of Juncus effusus was extracted with 95% ethanol. The ethanolic extract was further separated with petroether, chloroform, ethyl acetate and methanol in turn to give four fractions.

用95%乙醇提取制备了总提取物,然后将总提物用石油醚、氯仿、乙酸乙酯、甲醇依次萃取,分成极性大小不同的部位,通过药理活性筛选后确定了有效部位为乙酸乙酯部分。

The fractions of Ligroine and chloroform part of the the EtOH extraction were isolated and purified by column chromatography on silica gel and Sephadex LH 20 and recrystallization. Their structures were studied by using UV, IR, H-NMR, 13C-NMR, and MS, techniques.

运用硅胶、Sephadex LH-20柱色谱等方法对芫花乙醇提取物的石油醚及氯仿萃取部分进行化学成分研究,并利用UV、IR、1HNMR、13CNMR、MS等光谱技术鉴定其化学结构。

According to explore the extracting process of coumarin from melilotus, include extracting with ethanol, decoloring with petroleum ether and extracting with chloroform was determined.

通过对提取工艺进行探索后,确定了乙醇提取、石油醚脱色、氯仿萃取的工艺路线。

Methods: Transfer the sample about 1ml, equvalent to about 2mg of Monoammonium Glycyrrhizinate, add 1 ml of 20% trichloroacetic acid using ethanol as the solvent, evaporate on a water bath to nearly dry, the residue appeares purple.

取本品1ml(约相当于甘草酸单铵2mg),加入20%三氯乙酸乙醇溶液1ml,置水浴蒸至近干,残留物显红紫色。

In the CMKGM preparation section,with the indicators of DS andη, the optimum laboratory conditions preparation of a certain molecular weight of the high DS of CMKGM: reaction time (5~6) h, the theory of the degree of substitution (2~3), the molar ratio of monochloroacetic acid to Sodium hydroxide (2:1~3:1),the reaction temperature (55~65)℃, liquid ratio (10:1~12:1)mL/g, containing enthanol (50~70)%.

CM(来源:5e60ABC论文网www.abclunwen.com)KGM制备工艺研究中,以取代度、表观粘度为指标,建立了制备一定摩尔质量的高DS的CMKGM的实验室制备条件:反应时间(5~6)h、理论取代度(2~3)、氢氧化钠与氯乙酸摩尔比(2:1~3:1)、反应温度(55~65)℃、液料比(10:1~12:1)mL/g、乙醇体积分数(50~70)%。

The parasiticidal effect of ethanol extracts from a plant Dioscorea zingiberensis on dactylogyrid Dactylogyrus intermedius found in goldfish was studied to search for parasiticidal substances by standard laboratory procedures compared with the other four drugs mebendazole, abamectin, ivermectin and praziquantel.

以寄生在金鱼Carassius auratus鳃部的中型指环虫Dactylogyrus intermedius为指示寄生虫,采用活体感染、活体杀虫的方法,研究了用不同溶剂(石油醚(沸程60~90℃)、氯仿、乙酸乙酯、乙醇和水)分别对盾叶薯蓣Dioscorea zingiberensis进行提取,其5种提取物的杀虫活性。

A method using α methylstyrene as raw material to prepare β methylene phenethyl alcohol,a new rose flavor ,by chlorination,esterification and saponification was studied.

对α 甲基苯乙烯经氯代、酯化、皂化合成新型玫瑰香料β亚甲基苯乙醇的方法进行了研究,选择PTC1作为相转移催化剂,当m∶m (NaAc·3H2 O)∶m (PTC1 )=1 。0 0 0∶0 30 0∶0 0 2 4时,80℃下反应 6h ,产率为 67 3%。

It was firstly found that the Pb-pheophytin complex could be easily formed only with the reaction of Pb〓 with pheophytin in ethanol medium.

首次发现用高氯酸铅与脱镁叶绿素在乙醇溶液中形成铅叶绿素配合物。

The preparation of the membrane is that the phthalazine polyether-sulfone-ketone polymer is mixed with chloroform, Ethanol or butanol according to certain quality proportion; after the magnetic stirring, the evenly mixed casting solution is obtained, filtered and carried out with vacuum deaeration; The casting solution is scraped into membrane of certain thickness on the non-woven fabric by adopting the scraper; the membrane is standed for 24 hours in the air of certain humidity and temperature to obtain the plate ultrafiltration membrane of phthalazine polyether-sulfone-ketone.

本发明公开了属于高分子膜分离技术领域的一种二氮杂萘聚醚砜酮类聚合物平板超滤膜的制备方法,所述膜的制备方法为:用二氮杂萘聚醚砜酮类聚合物与氯仿、无水乙醇或正丁醇按照一定的质量比混合,磁力搅拌后得到混合均匀的铸膜液,过滤并真空脱泡;将铸膜液采用刮刀在无纺布上刮制成一定厚度的膜,该膜在一定湿度和温度的空气中静置24h后即得到二氮杂萘聚醚砜酮类平板超滤膜。

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