氯乙醇

Spiral Spirobifluorene acetylated is oxidated by m-chloroperoxybenzoic acid and hydrolyzed by sodium hydroxide ,obtaining 2,2 '- dihydroxy -9,9'- spiral Spirobifluorene .Through nitrification,Reduced by hydrazine hydrate, we may get the 2,2 '- diamino -9,9'- spiral Spirobifluorene which are characterizated by IR, 1H-NMR !

L-酒石酸和乙醇酯化得到酒石酸二乙酯，将保护羧基保护起来，然后用碘甲烷在2，3-位上两个甲基，得到2，3-二甲氧基-酒石酸二乙酯，再用氢氧化钠将其水解，得到2，3-二甲氧基-酒石酸，用五氯化磷将羧基酰化，得到2，3-二甲氧基- 1，4-丁二酰氯，经过与二环己胺反应，得到拆分配体2，3-二甲氧基–N，N，N'，N'-四环己丁二酰胺。

By bioactivity-guided isolation, 14 compounds were obtained from the active fractions. 13 of them were determined as 9,9'-dihydroxy-8,8'-dimethoxy- l,r-methyl-lH,lH'-[4,4']binaphtha

本研究利用稻瘟霉筛选体系对红葱的60％乙醇提取物及其氯仿、正丁醇和水的萃取部分进行了活性筛选，并对活性部位的活性化学成分进行了跟踪分离，从中分离得到十四个化合物，利用物理化学和光谱学的方法对其中十三个化合物的结构进行了鉴定，分别为9，9'-二羟基-8，8'-二甲氧基-1，1'-二甲基-1H，1H'-[4，4']双萘并

Under ultrasonic extraction, comparing the ratio of total alkaloid with 95% ethanal, hloroform, methanol.

用超声波提取法比较了以95%乙醇、氯仿、甲醇为溶剂的提取率，结果依次为1.21%、1.57%、1.54%。

Methhods:1:The chemical components of Chinese herbal medicines extracted with petroleum ether,chloroform, ethyl acetate,ethenol and water respectively were analyzed and compared.2.The specimens were analyzed with ultraviolet-visible absorption spectrophotometry.

(1)按中药多分子体系的脂溶性差异，分为石油醚、氯仿、乙酸乙脂、乙醇和水的溶出性成分集合，然后进行&对药&与非&对药&的对比分析；(2)用紫外-可见光光度计测定吸收光谱曲线。

The long wave ultraviolet grass green fluorescence function material is synthesized with the p-toluensulfonyl chloride and o-amino benzoic acid as raw materials,pyridine as solvent,and sodium ethoxide as activator.

缑卫军，刘新奇，紫外长波草绿荧光功能材料的合成研究以对甲苯磺酰氯和邻氨基苯甲酸为原料，吡啶为溶剂，乙醇钠为催化剂，合成紫外长波草绿荧光功能材料。

A process for preparingp-fluo-2-(2-methyl-3-propionyl)-4-oxy-N,3-diphenyl-phenylbutylamide includes such steps as Friedle-Craft acylating of newly prepared phenylacetyl chloride and fluorobenzene under catalysis of AlCl3 to obtain 4-fluoro-phenylbenzyl ketone, brominating at carbonyl alpha position under catalysis of less AlCl3 to obtain alpha-bromo-4-fluo-phenylbenzyl ketone, and condensing with isobutyryl acetanilide under action of sodium ethoxide.

本发明涉及一种制备对氟－2－(2－甲基－3－氧丙基)－4－氧－N，3－二苯基－苯丁酰胺(1)的方法，其包括以下步骤：新制的苯乙酰氯与氟苯在AlCl3催化下进行Friedle－Craft酰化反应，得到对4－氟－苯基苄基酮(4)；化合物(4)在少量AlCl3催化下进行羰基α位溴化，得到α－溴－4－氟－苯基苄基酮(5)；然后(3)异丁酰乙酰苯胺在乙醇钠作用下与化合物(5)进行缩合。

Using a simple and reliable apparatus,the solubilities of glutaric acid in water,ethanol,toluene,chloroform,n-butanol and acetone are determined by the analytic method.

用平衡法分别测定了戊二酸在水、乙醇、甲苯、氯仿、正丁醇、丙酮中的溶解度数据。

At the same time, for the alternatives, another set of devices was also set up according to balanced method. From above two experiments, we got solubility datas of succinic acid, glutaric acid and adipic acid in six solvents of water, ethanol, n-butanol,choloroform, acetone and toluene, of which most were measured for the first time.

由合成法和平衡法实验测定了丁二酸、戊二酸和己二酸三种溶质在水、乙醇、正丁醇、氯仿、丙酮、甲苯六种溶剂中的溶解度数据，其中大部分体系和溶解度数据是首次测定。

They usually contain Salicylic Acid, Glycolic Acid, Benzoyl Peroxide, Chlorhexidine and Tea Tree Oil.

他们通常含有水杨酸、乙醇酸、过氧化苯甲酰、氯、茶树油。

Four kinds of systematic solvents: hexamethylene, chloroform, alcohol and water were applied to extract the different components orderly from Maca, and the finger print spectra of the components were measured and analyzed by virtue of the two indexes.

测定了内蒙、甘肃、新疆的十种甘草的系统三溶剂氯仿、无水乙醇和水提取物的三维紫外指纹图谱、HPLC指纹图谱、红外指纹图谱，进行了共有峰率和变异峰率分析。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了