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The route include three steps: etherification, ammoniation and then oxidation. Factors such as chloracetate, reaction temperature on process were studied. And discussed the ionic liquid was recovered.

讨论了不同的氯乙酸酯和反应温度对醚化反应收率的影响,讨论了不同的二苯甲硫乙酸酯对氨解反应收率的影响,及离子液体的回收使用。

P chlorophenoxyacetic sodium was synthesized by p chlorophenol with 2 chloroacetic acid in the 20% hydroxide sodium aqueous solution.

采用一步法由氯乙酸与对氯苯酚在氢氧化钠质量分数为 0 2的水溶液中的反应制得。

After pioneering the development of recent years has become a larger national, Henan The largest amino acid, chloroacetic acid production base.

经过近几年的创业发展,已成为全国较大、河南最大的氨基乙酸、氯乙酸生产基地。

Production technology of synthesis of allantoin are reviewed, including glyoxal oxidation, electrochemical synthesis, calcium glyoxylate synthesis, dichloroacetic acid synthesis, ace-tochloral method, and oxidative decarboxylation.

评述了乙二醛氧化法、化学法、醛酸钙法、素三氯乙醛合成法、酸二氯乙酸法和尿酸氧化脱羧法等合成尿囊素的各种工艺。

The difficulty of route is the refinement of products. There is a lot of sodium chloride in solution. In order to refine the glycolic acid, the methods of vacuum distillation and organic solvent extraction are adopted.

水解合成后得到的是羟基乙酸的水溶液,其中含有大量的氯化钠和少量未水解的氯乙酸及其它杂质,采用减压蒸馏及有机溶剂萃取方法进行精制是比较适宜。

In this method, titration with standard solution of perchloric acid in glacial acetic acid was used.

建立了在非水条件下快速测定食品中糖精钠的方法,以冰乙酸为溶剂,用高氯酸的冰乙酸标准溶液滴定,经过反复试验,相对标准误差0.92%~2.93%,加标回收率97.13%~100.3%,结果表明;该法定量分析准确,精确度高,可靠性和重现性好。

The extraction of Pr3+was studied by using heptane containing bis(2-ethylhexyl)phosphinic acid in sodium perchlorate,chloroacetic acid and citric acid medium ,respectively.

研究了二(2-乙基己基)膦酸(PIA-8)的庚烷溶液分别在高氯酸钠、氯乙酸、柠檬酸介质中对Pr3+的萃取。

The biogenic amines in test samples were extracted by 10% trichloroacetic acid and then derived with benzoyl chloride. The HPLC analysis for the samples were conducted as the following condition: mobile phase was a gradient elution program of methanol and water, the flow rate was 0.8 mL/min.

用10%的三氯乙酸提取样品中的生物胺,采用苯甲酰氯衍生处理后,以甲醇/水为流动相,进行梯度洗脱,流速0.8 mL/min,紫外检测器波长为254 nm。

In the current study, anoxic dechlorinations of p, p'-DDT,γ-HCH, HCB in the Liao River sediment were studied under the following conditions: without any additional short chain carbon substrates or vitamin B〓; with the addition of short chain carbon sources (including sodium lactate, sodium propionate or sodium acetate); with the addition of vitamin B〓; with the addition of both short chain carbon substrates and vitamin B〓, with the addition of sodium dodecyl sulfate , a kind of surfactant; the coexistence of the three chlorinated compounds.

本文分别采用不外加碳源和维生素B〓外加碳源(包括乳酸钠、丙酸钠或乙酸钠)、外加维生素B〓以及同时外加碳源和维生素B〓的方法,考察了p,p'-DDT、γ-HCH和HCB三种氯代有机污染物单独或混合存在下,在辽河沉积物中缺氧脱氯降解的情况,主要得到以下结论

Absorption kinetic curves for two mixed solvent/polyurethane membrane systems (ethanol-1, 2-dichloroethane/PU and ethanol-ethyl acetate/PU) are measured, the replacement is observed in experiment. Dual mode theory combining Henry's law and B.

系统地测定了乙醇-乙酸乙酯和乙醇-1.2-二氯乙烷混合溶剂在聚氨酯膜中的吸收动力学曲线,发现了乙醇对膜内1,2-二氯乙烷的顶替现象,并运用亨利定律+B.E.T。

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