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This paper introduces in detail the factors influencing the yield of the amino acetic acid with the chloroacetic acid ammonolysis process, and connecting with the production procedures, makes deep analysis, and puts forward some corresponding methods for increasing the yield.

详细介绍了氯乙酸氨解法氨基乙酸生产过程中影响收率的因素,并结合生产过程进行了深入分析,有针对性地提出了提高收率的办法。

When the molar ratio of 2 chloroacetic acid∶ p chlorophenol is 1.25 and pH=5~7 at 104 ℃ reaction for 20 min in the 20% NaOH solation,the yield of PCPA can be reached 90%.

氯乙酸∶对氯苯酚为 1 2 5 ,质量分数为 0 2的氢氧化钠溶液中,pH值在 5~ 7之间,温度在 10 4℃左右为宜,反应时间为 2 0min ,PCPA收率为 90 3%。

The productions of glycin oxidation are complicated and the cost is high. The cyanogenesis is poisonous and unsafe.

国内外合成羟基乙酸的方法主要有甘氨酸氧化法、氰化法、醛类羧化法、甲醛和甲酸甲酯偶联法、草酸电解法、氯乙酸水解法等。

Six derivatives of 4-phenyl-3-phenoloxymethyl-5-mercapto-1,2,4-triazlyole were synthesized from phenoloxyacetyl hydrazide by two-steps reaction under microwave irradiation, then reacted with 2-chloroacetic acid to give six novel derivatives of 2-(3-phenoxymethyl-4-phenyl-[1,2,4]triazole-5-thio)-acetic acid.

在微波辐射条件下,芳氧乙酰肼经两步反应制得4-苯基-3-芳氧甲基-1,2,4-三唑-5-硫酮衍生物,再与氯乙酸反应得到6种尚未见文献报道的2-(3-芳氧甲基-4-苯基-1,2,4-三唑-5-硫基)乙酸衍生物。

On the basis of the development of a new CE method for the analysis of α-lactalbumin,β-lactoglobulin A and β-lactoglobulin B, different concentrations of acetic acid and trichloroacetic acid for the removal of proteins in raw milk, infant formula A and B, and yogurt were investigated.

建立了毛细管电泳法分析α-乳白蛋白、β-乳球蛋白A及β-乳球蛋白B的方法,考察了不同浓度冰乙酸及三氯乙酸对原料奶、婴儿配方奶粉A和B及酸奶中蛋白的去除效果。

The surface hydroxyl group onto magnetic polyvinyl acetate nanoparticles can be obtained by saponification reaction on their surface.

结果表明,磁性聚苯乙烯颗粒与丁二酸酐发生Freidel-Crafts酰基化反应,可以在颗粒表面引入少量羧基;磁性聚甲基丙烯酸甲酯颗粒分别与乙二醇、二缩三乙二醇、聚乙二醇等发生醇-酯交换反应,可以在颗粒表面接枝不同分子链长度的末端羟基;磁性聚醋酸乙烯酯颗粒经过醇解或皂化反应可以获得表面羟基;磁性聚丙烯酸甲酯颗粒通过乙二胺或1,6己二胺的胺解反应可以得到表面氨基,继而与一氯乙酸反应可以引入亚胺二乙酸基团。

Production technology of synthesis of allantoin are reviewed, including glyoxal oxidation, electrochemical synthesis, calcium glyoxylate synthesis, dichloroacetic acid synthesis, acetochloral method, and oxidative decarboxylation.

评述了乙二醛氧化法、电化学法、乙醛酸钙法、尿素三氯乙醛合成法、尿酸二氯乙酸法和尿酸氧化脱羧法等合成尿囊素的各种工艺。

By single factor experiment,experiment studied on the effect on the dosage of NaOH、CHPTMA、sodium chloroacetate 、temperature and time to reaction.

并通过单因素实验讨论了NaOH用量、氯乙酸钠用量、3-氯-2-羟丙基三甲基氯化铵用量、反应温度和反应时间等对合成反应的影响。

Ethyl phenoxyacetate has been synthesised by the reaction of phenol with ethyl chloroacetate under the condition of solid-liquid phase transfer catalysis using PEG-400 as the catalyst.

于固一液相转移催化条件下,以PEG-400为催化剂,通过苯酚与氯乙酸乙酯反应合成了苯氧基乙酸乙酯。与85%的水合肼作用得到相应的酰肼。

The article introduced that α-Naphthaleneacitic acid was synthesized from naphthalene and chloroacetic acid in presence of aluminium powder.

介绍了萘和氯乙酸在铝粉催化下合成α—萘乙酸的研究。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

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