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Their structures were confirmed by elemental analysis, 1H NMR, and IR spectral data. The preliminary bioassay results showed that α-phenyl-sul-fonylcyclododecanone oxime 2,4-dichlorophenoxy acetate (8p) had inhibition ratio 100% and 80.07% against Digitaria sanguinalis Scop., and 100% and 88.70% against Abutilon theophrasti Medic. at concentrations of 100 and 1 mg/L.

初步生物活性测定结果显示,部分化合物具有一定的除草活性,如α-苯磺酰基环十二酮肟-2,4-二氯苯氧乙酸酯(8p)在浓度为100和1 mg/L时对马唐的抑制率分别为100%和80.07%;对苘麻的抑制率分别为100%和88.70%。

Our company adopt advanced production technology and equipment, to paint in different modified resin system pre-dispersion, used for high-grade inks, paints and coatings production, the main products are lipid soluble and alcohol soluble nitrocellulose pre-dispersed pigment-based color films, water-based acrylic paints pre-dispersed color tablets, chlorine vinegar pre-dispersed pigment color polymer films, cellulose acetate butyrate pre-dispersed pigment color films, polyvinyl butyral pre-dispersed pigments, such as color film.

本公司采用先进的生产技术和设备,把颜料在不同的改性树脂体系中进行预先分散,用于高档油墨、油漆和涂料的生产,主要产品有脂溶和醇溶型硝化棉预分散颜料色片、水性丙烯酸预分散颜料色片、氯醋聚合物预分散颜料色片、乙酸丁酸纤维素预分散颜料色片、聚乙烯醇缩丁醛预分散颜料色片等。

And the operational condition was as follows: 100-200 mesh silica gel to be the stationary phase, solvent system of methlene chloride: ethyl acetate: ethanol = 80:35:5 to be the eluent, the flow rate of the eluent to be 2.0 mL/min, the feeding concentration of pristinamycins to be 2.26 g/L, the total loading amount of the silica gel to be 0.81 mg/g and the temperature to be 25℃.

优化后的柱层析操作条件为:选用100~200目的硅胶,二氯甲烷:乙酸乙酯:乙醇=80:35:5为洗脱剂,流速为2.0 mL/min,普那霉素的进样浓度为2.26g/L,硅胶的总负载量约为0.81 mg/g,温度为25℃。

Callus derived from petiole explants of Panax japomcus var. major produced three cyanidin glycosides as major anthocyanin pigments in darkness. Anthocyanin synthesis was remarkably stimulated by 2,4-dichlorophenoloxyacetic acid in combination with kinetin in MS medium. The pigment content of the callus reached up to 34. 14 mg/g fw.

从珠子参(panax japonicus var.major)叶柄诱导的愈伤组织在暗培养条件下主要形成3种花色甙色素,且均以矢车菊素为甙元。2,4-二氯苯氧乙酸和激动素的组合能明显地促进色素的合成,色素含量可达34.14mg/g fw。

Callus deried from petiole explants of Panax japomcus ar. major produced three cyanidin glycosides as major anthocyanin pigments in darkness. Anthocyanin synthesis was remarkably stimulated by 2,4-dichlorophenoloxyacetic acid in combination with kinetin in MS medium. The pigment content of the callus reached up to 34. 14 mg/g fw.

从珠子参(panax japonicus ar.major)叶柄诱导的愈伤组织在暗培养条件下主要形成3种花色甙色素,且均以矢车菊素为甙元。2,4-二氯苯氧乙酸和激动素的组合能明显地促进色素的合成,色素含量可达34.14mg/g fw。

Methhods:1:The chemical components of Chinese herbal medicines extracted with petroleum ether,chloroform, ethyl acetate,ethenol and water respectively were analyzed and compared.2.The specimens were analyzed with ultraviolet-visible absorption spectrophotometry.

(1)按中药多分子体系的脂溶性差异,分为石油醚、氯仿、乙酸乙脂、乙醇和水的溶出性成分集合,然后进行&对药&与非&对药&的对比分析;(2)用紫外-可见光光度计测定吸收光谱曲线。

The parasiticidal effect of ethanol extracts from a plant Dioscorea zingiberensis on dactylogyrid Dactylogyrus intermedius found in goldfish was studied to search for parasiticidal substances by standard laboratory procedures compared with the other four drugs mebendazole, abamectin, ivermectin and praziquantel.

以寄生在金鱼Carassius auratus鳃部的中型指环虫Dactylogyrus intermedius为指示寄生虫,采用活体感染、活体杀虫的方法,研究了用不同溶剂(石油醚(沸程60~90℃)、氯仿、乙酸乙酯、乙醇和水)分别对盾叶薯蓣Dioscorea zingiberensis进行提取,其5种提取物的杀虫活性。

The inhibition effect of chloroform fraction was the most potent, with the inhibition rate about more than 83% to 5 plant pathogenic fungi under the concentration of 15mg/mL. Under the concentration of 15mg/mL, the ethyl acetate fraction and n-butanol fraction thoroughly inhibited the growth of Alternaria solani and Valsa mali, with the inhibition rate up to 100%. The n-butanol fraction showed the highest potent virulence, with EC50 to Alternaria solani and Valsa mali about 0.09 and 0.279 mg/mL respectively.

其中氯仿部分的抑菌效果较好,当质量浓度为15mg/mL时,其对5种植物病原菌的抑制率均在83%以上;15mg/mL乙酸乙酯部分和正丁醇部分分别对番茄早疫病菌和苹果腐烂病菌有强烈且稳定的抑制作用,抑制率达100.00%,正丁醇部分对这两种菌丝生长抑制毒力最好,EC50分别为0.090和0.279mg/mL。

Results: The polymer taking MAA as functional monomer and acetic ether as solvent obtained higher selectivity for desloratadine.

结果:研究表明,采用MAA为功能单体,以乙酸乙酯做溶剂合成的地氯雷他定MIP对模板分子的结合性最佳。

Optimization technology was acetidin: N-hexane (3:7) as low-pole solvent system, methanol: dichloromethane (1:9) as polar solvent system, 20% glycerol filter paper as moisturizer, 14 h age Bacillus subtilis as indicating strain seed on thin layer plate cultivated for 14~18 h, 1% TTC staining time 1~2 h, bacterial mix method suitable to 0.2%~0.6% agar semisolid bouillon culture-medium, bacterial spread method suitable to 1% agar semisolid bouillon culture-medium.

结果:该方法展开系统筛选简单,抑菌斑位置准确、斑点清晰,其优化条件为:以乙酸乙酯:正己烷(3:7)为弱极性展开系统,甲醇:二氯甲烷(1:9)为强极性展开系统,用20%甘油滤纸对湿室保湿,以14h菌龄的枯草芽孢杆菌为指示菌种子液,自显影薄层板36℃培养14~18h,1%TTC显色时间为1~2h,含0.2%~0.6%琼脂的半固体肉汤培养基应使用混菌法生物自显影,含1%琼脂半固体肉汤培养基应使用涂布法生物自显影。

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