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Trichloroacetic acid was esterified by acid and methanol,and FID detector was used.

建立一种可靠的测定水中三氯乙酸含量的气相色谱法。

The method is raw material with pyrimidine of 5- fluorine make water, after reacting with chloric second acid below the intention that changes potassium in oxyhydrogen, with complex intermediate body 2- amino - 5- is replaced - 1, 3, 2 Zun reaction makes 4- Sai target content, evaluate its to fight tumor active.

方法以5-氟尿嘧啶为原料,在氢氧化钾的功能下和氯乙酸反应后,和合成的中间体2-氨基-5-取代-1,3,4-噻二唑反应制得目标物,并评价其抗肿瘤活性。

The yield of borneol and isoborneol was 52.93%,and selectivity for borneol was 60.46%at the conditions of programmed temperatures,reaction time 315 min,saponification time 1h,mass part of catalyst 5%,and terpineol:chloroacetic acid 100∶25.

酯化反应采用程序升温,时间315 min,皂化时间1 h。催化剂用量为松节油质量的5%,松节油∶氯乙酸为100∶25时,龙脑得率为52.93%,正龙脑的选择性为60.46%。

The yield of borneol and isoborneol was 52.93%,and selectivity for borneol was 60.46%at the conditions of programmed temperatures,reaction time 315 min,saponification time 1h,mass part of catalyst 5%,and terpineol:chloroacetic aci...

酯化反应采用程序升温,时间315 min,皂化时间1 h。催化剂用量为松节油质量的5%,松节油∶氯乙酸为100∶25时,龙脑得率为52.93%,正龙脑的选择性为60.46%。

Methyl chloroacetate is used widely as a industrial material,for example as a middle material in pesticide and medicine making.

氯乙酸甲酯是一种应用广泛的化工原料,多用于医药、农药生产的中间体,本试验对其进行了卫生毒理学评价。

Synthesis of ethyl chloroacetate with chloroacetic acid and ethanol catalysed by GdCl2-EDTB-H3SiW12O40was investigated.

研究了反应时间、醇酸比、带水剂用量及催化剂用量对杂多酸化合物GdCl2-EDTB-H3SiW12O40催化合成氯乙酸乙酯的影响,确定了最佳反应条件,醇酸摩尔比1.5∶1,带水剂量10mL,催化剂使用量为酸的1.0%,反应时间2.5h

Fibers with different degrees of carboxymethylation were prepared by controlling the ratio of the weight of fiber to chloroacetic acid.

通过控制氯乙酸和纤维的质量比得到不同反应程度的羧甲基纤维素纤维。

Based on the result of orthogonal experiment, theoptimum condition of the esterification reaction of chloroacetic acid with polyethylene glycolwas determined.

采用正交实验法对合成的双氯乙酸聚乙二醇酯的反应工艺条件进行了优化,确定了最佳合成路线。

Application of organic acid catalysis to the polymerization of pyrroles and pentafluorobenzaldehydes, with the xylene as reaction medium instead of expensive collidine used in the conventional methodology, resulted in a relatively high yield of TPFPPH〓.

本研究利用有机酸如氯乙酸催化吡咯和五氟化苯甲醛聚合,并以二甲苯替代传统方法所用的昂贵溶剂2,4,6-三甲基吡啶,获得了产率较高的TPFPPH〓。

Optimal process conditions for preparing 2-oxo-1, 4-piperazine diacetic acid(3-KP): 2-oxo-1-piperazine acetic acid was combined with chloroacetic acid at a mole ratio of 1 to 1.1, at temperature 40℃for 8 hours.

通过单因素分析,合成3-KP 的最佳反应条件为:反应温度为40℃,反应时间为8 小时,氯乙酸∶S-KP 的摩尔比为1.1∶1。

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