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氯乙酸

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To improve the yield of an Amide-type Tripodal Ligand and investigate its coordination with rare earth ion under mild condition,a series of Amide-type Tripodal Ligands(L1—L4) have been prepared by the reactions of nitrilotriacetic acid and oxalyl chloride with four kinds of amides,respectively.

为了提高酰胺型三脚架型配体的产率,进一步研究其与稀土离子的配位形式及配合物的荧光性能,以氨三乙酸为母体,草酰氯为氯化试剂,与4种胺在较温和的条件下合成了具有三脚架型结构的配体(L1—L4),并考察了实验条件、反应温度、反应体系溶剂、缚酸剂、反应时间及催化剂对反应产率的影响。

Kinetic spectrophotometric method for the determinationof trace nitrilotriacetic acid;2. To improve the yield of an Amide-type Tripodal Ligand and investigate its coordination with rare earth ion under mild condition,a series of Amide-type Tripodal Ligands(L1—L4) have been prepared by the reactions of nitrilotriacetic acid and oxalyl chloride with four kinds of amides,respectively.

为了提高酰胺型三脚架型配体的产率,进一步研究其与稀土离子的配位形式及配合物的荧光性能,以氨三乙酸为母体,草酰氯为氯化试剂,与4种胺在较温和的条件下合成了具有三脚架型结构的配体(L1—L4),并考察了实验条件、反应温度、反应体系溶剂、缚酸剂、反应时间及催化剂对反应产率的影响。

Cefixime open side chain acid was prepared by oximation,etherification,chlorination,ester decomposition using t-butyl acetoacetate as starting material.

以乙酰乙酸叔丁酯为原料,经过肟化、醚化、氯代酯解反应合成了头孢克肟开环侧链酸。

The method of degradation of 2,4-dichlorophenoxyacetic acid by ozonation in a cylindrical bubbling tower reactor was proposed.

引言2,4-二氯苯氧乙酸(2,4-D,又名2,4-滴)是一种广泛使用的除草剂[1],应用历史较长,是我国主要的除草剂品种之一,用量也比较大。

The parasiticidal effect of ethanol extracts from a plant Dioscorea zingiberensis on dactylogyrid Dactylogyrus intermedius found in goldfish was studied to search for parasiticidal substances by standard laboratory procedures compared with the other four drugs mebendazole, abamectin, ivermectin and praziquantel.

以寄生在金鱼Carassius auratus鳃部的中型指环虫Dactylogyrus intermedius为指示寄生虫,采用活体感染、活体杀虫的方法,研究了用不同溶剂(石油醚(沸程60~90℃)、氯仿、乙酸乙酯、乙醇和水)分别对盾叶薯蓣Dioscorea zingiberensis进行提取,其5种提取物的杀虫活性。

NAA, CPPU and EBR all induced parthenocarpic growth together with active cell division and enhanced transcripts of cell cycle-related genes.

奈乙酸,N-(2-氯-4-吡啶基)-N-苯基脲和表油菜素内酯都能诱导黄瓜单性结实,加快细胞分裂和提高细胞周期相关基因的表达。

An ester or a salt of perchloric acid .Indocin is the trade name of this nonsteroidal anti-inflammatory drug.

氯苯基甲氧基甲基吲哚乙酸是一种非固醇抗炎药物的商标名称。

Goodcatalytic activities of the phosphine palladium complexes were observed incarbonylation of benzyl chloride with atmospheric CO. In some reactions the yieldof phenylacetic acid was 91% and the catalyst could be reused repeatedly in severaltimes.

这些钯配合物催化苄基氯的常压羰基化反应有较好的催化活性,有些反应中苯乙酸的产率可达91%,可重复使用,是一类环境友好的新型绿色催化剂。

The synthetic route starts from penicillin G, peroxyacetic acid(8.5%) as Oxidizing Agent to get penicillin G sulfoxide; esterifided with p-nitrobenzyl bromine to synthesize penicillin G sulfoxide ester; we synthesize 3-exomethylenecepham sulfoxide ester with phthalimide potassium and 4A molecular sieve as acid scavenger to open the ring, SnCl_4 as catalyzation to close the ring. The yield is over 60%.

本研究采用的合成路线为:以青霉素G钾盐为原料,选用工业过氧化氢制备的过氧乙酸(22.3%)稀释至8.5%为氧化剂,氧化得青霉素亚砜;采用对硝基溴苄为酯化试剂,制备青霉素亚砜酯;以NCP(N-氯代邻苯二甲酰亚胺)为开环试剂,酞酰亚胺钾和4A型分子筛为酸清除剂,顺利开环;再经无水SnCl_4催化闭环得3-环外亚甲基头孢亚砜酯,最终产率在60%以上。

The effects of the extracts from Brucea javanica using chloroform and ether acetate on the activity of protease and the protein contents of Pieris rapae were studied.

鸦胆子氯仿和乙酸乙酯提取物对菜青虫幼虫蛋白酶的活性和蛋白质含量均有明显影响。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

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