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Firstly, we studied the photocatalytic hydrogen evolution and decomposition of the pollutants over Pt/TiO_2 in the presence of chloroacetic acids.

首先,我们研究了氯代乙酸存在下Pt/TiO_2上光催化生成氢的反应。

Firstly, 3-ethylthiobutanal was prepared from crotonaldehyde reacting with ethanehiol in triethylamine with high yield. Secondly, methyl acetoacetate was converted to 6-ethylthiohept-3-en-2-one by three steps via hydrolysis, condensation with 3-ethyltio-butanal and dehydration, then 6-ethylthiohept-3-en-2-one was cycloco ndensed with dimethyl malonate by Michael addition and Claisen condensation, followed by saponification and decarboxylation to give the intermediate of 5-(2-ethylthiopropyl)-cyclohexane-1,3-dione.

首先,以巴豆醛与乙硫醇为原料,在三乙胺的催化作用下高收率制得3-乙硫基丁醛;然后从乙酰乙酸甲酯出发,通过碱水解、与3-乙硫基丁醛缩合、脱水三步反应合成6-乙硫基-3-烯-2-庚酮,接着6-乙硫基-3-烯-2-庚酮与丙二酸二甲酯通过Michael加成和Claisen缩合成环,再通过皂化和脱羧反应生成中间体5-[2-丙基]-1,3-环己二酮;再与丙酸酐反应丙酰化,最后与0-3-氯-2-丙烯基羟胺肟化,得到目标化合物烯草酮。

Callus derived from petiole explants of Panax japomcus var. major produced three cyanidin glycosides as major anthocyanin pigments in darkness. Anthocyanin synthesis was remarkably stimulated by 2,4-dichlorophenoloxyacetic acid in combination with kinetin in MS medium. The pigment content of the callus reached up to 34. 14 mg/g fw.

从珠子参(panax japonicus var.major)叶柄诱导的愈伤组织在暗培养条件下主要形成3种花色甙色素,且均以矢车菊素为甙元。2,4-二氯苯氧乙酸和激动素的组合能明显地促进色素的合成,色素含量可达34.14mg/g fw。

Callus deried from petiole explants of Panax japomcus ar. major produced three cyanidin glycosides as major anthocyanin pigments in darkness. Anthocyanin synthesis was remarkably stimulated by 2,4-dichlorophenoloxyacetic acid in combination with kinetin in MS medium. The pigment content of the callus reached up to 34. 14 mg/g fw.

从珠子参(panax japonicus ar.major)叶柄诱导的愈伤组织在暗培养条件下主要形成3种花色甙色素,且均以矢车菊素为甙元。2,4-二氯苯氧乙酸和激动素的组合能明显地促进色素的合成,色素含量可达34.14mg/g fw。

Using ethyl cyanoacetate , triethyl orthoformate and methylhydrazine as main raw materials, the herbicide pyrazosulfuron was prepared through the reactions of substitution, amination, cylclization, diazotization and chlorosulfonation.

以氰乙酸乙酯、原甲酸三乙酯和甲肼等为主要原料,通过取代、胺化、环化、重氮化和氯磺化等反应制得了除草剂吡嘧磺隆原料药。

Pharmaceutical characteristics of dimethylamino ethyl(4-chlorophenylmethfoxy )acetate hydrochloridein rabbit was studied and several parameters at different timeand way of medicine administration were determined.

研究了4-氯代苯甲氧基乙酸二甲氨基乙酯盐酸盐在家兔体内的药代动力学,测定了不同时间不同给药方式家兔体内的血药浓度及动力学参数。

Methhods:1:The chemical components of Chinese herbal medicines extracted with petroleum ether,chloroform, ethyl acetate,ethenol and water respectively were analyzed and compared.2.The specimens were analyzed with ultraviolet-visible absorption spectrophotometry.

(1)按中药多分子体系的脂溶性差异,分为石油醚、氯仿、乙酸乙脂、乙醇和水的溶出性成分集合,然后进行&对药&与非&对药&的对比分析;(2)用紫外-可见光光度计测定吸收光谱曲线。

The hypha growth-inhibiting method and the virulence determination method were used to investigate the inhibition effects of the petroleum ether fraction, chloroform fraction, ethyl acetate fraction, n-butanol fraction and water fraction in the alcoholic extracts from the aboveground of Peganum harmala L.

采用抑制菌丝生长法和毒力测定法,研究了骆驼蓬地上部醇提物的石油醚、氯仿、乙酸乙酯、正丁醇和水5个极性部位对南瓜枯萎病菌、西瓜枯萎病菌Fusarium oxysporum f。

Results There were about 15 kinds of chemical poisons including vinyl chloride,polyvinyl alcohol,isoparaffin,polyvinylacetate,sodium hydrate,ammonia,acid hydroc,methanol,diesel oil,carbon monoxide,carbon dioxide,sulfur dioxide,nitrogen oxides,ozo...

结果在聚氯乙烯的生产过程中,作业场所存在化学毒物较多,主要包括氯乙烯、聚氯乙烯、聚乙烯醇、过氧化物、异链烷烃类、聚乙烯乙酸酯、氢氧化钠、氨、盐酸、甲醇、柴油、一氧化碳、二氧化碳、二氧化硫、氮氧化物、臭氧、二氧化锰等。

Rats in the experimental group received conventional fixation, and then decalcified with modified decalcifying fluid [10 mL of methanoic acid, 8 mL of concentrated hydrochloric acid (1.19 relative density, 3 g of aluminum chloride, 20 mL of formaldehyde (0.4 volume fraction), 3 mL of glacial acetic acid, adding to 200 mL with saline solution], dehydrated, transparentized with chloroform, and then embedded for a long time, dyed, mounted and made into tissue sections.

实验组经过常规固定,而后应用改良脱钙液(甲酸10 mL、浓盐酸(相对密度1.19)8 mL、氯化铝3 g、体积分数为0.4的甲醛20 mL、冰乙酸3 mL,加生理盐水至总体积200 mL)脱钙、脱水、氯仿透明、包埋时间延长、染色、封固和切片;对照组进行常规固定、脱钙、脱水、透明、包埋、染色、封固和切片。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

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