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氯乙酸

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The process of synthesizing DMGHCl with monochloroacetic acid as the starting material was simple and safte and the raw materials were easily obtained. It was suitable for Industry.

氯乙酸路线合成二甲基甘氨酸盐酸盐工艺简单,原料易得,安全性高,适合进行产业化。

Under alkaline conditions, carboxymethyl konjac glucomannan with different degree of substitution was prepared through reaction of monochloroacetic acid and konjac glucomannan using isopropyl alcohol as dispersing agent.

以异丙醇为分散剂,在碱性介质中一氯乙酸和魔芋葡甘聚糖反应制备了系列羧甲基魔芋葡甘聚糖。

In the CMKGM preparation section,with the indicators of DS andη, the optimum laboratory conditions preparation of a certain molecular weight of the high DS of CMKGM: reaction time (5~6) h, the theory of the degree of substitution (2~3), the molar ratio of monochloroacetic acid to Sodium hydroxide (2:1~3:1),the reaction temperature (55~65)℃, liquid ratio (10:1~12:1)mL/g, containing enthanol (50~70)%.

CM(来源:5e60ABC论文网www.abclunwen.com)KGM制备工艺研究中,以取代度、表观粘度为指标,建立了制备一定摩尔质量的高DS的CMKGM的实验室制备条件:反应时间(5~6)h、理论取代度(2~3)、氢氧化钠与氯乙酸摩尔比(2:1~3:1)、反应温度(55~65)℃、液料比(10:1~12:1)mL/g、乙醇体积分数(50~70)%。

Then, the multidentate amine immobilized on silica gel was used as ligand for CuCl in ATRA of CCl_4 with MMA and methyl trichloroacetate with St repeatly. The conversion and purity of the product were determined through the gas chromatography and ~1H NMR respectively. Finally, the multidentate amine immobilized on silica gel was used as ligand for CuCl in ATRP of St initiated by TCPP and MMA initiated by MMTCB. The number average molecular weights of the polymers were determined through GPC.

此多齿胺改性硅胶配体被分别多次重复用于四氯化碳与甲基丙烯酸甲酯,三氯乙酸甲酯与苯乙烯的ATRA反应中,通过气相色谱测定了原料的转化率随时间的变化,且通过核磁~1H NMR测定了产物的纯度,我们还进一步将此种多齿胺改性硅胶配体用于TCPP引发St的ATRP和MMTCB引发MMA的ATRP反应中,通过GPC测定所得聚合物的分子量。

According to the result showed at 280nm and at 490nm,in the comparison of whether protein absorption top and sugar quantity top overlapped,glycoproteins would be detected preparatorily,and as a result,tubes in two distinct areas had glycoproteins by this method. Proteins were precipitated with trichloroaceticacid and with cold acetone,and glycoprotein was determined from SDS-gel.

再从各收集管的收集液中,用三氯乙酸沉淀蛋白法、冷丙酮沉淀蛋白法相结合浓缩、制备蛋白样品,进行SDS—PAGE,对SDS胶进行PAS糖链染色鉴定糖蛋白,并从茶树叶分级蛋白中准确地鉴定出两个区域的收集管中含有多种糖蛋白。

Firstly the mid-pruduct imidazoline was produced by reaction of naphthenic acid and diethylene triamine, then the corrosion inhibitor amphoteric imidazoline, which is soluble in water, was produced by reaction of imidazoline and sodium monochloroacetate in aqueous solution.

以高纯环烷酸与二乙烯三胺反应合成了中间体咪唑啉,再以去离子水为溶剂,用氯乙酸钠对该中间体进行两性化,制得了水溶性两性咪唑啉缓蚀剂。

Results It has been shown that trichloroacetic acid was the better one as cross-link agent.

结果 三氯乙酸是较好的交联剂。

BCA method conjugated with trichloroacetic acid is adaptable to the rapid and sensitive determination of protein in powdered milk.

结合三氯乙酸沉淀的BCA法适用于奶粉中蛋白质的快速检验和掺伪检验。

The two indexes, degree of hydrolysis and 10% trichloroacetic acid-soluble nitrogen content, were used to compare the four kinds of proteolysis in naturally .

以蛋白水解度和10%三氯乙酸可溶性氮含量为指标,比较四种蛋白酶在两种工艺下水解的情况。

Tissues were treated with trichloroacetic acid to precipitate impurities.

样品处理采用30%三氯乙酸沉淀内源性杂质。

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