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氯乙烷

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Using a phase equilibrium apparatus, the solubilities of anthracene and carbazole in dimethyformamide, N-methylpyrrolidinone, cyclohexanone, xylene, dichloroethane and tetrachloroethylene were determined and solubility curves were drawn, providing useful data for crude anthracene processing.

利用液固相平衡实验装置,测定了蒽和咔唑在二甲基甲酰胺、N-甲基吡咯烷酮、环己酮、二甲苯、二氯乙烷和四氯乙烯中的溶解度,并作出溶解度曲线,为粗蒽的分离和精制提供了有用数据。

Using pentaerythritol as initiator, boron trifluoride diethyl etherate as catalyst.dichloroethane as dispersion agent, the chloride polyether polyol is synthesized based on the mechanism of cationic ring-opening polymerization of epiclilnrohyclrin.The azide polyether polyol is synthesized, in DMF through A and sodium azide, and the non-reported azide energetic curing agent is synthesized through the adduction of B and IIDI.

以季戊四醇为起始剂,三氟化硼乙醚为催化剂,1,2—二氯乙烷为分散剂,环氧氯丙烷经阳离子开环聚合反应制成氯化聚醚多元醇,A在N,N—二甲基甲酰胺中与叠氮化钠反应制得叠氮聚醚多元醇,B与六亚甲基二异氰酸酯加成反应制得未见文献报道的叠氮固化剂。

In the process of the sulphonate reaction, we use 1,2-dichloroethane as solvent and chlorosulfonic acid as the agent of sulfonation.

环化反应采用1,2-二氯乙烷作溶剂,用氯磺酸作磺化剂,在回流温度下进行磺化反应,3-十二烷基蒽醌磺酸的收率为85.75%。

Diaminoalkanes react with sym - tetrachloroethane to give crystaline 2,2'- Bis -( hexahydropy-rimidine) derivatives 1 - 5, after treatment with aqua ammonia.

利用均四氯乙烷及二氯甲烷的胺化反应,合成了联氢化嘧啶衍生物1~5,4a,8b-反-4,5,8a,9a-四氮杂全氢芴(6)和8b,8c-顺-3a,4a,7a,8a-四氮杂环戊并全氢芴(7)。

Trichloroethane, trichloroethylene or tetrachloromethane is prohibited using.

严禁使用三氯乙烷、三氯乙烯或四氯化碳!

Methyl-trichloro-silane; Trichloro- silane

甲基氯仿见1, 1, 1-三氯乙烷

The thermal property studies indicate that the mass loss of compound B was 54.39% at 242.2~750℃, and when the temperature was 1000℃, there was 25.11% char residue left, which showed that the title compound has a good thermal stability and char forming capability. Using acetonitrile as the solvent instead of trichloromethane or 1, 2-dichloethane gave higher yield. During the synthesis, the yield was very low when triethylamine was used as acid acceptor alone, and when a little amount of 4-dimethylaminopyridine was added at the same time, the yield could be 81%.

结果表明,所合成的化合物B的结构与预期的结构一致;热性能研究表明,化合物B在242.2~750℃质量损失为54.39%,1000℃时仍有25.11%的炭残渣,显示出优异的热稳定性和成炭性;在相同反应条件下,用乙腈作为溶剂的反应产率比使用氯仿和二氯乙烷为溶剂的高,并且在合成过程中,单独使用三乙胺作为缚酸剂时产率很低,而当同时加入少量4-二甲氨基吡啶时,产率可达81%。

Because of its nonpoisonous, DMC can substitute phosgene , dimethyl sulfate or methylating used as methyl pharmaceutical to improve the security of production and reduce the environmental pollution; As the solvent, DMC can substitute fluorine lyons , methyl chloroform , trichloroethylene , benzene , dimethylbenzene, etc.. And it can be used as the paint dope, clean solvent. As gasoline additive, DMC can raise hard octane value and oxygen content and improve its antiknock possibility.

由于DMC无毒,可替代剧毒的光气、硫酸二甲酯等作为甲基化剂或羰基化剂使用,提高生产操作的安全性,降低环境污染;作为溶剂,DMC可替代氟里昂、三氯乙烷、三氯乙烯、苯、二甲苯等用于油漆涂料、清洁溶剂等;作为汽油添加剂,DMC可提高其辛烷值和含氧量,进而提高其抗爆性。

A study has been made on Synthesis of poly with diphenyl ether and terephthaloyl chloride as reactants, 1,2 dichloroethane as solvent, and aluminum chloride as catalyst.

研究了以1,2-二氯乙烷为溶剂,以无水三氯化铝/DMF为复合催化剂体系,在温和条件下,以二苯醚和对苯二甲酰氯为原料合成高分子量聚醚酮酮的方法。

Effects from high-temperature and low-temperature direct chlorination on refining, energy saving and economics of ethylene chloride in chloroethylene production revamping are analyzed.

分析了高温、低温直接氯化技术对氯乙烯改造中二氯乙烷的精制、节能、技术经济等方面的影响。

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