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The results of N/P ratio test show that the removal of nitrogen and phosphorus by immobilized Chlorella is influenced by N/P ratio.

氮磷比试验结果表明,固定化小球藻对氮磷的去除受氮磷比的影响。

Adding N, P could improve cucumber root activity, increased the absorptionof N, P and Mg, decreased that of K; Adding N improved the contents of Ca,Fe, Mn and Zn in leaves, and adding P accelerated absorption of cucumberroot to Fe. Adding K decreased the contents of N, P in leaves, but increased K,Fe content, contents of Ca, Mn and Zn decreased at the same time.4. Adding the rates and ratio of N, P, and K increased the activity of SOD incucumber leaves and root. The changes of POD activity were complex, maybeP played the more important role.

增加氮、磷的用量和配比有利于增强黄瓜的根系活力,促进黄瓜对氮、磷的吸收,减少对钾素的吸收,提高叶片镁含量,增氮提高了叶片中钙、铁、锰和锌的含量;增磷促进了植株对铁的吸收;增钾降低叶片中氮、磷含量,增加植株对钾的吸收,提高了叶片中铁的含量,但钙、锰和锌的含量降低。4。

It also classifies them in accordance with the compound method of triazene reagents as follows: reagents diazotizated with sodium nitrite and muriatic acid, reagents diazotizated with nitrosyl positive ion, reagents diazotizated with n-butyrate nitrite.These reagents with high sensitivity and good choice have been widely applied to the determination of microa mounts of cadmium and...

按三氮烯类试剂合成的方法进行分类,分别为在亚硝酸钠和盐酸作用下重氮化的试剂,在亚硝酰正离子作用下重氮化的试剂,在亚硝酸正丁脂作用下重氮化的试剂,此类试剂灵敏度高,选择性好,广泛应用于被镉、汞等过渡金属离子污染的环境样品的分析中。

The prepared powders were characterized by XRD, UV-Vis, FTIR, N_2 adsorption, Fluorescence spectroscopy, etc. N-doped TiO_2 evidently shows its absorbance shoulder shift into visible light region. Moreover, N-doping retards the transition of TiO_2 from anatase to rutile type as well as restrains the growth of the crystal size which leads to less decrease of surface area. These characteristics are considered to benefit the photoactivity of TiO_2; When all the samples were applied to the photodecomposition of Methylene Blue under visible light(λ>400 nm), the N-doped TiO_2 show an obvious superiority when compared to the undoped TiO_2, the active hydroxyl groups are found to play a important role in this high photoactivity; When the same experiment was performed under UV light, all the samples show the consistent sequence of photoactivity as in the visible light.

通过UV-Vis、XRD、BET、IR、FL等表征手段测试表明:掺氮不仅使TiO_2的光吸收区域拓展到可见光区,而且有利于延缓TiO_2晶相的转换,从而抑止了高温煅烧下所引起的晶粒增大以及比表面积的降低,且氮源浓度越高,此现象越明显,这些特征都有利于催化剂光催化活性的提高;在主波长大于400nm的可见光催化亚甲基蓝实验当中,掺氮TiO_2的光催化活性明显优越于未掺氮样品,亚甲基蓝在90min内达到88%的脱色率。

The optimum hydrolytic conditions of razor clam for neutral protease were : enzyme concentration 2.4%, hydrolysis temperature 50癈, substrate concentration 1:3, pH 7 and reaction time 6 hrs with the degree of hydrolysis and extraction rate of total nitrogen 42.46% and 83.04% respectively; and foracid protease they were: en/yme concentration 6.0%, hydrolysis temperature 50癈, substrate concentration 1:4, pH3.5 and reaction time 5 hrs with the degree of hydrolysis and extraction rate of total nitrogen 46.37% and 87.94% respectively, the hydrolysate being clear light yellow. For the combination of two kinds of proteases they were: first hydrolyzing with 2.6% f 1 avouryme for 3 hrs, then hydrolyzing with 2.4% neutral protease for 3 hrs with the degree of hydrolysis and extraction rtiie of total nitrogen 4-1.57% and 86.95% respectively.

最后综合考虑了水解率、总氮回收率和水解液的色泽、澄清度等指标,得出了较适宜的酶种为单酶以枯草杆菌中性蛋白酶和酸性蛋白酶效果较好,双酶以风味蛋白酶与枯草杆菌中性蛋白酶双酶组合水解效果较好,其适宜的水解工艺条件分别为:枯草杆菌中性蛋白酶加酶量为2.4%,水解温度50℃,料水比1:3,pH值中性条件下水解6h,绕蛙蛋白质的水解率和总氮回收率分别为42.46%和83.04%;酸性蛋白酶水解编蛙肉的适宜的工艺条件为加酶量6.0%、水解温度50℃,料水比l:4,pH值3.5条件下水解sh,水解率为46.37%,总氮回收率为87.94%,水解液呈较清澈的淡黄色;双酶采用先用2.6%风味酶水解3h后,再加入2.4%中性蛋白酶水解3h,水解率达44.57%,总氮回收率为86.95%。

Bacterially triggered CDDS 细菌触发型细菌触发型 CDDS The presence of azo reductase enzymes play pivotal role in the release of drug from azo bond prodrugs while glycosidase activity of the colonic microflora is responsible for liberation of drugs from glycosidic prodrugs.

偶氮还原酶溶解酶的存在在偶氮键药释放过程中发挥关键作用,结肠菌群的糖苷酶活性负偶氮还原酶溶解酶的存在在偶氮键药释放过程中发挥关键作用,结肠菌群的糖苷酶活性负溶解释放过程中发挥关键作用的糖苷酶活性糖苷药物的解放。

The mandarin fish is a piscivorous fish, feeding on other fish species. It is tasty, devoid of fine skeletal spines, and fetches high price. Certain research institutes have tried to stock this fish into lakes with plenty of trash fishes, and the result seems promising.

就水体中氮、磷的负荷而论,只要输出水体的渔获物中氮、磷的含量大大超过输入水体的全部&鱼种&的氮、磷含量加上这些&鱼种&生长代谢过程中所排泄的氮磷总量,那么这种放养对延缓富营养化的进度还有积极意义

A one-step method for the synthesis of aromatic indolizine derivatives byintramolecular 1,5-dipolar cyclization reaction of 2-(2-arylethenyl)pyridinium N-ylidesin the presence of an oxidant has been studied for the first time. In the presence ofelectron-deficient olefins, however, 2-(2-phenylethenyl)pyridinium N-ylides underwent1,3-dipolar cycloadditions and then aromatized in situ by TPCD to produce indolizinederivatives, indicating 1,3-dipolar cycloaddition proceed more readily than 1 ,5-dipolarcyclization in these conditions. Pyridinium disubstituted N-ylides, readily obtainedfrom corresponding pridinium and β-chlorovinyl ketone, underwent thermalintramolecular 1,5-dipolar cyclization to give indolizine derivatives easily.Indolizinecarbaldehyde derivatives were synthesized starting from 2-pyridinecarbaldehyde in four-steps involving 1,3-dipolar cycloaddition reaction.

本文首次研究了2-(2-芳基乙烯基)吡啶N-叶立德在氧化剂存在下的分子内1,5-偶极环化反应,采用一锅法合成了中氮茚衍生物;研究了这些N-叶立德的1,5-偶极环化和1,3-偶极环加成反应的选择性,发现当有缺电子烯烃存在时,优先进行1,3-偶极环加成反应,而不再发生分子内1,5-偶极环化反应;由β-氯乙烯酮方便地得到了烯丙基N-叶立德,他们在加热时进行分子内1,5-偶极环化反应而得到中氮茚衍生物;由2-吡啶甲醛为起始原料,通过1,3-偶极环加成反应等四步反应,得到了重要的中氮茚甲醛衍生物,这些反应都具有条件温和和操作简便的特点,是合成中氮茚衍生物的新方法。

The calculated results show that azido in azides has linear structure , the most optimized CaN6 has linear structure , and the most optimized (CaN6)n (n=2~5) clusters have chain structure of perpendicularity of approximate diamond composed by two azido with two Ca atoms . The middle N atoms of azido show positive, the N atoms at both ends of azido show negative, and the N atoms effected with Ca atoms directly show more negative . There is strong ionic bond between the Ca and N atoms. The IR spectra of the most optimized (CaN6)n (n=1~5) clusters have four vibrational sections , the whole strongest vibrational peak lies in 2195~2280cm-1,and the vibrational mode is anti-symmetric stretching vibration of N-N bonds in azido . Stability analysis show that (CaN6)3 and (CaN6)5 clusters are more stable than other clusters .

结果表明,叠氮化合物中叠氮基以直线型存在,CaN6团簇的最稳定结构为线型结构,(CaN6)n(n=2~5)团簇首先由两个叠氮基与两个Ca原子构成一个近似菱形,再由菱形相互垂直形成链状最稳定结构;叠氮基中间的N原子显示正电性,两端的N原子显示负电性,且与Ca直接作用的N原子负电性更强,金属Ca原子和N原子之间形成很强的离子键;(CaN6)n(n=1~5)团簇最稳定结构的IR光谱分为4个部分,其最强振动峰均位于2195~2280cm-1,振动模式为叠氮基中N-N键的反对称伸缩振动;稳定性分析显示,(CaN6)3和(CaN6)5团簇相对于其他团簇较为稳定。

The results showed:(1)Nitrogen addition changed the soil physical and chemical properties, enhancing the content of NO3—- N available resources in the soil, increasing the plants height and cover, reducing the vegetation light penetration. With increasing of N addition, both the species richness and the diversity decrease sharply (P 0.001).(2)N addition increased the aboveground biomass significantly (P 0.05). With increasing of N addition, the aboveground biomass increased first then decreased, and the grasses biomass increased while the forbs and legumes biomass decreased.(3)There was a significant linear positive relationship between species richness and vegetation light penetration (P 0.05), and also between aboveground biomass and soil NO3—- N content (P 0.05). The relationship between aboveground biomass and species richness was negative upon enhanced N supply.

结果表明:(1)氮素添加提高了土壤中NO3—- N等可利用资源的含量,增加了植物群落植被的盖度,减小了植被的透光率,随着施氮量的增加群落中物种丰富度显著降低(P 0.001);(2)氮素添加显著改变了植物群落地上生产力(P 0.05),随着施氮量的增加地上生产力呈现先增加后降低的变化趋势,各功能群中禾草生物量显著增加,而杂草和豆科生物量随施氮量增加逐渐减少;(3)物种多样性与植被透光率呈线性正相关(P 0.05);地上生产力与土壤NO3—- N含量呈线性正相关(P 0.05);随着施氮量的增加物种丰富度与生产力之间呈负相关关系。

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