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The results indicated that the high level density functional theory calculations can be used to predict the 13C chemical shifts of the modified nanotubes. The calculated results also provided the characteristic chemical shifts values of nitrene (superscript -), carbene (superscript -) and 1,2- and 1, 4-fluorinated nanotubes, which would be helpful for experimental spectrogram assignments. Combined with NMR experiments, these predicted characteristic chemical shifts can be further used to monitor the addition mechanism and the extent of surface modifications on nanotubes.

研究表明高精度的密度泛函理论计算能够用来预测纳米管的13C化学位移,理论研究的结果揭示了氮烯、卡宾以及1,2和1,4氟化的单壁纳米管的若干13C信号特征化学位移值,为实验NMR谱图的归属提供了一定的依据,并且可通过与实验相结合来监测表面官能化碳纳米管加成反应是否发生以及确认其加成方式。

In paper effect of oxygen and carbon action on minority carrier lifetime in thermal process of mc-Si cell and properties of Si_3N_4 film and effects of antirefle-ction and passivation were studied.

为此本文重点研究了多晶硅片在电池制造热工艺中氧碳的行为及其对少子寿命的影响;并研究了氮化硅薄膜的性能及对多晶硅电池的减反射及钝化作用。

If the steel is not killed with aluminum .the Nitrogen content shall not exceed 0.008. warm rolling steel bands for pipes shall be without defects such as foliation inner blisters, nickel fractures cracks or any other defects which can cause break-down corrosion or porosity of pipe walls. the plate or skelp used for PSL 2 pipe shall not contain any repair welds.

如果钢管不是因为铝化断开的话,其实含氮量不应该超过0.008,用于钢管的热轧钢板应无任何如内部水泡面理、镍断口裂痕及其它可引起腐蚀或使管壁多孔化的瑕疵,用于生产 PSL2钢管的金属板或焊接管坯钢不应含有任何修补焊接的痕迹。

The mouse was carried out half nephric duct ligation to induce the renal interstitial fibrosis animal model,afterwards,to set up three groups,control group,sham operation group(intragastric administration with normal sodium according to 10ml/kg weight),treatment group...

采用小鼠单侧输尿管结扎法诱导肾间质纤维化的动物模型,用盐酸青藤碱治疗,并设对照组、假手术组(小鼠每日按10m l/kg体重用生理盐水灌胃,直至治疗结束)、治疗组(选用正清风痛宁缓释片按每日30mg/kg体重给小鼠灌胃,连续3周,),检测血尿素氮、血肌酐、血清层粘连蛋白、纤维连接蛋白的含量,免疫组化法测肾脏组织转化因子β1(TNF-β1)的表达并进行肾脏病理学的观察。

Fourthly, The preparation of 1 -triazolyl-2-isoxazolinyl substituted-ethenes was developed through an one-pot 1, 3-dipolar cycloaddition of NaN_3 and RI,α-alkylation reaction of substituted allyl bromides and 1, 3-dipolar cycloaddition of nitrile oxidesbased on polystyrene-supported propargyl selenide.

四、从聚苯乙烯负载的炔丙基硒醚出发,通过与叠氮化钠和碘化物的一锅法1,3-偶极环加成反应、取代烯丙基溴的α-烷基化反应和腈氧化物的1,3-偶极环加成反应固相合成了1—三唑—2—异噁唑啉取代的-乙烯。

In this study, new benzo[l,2,3]thiadiazole derivatives were designed according to relationship of structure and efficacy. The 9 novel compounds were synsthesized with following reactions. The chlorine atom in 2-chloro-3,5-dinitro-benzoic acid as beginning raw material was substituted by 2-methylpropane-2-thiol, esterified then with bromoethane, reduced by iron powder and cyclized to obtain ethyl benzo[l,2,3]thiadiazole-7 after diazonation reation.

本论文根据苯并噻二唑诱导剂的构效关系设计了新的苯并噻二唑的结构,并合成了9个未见文献报道的化合物,合成步骤如下:采用2-氯-3,5-二硝基苯甲酸为起始原料,苯环上的氯原子被叔丁基硫醇置换,羧酸由溴乙烷酯化,硝基由铁粉还原,随后经重氮化关环生成苯并[1,2,3]噻二唑-7-羧酸乙酯。

Geotrichum candidum was cultured in liquidized WWWSI and saccharificated WWWSI respectively and the varitity of reducing sugar, biomass, the activities of glucoamylase and proteinase,amino-N,pH in the culturing process were studied,The results showed that the Geotrichum candidum grew better and gave high biomass in saccharificated WWWSI .

将白地霉分别培养在液化及液化后再糖化的小麦淀粉废水中,对培养过程中的降糖、生物量、蛋白酶和糖化酶活力、氨态氮、pH值的变化进行了研究。

In this paper boron-doped diamond single crystals was synthesized at high pressure and high temperature with iron-based catalyst doped with B4C, h-BN and Na2B4O7. The effects of multiple boron sources on diamond were studied according to the characterization of structure and properties of the boron-doped diamond.

本文使用碳化硼、六方氮化硼和硼砂三种硼源材料复合添加的铁基触媒在高温高压下合成含硼金刚石,通过对金刚石结构与性能的表征,探讨多种硼源复合添加对含硼金刚石的影响。

To investigate the wear mode of the silicon nitride balls in lapping process, a series of abrasion tests were carried out on a ball-plate wear test apparatus with different loads, abrasive girt diameter, and slurry concentrations.

为掌握不同研磨条件下氮化硅(Si3N4)陶瓷球表面的磨损形式,在球-盘式磨损实验装置上,采用不同载荷及磨料粒度和浓度的碳化硼(B4C)磨料进行了磨损实验。

The results indicated that effect of silicon carbide or sodium silicate on inhibiting crystallization of fused quartz was not obvious,5wt% boric a.

以粒径。16mm的熔融石英颗粒为原料,以硼酸、碳化硅、氮化硅、水玻璃为晶化抑制剂,以聚乙烯醇(浓度1%)为结合剂,试样成型压强为20MPa,试样经1200℃保温2h烧成,对烧后试样进行1500℃保温1h的强化脱玻处理、RT~1300℃的差热分析以及RT-1300℃的热膨胀测定。

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Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书,王祥生,李德昌。安徽省首次发现嗜群血蜱。

Chapter Three: Type classification of DE structure in Sino-Tibetan languages.

第三章汉藏语&的&字结构的类型划分。