氮化法

The resultant was hydrogenised to remove protective group of amino group, then the product was reacted with NaNO2 to give diazonium salt, which was conjugated with salicylic acid, hydroxybenzene, N-salicyloyl glycine acid to get azo derivatives of 4-ASA.

本文首先对4-ASA的氨基和羟基进行了选择性保护，通过氢化还原法选择性脱除氨基的保护基，然后将氢化产物制成重氮盐，通过与水杨酸、苯酚和水杨酰甘氨酸发生反应生成4-ASA的偶氮衍生物，最后在碱性条件下水解得到最终产物。

Methods 60 female sd rats were randomly divided into four groups, namely normal control, pathological, solfasalazine and jckt groups. experimental colitis model in rats were induced by trinitrobenzene sulphonic acid.

雌性 sd 大鼠 60 只，随机分为 4 组，分别为正常对照、模型、柳氮磺胺吡啶及结肠康泰组，以 5% 2，4，6-三硝基苯磺酸诱导大鼠形成结肠炎症，免疫组化法观察 egfr 及 pcna 的表达。

An elastic checking criterion was proposed and carried out to screen out unelastic microbridge samples.

用微机械悬桥法研究低应力氮化硅薄膜的力学性能。

A one-step method for the synthesis of aromatic indolizine derivatives byintramolecular 1,5-dipolar cyclization reaction of 2-(2-arylethenyl)pyridinium N-ylidesin the presence of an oxidant has been studied for the first time. In the presence ofelectron-deficient olefins, however, 2-(2-phenylethenyl)pyridinium N-ylides underwent1,3-dipolar cycloadditions and then aromatized in situ by TPCD to produce indolizinederivatives, indicating 1,3-dipolar cycloaddition proceed more readily than 1 ,5-dipolarcyclization in these conditions. Pyridinium disubstituted N-ylides, readily obtainedfrom corresponding pridinium and β-chlorovinyl ketone, underwent thermalintramolecular 1,5-dipolar cyclization to give indolizine derivatives easily.Indolizinecarbaldehyde derivatives were synthesized starting from 2-pyridinecarbaldehyde in four-steps involving 1,3-dipolar cycloaddition reaction.

本文首次研究了2-(2-芳基乙烯基)吡啶N-叶立德在氧化剂存在下的分子内1，5-偶极环化反应，采用一锅法合成了中氮茚衍生物；研究了这些N-叶立德的1，5-偶极环化和1，3-偶极环加成反应的选择性，发现当有缺电子烯烃存在时，优先进行1，3-偶极环加成反应，而不再发生分子内1，5-偶极环化反应；由β-氯乙烯酮方便地得到了烯丙基N-叶立德，他们在加热时进行分子内1，5-偶极环化反应而得到中氮茚衍生物；由2-吡啶甲醛为起始原料，通过1，3-偶极环加成反应等四步反应，得到了重要的中氮茚甲醛衍生物，这些反应都具有条件温和和操作简便的特点，是合成中氮茚衍生物的新方法。

Methylimidazole in soy sauce was extracted with methylene chloride,diazotized to forms a red colored azo-compound with the highly absorbance at the wave length of 440nm and determined by ultraviolet-visible spectrometry.

酱油样品在层析柱中用二氯甲烷洗脱，经重氮化后在波长440nm处具有最大吸收，据此建立了紫外可见光谱法测定酱油中4-甲基咪唑的方法。

The supported WP catalysts showed considerable activity in HDS reaction of dibenzothiophene and HDN reaction of quinoline. The ibenzothiophene HDS activity and quinoline HDN activity of the spported WP catalysts synthesized by co-impregnation method was better than that synthesized by mixing method. The HDS and HDN activities of 25～30% WP catalysts synthesized by co-impregnation method and reduced at 650～750℃ were better than those of the corresponding sulfurized catalyst.

负载型WP催化剂具有较好的二苯并噻吩加氢脱硫和喹啉加氢脱氮活性，共浸渍法制备的磷化钨催化剂二苯并噻吩加氢脱硫和喹啉加氢脱氮活性要高于混合法制备的磷化钨催化剂。650～750℃还原制备的负载量25～30%的浸渍法磷化钨催化剂具有较高的二苯并噻吩加氢脱硫和喹啉加氢脱氮活性，高于相应的硫化态催化剂。

IT is by far the hardest of all known natural substances (10 on Mohs' scale); only manmade Borazon and synthetic diamond are as hard.

这是目前已知的所有天然物质最难(10月Mohs法大)；只有氮化硼、人造金刚石是人工硬。

GaN with a thickness of 150~200μm was grown by hydride vapor phase epitaxy.

接著利用氢化物气相磊晶法成长150~200μm的氮化镓厚膜。

The influence of deposition, annealing conditions, and etchants on the wet etch rate of plasma enhanced chemical vapor deposition silicon nitride thin film is studied.

本文研究了沉积、退火条件及刻蚀液对等离子体化学气相沉积氮化硅湿法刻蚀速率的影响。

A series of alumina-supported nickel molybdenum nitrides were prepared by temperature programmed reduction successfully.

采用程序升温还原法制备氧化铝载体负载的氮化镍钼。

Finally, according to market conditions and market products this article paper analyzes the trends in the development of camera technology, and designs a color night vision camera.

最后根据市场情况和市面上产品的情况分析了摄像机技术的发展趋势，并设计了一款彩色夜视摄像机。

Only person height weeds and the fierce looks stone idles were there.

只有半人深的荒草和龇牙咧嘴的神像。