氮化法

The extent of nitridation is evaluated by the nitrogen content determined by a LECO Nitrogen/Oxygen determinator.

采用氮/氧分析仪测定产物氮含量，评价氮化反应程度；以BET氮气吸附法测定比表面积，分析粉体活性；以扫描电镜分析样品表面形貌；以热重分析仪测定碳含量，X射线能谱仪估计元素组成。

OBJECTIVE To determine the relative and absolute molecular weight of working reference substance of Grifolafrondosa beta-Glucan and compare the two analysis methods.

目的测定灰树花倍他葡聚糖工作对照品的相对及绝对分子质量，并对两种分析方法进行比较。方法色谱柱为TSK-G4000PW，流动相为0.7%硫酸钠(含0.02%叠氮化钠)或0.2%叠氮化钠溶液，流速为0.5 mL.min-1，柱温为35℃，高效凝胶渗透色谱法用示差折光检测器，高效凝胶渗透色谱和激光光散射联用法用DNDC仪和激光光散射仪联用。

In order to find biologically active urea compounds,seven new N-[5-(3-pyridyl)-1,3,4-thiadiazol-2-yl]-N'- urea derivatives were synthesized by the reaction of 2-amino-5-(3-pyridyl)-1,3,4-thiadiazole with aroylazides,which were prepared starting from carboxylic acids,ethyl chloroformate and sodium azide by one-pot procedure.

为了寻找高生物活性的脲类化合物，通过2-氨基-5-(3-吡啶基)-1，3，4-噻二唑与酰基叠氮化物反应，设计合成了7个新的N-[5-(3-吡啶基)-1，3，4-噻二唑-2-基]-N'-取代苯基脲，其中芳酰基叠氮化物是以芳酸、氯甲酸乙酯、叠氮化钠为起始原料采用&一锅法&所制得。

The primary performances of nitrogen-rich compounds on the gas generant composition of automobile crash airbag system are studies. Based on the closed bomb tests, the P—t curves are obtained and compared with NaN〓. It is shown that the burning velocity of five compounds are higher than that of NaN〓.

研究了富氮化合物作为气体发生剂使用的基础性能，采用密闭爆发器法测出了它们燃烧过程的P-t曲线，并与常用的叠氮化钠类气体发生剂的性能进行了比较，结果表明其中5种药剂的燃烧速度优于叠氮化钠。

The mouse was carried out half nephric duct ligation to induce the renal interstitial fibrosis animal model,afterwards,to set up three groups,control group,sham operation group(intragastric administration with normal sodium according to 10ml/kg weight),treatment group...

采用小鼠单侧输尿管结扎法诱导肾间质纤维化的动物模型，用盐酸青藤碱治疗，并设对照组、假手术组(小鼠每日按10m l/kg体重用生理盐水灌胃，直至治疗结束)、治疗组(选用正清风痛宁缓释片按每日30mg/kg体重给小鼠灌胃，连续3周，)，检测血尿素氮、血肌酐、血清层粘连蛋白、纤维连接蛋白的含量，免疫组化法测肾脏组织转化因子β1(TNF-β1)的表达并进行肾脏病理学的观察。

The formation mechanism of titanium nitride powders by reduction of carbon and nitridation was researched by method of continuous weighing.

用连续称重法研究了钛白粉被活性碳还原氮化合成氮化钛粉末的还原氮化反应机理，并进行了反应的热力学、反应产物的显微结构以及X-ray衍射分析。

In the depth surpasses in 10 meter deep well nitrogenation oven technique of manufacture, applied the multi-link graduation to enter the ammonia active nitrogen atom weaken compensation method, caused the nitrided uniformity distinct enhancement.

在深度超过10米的深井氮化炉制造技术中，应用了多环分级进氨气活性氮原子衰减补偿法，使氮化均匀性明显提高。

The permanent magnets of single-phase exchange coupling Nd 〓N〓 and Nd 〓N〓 with ThMn〓 structure have been prepared by MM and MA process and the following treatments of crystallization、nitrogenation. By means of XRD、SEM、TEM、DTA/DSC and magnetic measurements, the variations of microstructure in each corresponding stage and the related magnetic properties have been studied systematically.

本文采用机械合金化和机械研磨法及随后的晶化、氮化处理分别制备了具有ThMn〓结构的Nd〓N〓单相耦合及Nd〓N〓纳米永磁材料，借助于X射线衍射、扫描电镜、电子探针、透射电镜、差热分析以及磁测量等分析技术系统地研究了上述工艺各阶段对应的组织结构的变化以及它们与磁性能的相互关系。

Said metal nitride is prepared through mixing the aqueous soltuion of nitrate or sulfate of A with the aqueous soltuion of Cr, Mo or W acid or one of their ammonium salts, coprecipitation or impregnation to obtain load-type or non-load-type dual-component metal salt or compound oxide, then pass in NH3, sequentially heating and azotizing at 600-750 deg.C.

该金属氮化物是由含A过渡金属元素的硝酸盐或硫酸盐水溶液与Cr、Mo或W酸或者Cr、Mo或W酸铵水溶液混合，通过共沉淀法或浸渍法制成负载型或非负载型双组元金属盐或复合氧化物，再将双组元金属盐或复合氧化物通NH3进行程序升温，至最终氮化温度600～750℃下进行反应而制得。

In this thesis, we report an investigation of two-wavelength excited photoluminescence on InGaN/GaN multiple quantum wells to study the nonradiative defects.

在这一篇论文之中，我们利用双光源激发的萤光光谱法来研究氮化铟镓/氮化镓多重量子井结构中的非辐射缺陷。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。