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氮化偶氮苯

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In this thesis, we study the photoisomerization dynamics of azobenzene in theexcited state using femtosecond fluorescence up-conversion method.

在这篇论文里,我们介绍利用飞秒萤光上转移方法研究偶氮苯在激发态的的光致顺反异构化动力行为。

3 Recently, we reported an efficient tin-free version of this reaction involving thiophenol for the preparation of cyclopentane derivatives through a 1,5-hydrogen transfer/cyclization sequence [Eq.(1); AIBN=azobisisobutyronitrile].

最近,我们报道了高效的、不使用锡试剂而使用苯硫酚的反应,这个反应是通过1,5-氢转移/环化步骤制备环戊烷衍生物的[化学反应式(1);AIBN=偶氮二异丁腈][4]。

The deoxygenation and reduction of some organic substrates with samarium diiodide were investigated.

本文研究了二碘化钐对一些有机化合物的脱氧反应,以及它在醇存在下对α-卤代酮、偶氮苯和苯醌的还原反应。

A series of azobenzenes with different electron effect substituents were prepared from diazonium salts and benzoguanamine.

将含有不同取代基的芳胺在盐酸介质中进行重氮化反应,制得相应的重氮盐,再与苯代三聚氰胺发生偶合反应,最终得到一系列含有不同取代基的偶氮化合物。

A new spectrophotometric method for the determination of chromium has been developed. In HCl medium, the chromium oxidizes hydroxylammonium chloride to form nitrite, which produces a pink azo dye when reacting with p-aminobenzene sulfonic acid and α-naphthylamine.

基于铬在稀盐酸介质中氧化盐酸羟胺产生亚硝酸根,而亚硝酸根与对氨基苯磺酸重氮化后可与α-萘胺偶联产生粉红色偶氮染料,提出了分光光度法测定铬的新方法。

The adsorbent could efficiently adsorb a vatiety of organic dyes belonging to the triphenylmethane, heteropolyeyclic and azodye groups were used as model compounds.

研究了粉状磺化煤加到Fe3O4结构中制备磁性磺化煤,这种吸附剂能够有效地吸附许多有机化合物,用含三苯甲烷、杂多环和偶氮基等水溶性有机染料进行测定。

In the presence of CPB, the chromogenic reaction of V with DPCO has been studied.

研究在溴化十六烷基吡啶存在下,钒与二苯偶氮羰酰肼显色反应的分析特性。

It is shown that the optimal conditions for the reaction of CADB with SESA are pH 12.0 and m:m=6:1.The product p-aminobenzart sulfanily ethyl CADBwas diazotized and linked with lipase.The optimal pH for lipase linked to diao-compound is 7.5.The link time is at last 12h.

试验结果表明:CADB与SESA反应的最适条件是pH=12.0,SESA与CADB质量比为6:1,反应生成的对氨基苯磺酰乙基交联烯丙基葡聚糖凝胶经重氮化后与脂肪酶偶联的最适条件是pH7.5,偶联时间≥12h。

Second, we discuss two materials which are cinnamoyl chloride and azobenzene. The cinnamoyl chloride can induce the photo-dimerization reaction under linear-polarized UV light. Similarly, azobenzene can induce the cis-trans photoisomerization under UV light.

第二部分采用光诱导配向的方式,将偶氮苯与PI结合,再利用偏极化紫外光曝光使其产生顺-反异构化反应,再用polarized-ATR-FTIR研究其三度空间之分子排列,做为未来显示器配向膜的参考。

A new monomer,4-hexanoxyl-4′-undecylene-[10]-acyloxyazobenzene was synthesized using the main materials:phenol,underlenic acid,1-bromo- n -hexane, p -nitrophenol,thionyl chloride,by the substitution,reduction,couping and diazotization methods.A new polymer was prepared by hydrosilation reaction of poly (methylhy-drosiloxane) with the monomer.

以苯酚、十一烯酸、正溴己烷、对硝基苯酚和二氯亚砜为主要原料,通过取代、还原、重氮化和偶合等反应,合成了一种新的液晶单体 4-己氧基-4′-十一烯-[10]-酰氧基偶氮苯,并与聚通过硅氢加成生成一种新的高分子液晶。

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