氮

Through using Mythylene DinitrAmine as rude product, the knowledge of its reaction properties in different phases have been increased, Through using Mythylene BisAcetAmide as rude product, intermediates which include 1,3-Diacetyl -4,5-dihydroxy -1,3-diazacyclopentane and 1,3-Diacetyl- 4,5-diacetoxy-l,3-diaza cyclopentane have been obtained. 2,4,6,8-tetracetyl- 2,4,6,8-tetraaza bicyclo[3,3,0]octane which can be used to produce Bicyclo-HMX by nitrolysis was also produced. Through using Mythylene BisFormAmide as rude product, intermediates which include 1,3-Diformyl-4,5-dihydroxy- 1,3-diazacyclopentane and 1,3-Diformyl- 4,5-diacetoxy-l,3-diazacyclopentane have been abtained.

以亚甲基二硝胺为初始原料，加深了对亚甲基二硝胺在不同反应相反应特征的认识；以亚甲基二乙酰胺为初始原料，制备了中间体1，3-二乙酰基-4，5-二羟基-1，3-二氮杂环戊烷和1，3-二乙酰基-4，5-二乙酰氧基-1，3-二氮杂环戊烷，最终制备了可被直接硝解为双环HMX的2，4，6，8-四乙酰基-2，4，6，8-四氮杂双环[3，3，0]辛烷；以亚甲基二甲酰胺为初始原料，制备了中间体1，3-二甲酰基-4，5-二羟基-1，3-二氮杂环戊烷和1，3-二甲酰基-4，5-二乙酰氧基-1，3-二氮杂环戊烷。

Irrigation during over-winter promoted significantly N absorption and accumulation, increased N content in the plants at early stage (before 10, April) and final single stem weight, and reduced stem flowering percentage and florets per cyme, leading to an improved quality of rush stem. With the increased level of N application, N content and accumulation in plants, stem flowering percentage and florets per cyme were significantly increased.

越冬期灌水能显著促进植株对氮的吸收和积累，增加前期（10/4前）植株含氮量和收获期单茎干重，显著减少草茎开花率和平均每花序小花数，从而改善草茎品质；随着施氮水平的提高，植株氮吸收和含氮量相应增加，开花率及平均每花序小花数显著提高。

A series of diazonium salts of 4-(N-methyl-N-phenylamino)-3-amino-1,8-naphthalic anhydride 5a, its naphthalimide derivative 5b, and 5e were designed and synthesized,and it was the first time to discover that aromatic radical-induced intramolecular aromatic 1, 5-hydrogen transfer was also involved in the nitrogen-contianed system during Pschorr cyclization.

实验设计合成了4--3-氨基-1，8-萘酐的重氮盐5a、其衍生物N-丁基-4--3-氨基-1，8-萘酰亚胺的重氮盐5b和N--4--3-氨基-1，8-萘酰亚胺的重氮盐5c，并首次发现了通过普朔尔环化反应以氮甲基化的氮为桥原子的体系存在着芳香自由基诱导的芳香1，5-氢转移。

The small size particles produced during ferrovanadium sizing operation are formed into nitrided briquette so as to obtain nitrided ferrovanadium, The effect of ferroalloy size, pressure, nitriding temperature and nitniding time was studied on the nitrogen content of the product.

对高钒铁合金精整过程中产生的细颗粒物料进行压块渗氮，得到氮化钒铁产品，研究了合金粒度、压块压强、渗氮温度、渗氮时间对产品含氮量的影响。

AlN MSM devices were fabricated on AlN epitaxial thin film deposited on GaN/Sapphire substrates using helicon sputtering system at the low temperature of 300°C. The device characteristic was found to be improved by in situ metallization of Al electrodes. The extremely low dark current (1.39pA at 20V), the ideal factor (1.0125) and the Schottky barrier height (0.916eV) are superior compared to those of AlN MSM in the literature. When the device was illuminated by the 150W D2 lamp, the ratio of the induced photocurrent to dark current is more than 2 orders of magnitude. The illumination effect also shows the linear relationship between the radiation power and the photo current for the MSM devices, indicating the potential applicability for deep UV sensors.

氮化铝金属-半导体-金属光侦测器则是用In situ metallization制程，利用低温回旋溅镀法在氮化镓/蓝宝石基板上沉积之氮化铝，再直接溅镀金属铝作为指叉电极，比较目前文献制作出来的氮化铝MSM元件，可得到很好的元件金半接面之理想因子1.0125，算出萧特基能障高度为0.916eV，并有很低的暗电流为1.39 pA，提升了元件的特性，使用150 W氘灯入射，光暗电流差距可到两个order，且元件之光电流与入射光功率呈线性，显示所制作之氮化铝MSM元件，很适合针对深紫外光波段侦测。

In one embodiment, the invention is a system for initiating free radical polymerization comprising: a in one part, one or more amido-borate compounds containing one or more anionic amido-borate moieties comprising an organoborate wherein the boron atom is bonded to a nitrogen atom of ammonia or an organic compound containing one or more nitrogen atoms, such as a hydrocarbyl amine, a hydrocarbyl polyamine, or an aromatic heterocycle containing one or more nitrogen atoms and optionally containing one or more heteroatoms or heteroatom containing functional moieties, and one or more cationic counter ions and b in a second part, a liberating compound which reacts with the nitrogen atom bound to the boron atom upon contact with the amido-borate to form an organoborane radical.

在一个实施方案中，本发明是引发自由基聚合的体系，包括：a在一个部分中，一种或多种含有一个或多个包含有机硼酸根的阴离子酰氨基-硼酸盐部分和一个或多个阳离子抗衡离子的酰氨基-硼酸盐化合物，其中的硼原子键合到氨的氮原子或含一个或多个氮原子的有机化合物，例如烃基胺、烃基聚胺或含一个或多个氮原子和任选含一个或多个杂原子或含杂原子的官能部分的芳族杂环的氮原子上，和b在第二部分中，在与酰氨基-硼酸盐接触时与键合到硼原子上的氮原子反应形成有机硼烷基团的释放化合物。

The results showed that: the influence of the aquaculture process on aquaculture water determined by type of aquaculture; the influence of aquaculture process on the water temperature, salinity and pH value were not wide.the descent of pH value was related to feed coefficients ; the dissolve oxygen of water in outfall was lower than the water in infall,but the concentration still maintained at the saturation level, is mainly affected by density of aquaculture ,rate of feed and artificial measures of increasing oxygen ;the major form of inorganic nitrogen was nitrate-N;the concentration of inorganic nitrogen and the organic matter tended to increase ,but the ammonium to decline ,this was relation with density of aquaculture ,rate of feed and variation of the different inorganic nitrogen form ; concentration of phosphate-P was low in outfall of pond , related with phosphate-P precipitating, as flowing water speed slowly in outfall;This phenomenon that the total number of bacteria and coli form group of water in outfall was lower than the water in infall , this caused by measures of sterilization and disinfection .

结果表明：养殖过程对水体影响与养殖类型有关。养殖过程对水体的水温、盐度和pH影响不大； pH下降与饲料系数高有关；溶解氧含量排水口比进水口低，但仍维持在饱和状态，与养殖密度、投饵率和人工增氧有关。硝酸氮是无机氮的主要存在形式，无机氮和有机物含量有升高趋势，氨氮有下降的趋势，与养殖密度，投饵率和各种无机氮之间的相互转换有关。活性磷酸盐含量在排水口含量下降，与排水口流水速度慢，磷酸盐沉淀有关。生物指标细菌总数和大肠杆菌总数在排水口比进水口低现象普遍存在，这与养殖场杀菌消毒等措施有关。

According to the above study results, especially the steady operation of two-sludge system（2A/O+N 2SBR）, it can be proved that denitrification and excess phosphorus uptake are relatively independent and intersectant biological processes. The overlap is that denitrifying phosphorus removing bacteriawhich possesses the two bacterial metabolisms, could utilize nitrate as an electron acceptor for phosphorus uptake. The two-sludge system can not only combined biological phosphorus removal and denitrification processes to form a process in practical wastwater treatment , but also solved the main difficulties of current single-sludge systems:①the sludge age competition between phosphorus removing bacteria and nitrifier;② the substrate competition between denitrification and dephosphatation.

以上的研究结果，尤其是时间序列的双泥生物反硝化除磷脱氮系统工艺（2A/O+N 2SBR法）的稳定运行，不仅证明了生物脱氮与生物除磷是两个既相对独立又相互交叉的生理过程，其交叉点是同时拥有硝酸盐还原性和超量吸磷这两种生化特性的细菌进行的反硝化吸磷脱氮生化反应，而且双泥系统工艺克服了常规单泥生物脱氮除磷工艺的两大问题（①聚磷菌和硝化菌的SRT相互干扰；②反硝化与生物除磷竞争VFA），同时保证了脱氮和除磷效果，排水指标达到污水综合排水标准（GB8978-1996）的一级标准，具有实际工程使用价值。

The results show that the bud bacilli can oxidate ammonia to nitrous, and when ammonia concentration in wastewater ranges from 25 mg/L to 70 mg/L, ammonia removal amount is direct proportion to ammonia concentration in wastewater and ratio of ammonia removal ranges from 58% to 69%.

结果表明，芽孢杆菌主要进行亚硝化脱氮，在氨氮进水浓度25～70 mg/L范围内，氨氮去除量与进水氨氮浓度成正比，氨氮的去除率稳定在58%～69%。

The results show that the bud bacilli can oxidate ammonia to nitrous, and when ammonia concentration in wastewater ranges from 25 mg/L to 70 mg/L, ammonia removal amount is direct proportion to ammonia conce...

结果表明，芽孢杆菌主要进行亚硝化脱氮，在氨氮进水浓度25～70mg/L范围内，氨氮去除量与进水氨氮浓度成正比，氨氮的去除率稳定在58%～69%。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。