氮

The process of preparing NCAGE included the following steps: alkalization of the treated cellulose; etherification of the alkali cellulose; nitration of the water-soluble cellulose ether; and azidation of nitrocellulose glycidol ether.

利用高压蒸汽闪爆处理后的Novel纤维素为原料，经过碱化、醚化、硝化和叠氮化反应，得到了一种新型高能粘合剂——硝化纤维素叠氮甘油醚，并采用元素分析、DSC、FIT红外光谱和X-射线等对其含氮量、结构和性能进行了分析表征。

Also studied was aza Diels-Alder reaction catalyzed by polyclonal antibody. The bicyclic [2, 2, 2] heptene and the aimed immunogen were synthesized via the key intermolecular asymmetric aza Diels-Alder reaction. Then four polyclonal antibodies were obtained by immunizing rabbit.

在研究多克隆抗体催化氮杂Diels-Alder反应中，通过分子间不对称氮杂Diels—Alder反应为关键反应合成了双环[2，2，2]庚烯类半抗原和目标抗原；用目标抗原免疫动物兔后得到了4株多克隆抗体，经动力学测试表明：多抗Aza-Bsa-3#能催化氮杂Diels—Alder反应的进行。

Good thermal stability and self-extinguishing behavior was observed with the cured polybenzoxazine resins. Second, furan-containing benzoxazine monomers, P-FBz, BPA-FBz, and 4FP-FBz were prepared using furfurylamine as a raw material. Formation of furfurylamine Mannich bridge networks in the polymerizations of P-FBz and BPA-FBz increased the cross-linking densities and thermal stability of the resulting polybenzoxazines. P-FBz and BPA-FBz- based polymers also exhibited high glass transition temperatures above 300℃, high char yields, and low flammability with a limited oxygen index value of 31. The dielectric (Dk3.21–3.39) and mechanical properties (high storage modulus of 3.0–3.9 GPa and low coefficient of thermal expansion of 37.7– 45.4 ppm) of the P-FBz and BPA-FBz-based polymers were superior or comparable to other polybenzoxazines. 4FP-FBz used for polybenzo- xazine modification by means of formation of benzoxazine hybridation with P-FBz.

第二部份以2-呋喃甲胺为起始物，制备了P-FBz、4FP-FBz与BPA-FBz 三个含呋喃官能基之氧代氮代苯并环己烷的单体；BPA-FBz与P-FBz於开环聚合中形成之Mannich bridge网状结构有效地提升聚氧代氮代苯并环己烷聚合物之交联密度与热安定性；Poly与Poly具有大於300℃之玻璃转移温度、高的焦炭生成率与具有31之极限氧指数(Limited oxygen index， LOI)的难燃性特质，Poly与Poly之介电常数(Dk=3.21~3.39)与机械性质[3.0~3.9 GPa的储存模数与37.7~45.4ppm之低热膨胀系数( Low coefficient of thermal expansion， Low CTE)]均较其他聚氧代氮代苯并环己烷为优；4FP-FBz具有低之介电常数(Dk=2.7)，以其作为降低介电常数之反应型改质剂，与P-FBz混成，证实可有效地降低Poly的介电常数。

Amino-6-nitrobenzodifuroxan was prepared through a three-step reaction from starting material 3, 5-dinitrobenzoic acid:(1)3, 5-dinitroaniline (1) was synthesized from the reaction of DNBA and hydrazoic acid in inert solvent 1, 2-dichioroethane through Schmidt rearrangement with yield of 89.6%;(2) 1 was subjected to nitration to prepare pentanitroaniline (2) with yield of 51.1%;(3) The title compound was prepared from 2 and sodium azide in acetic acid through denitrogenation and then Schmidt rearrangement with yield of 86.8%, m.p.204℃～206℃.

以3，5-二硝基苯甲酸为原料经过3步反应合成了7-氨基6-硝基苯并二氧化吠咱：第1步反应，在二氯乙烷惰性溶剂中，DNBA与叠氮酸反应并发生Schmidt重排反应生成3，5-二硝基苯胺(1)，产率89.6%；第2步反应，1在含100%硫酸的硝硫混酸中硝化生成五硝基苯胺(2)，产率51.1%；第3步反应，2与叠氮酸反应，不经分离直接进行热解脱氮、Schmidt重排反应，得到目标化合物， m.p.204℃~ 206℃，产率86.8%。

In order to measure the hardness of a special phase transformed in middle temperature from austenite,some 0 1mm thick pure iron sheets,nitrided at 640℃ and then isothermally treated at 225℃,were prepared for hardness test on the transverse section by using FM 700 micro hardness tester.

为了测定高氮奥氏体特殊的中温转变产物的硬度，用 0 1mm厚的薄片状纯铁试样于 6 4 0℃渗氮，获得高氮奥氏体，随后在 2 2 5℃等温至完全分解。

Under normal circumstances, this is not a problem because food proteins contain only the major components of nitrogen and other major components are not nitrogen, the Kjeldahl method is a very accurate determination of protein content .

在通常情况下，这不是个问题，因为食物中的主要成分只有蛋白质含有氮，其他主要成分都不含氮，因此凯氏定氮法是一种很准确的测定蛋白质含量的方法。

Objective:To compare the measurement methods of nitrogen between different Kjeldahl methods and the modified one.

中华人民共和国药典》(2005年版)所载氮测定法是由Kjeldahl首创，经多次改进，是适用于测定含氮有机物中含氮量的一种方法。

So Kjeldahl method is not actually measured the protein content, but by measuring the content of nitrogen to project protein content, it is clear that if there are other samples contain nitrogen compounds, this approach is not accurate.

所以凯氏定氮法实际上测的不是蛋白质含量，而是通过测氮含量来推算蛋白质含量，显然，如果样品中还有其他化合物含有氮，这个方法就不准确了。

In this assessment, two groups of evaluation factors were used: one group is stipulated in "Environment quality standards for surface water (GB3838-2002)"; the other factors included main pollutants of Jinhe River, such as kjeldahl nitrogen, nitrite nitrogen, nitrate nitrogen and chlorophyll a, and the standards of some of them were given by the author on the basis of relative data.

在此评价中，采用了两组评价因子，一组是地表水环境质量标准(GB3838-2002)内的因子，一组除了标准内的水质因子，还包括了津河的主要污染物凯氏氮、亚硝酸盐氮、硝酸盐氮和叶绿素，这些污染物的标准是经过查阅资料自定的。

The comparative experiments of rearing Penaeus vanname larvae fed the microencapsulated diets and micro-partical diets of "OK" brand and a searies of microgranular diets of "Bonasse" brand was performed. Two brands of diets are respectively formulated with rotifera at percentage of 70%, 80%, 90% and 100%. During the nursery period, the water quality factors such as the concentrations of NH3-Nt, NH3-Nm, NO2-- N, COD and main planktons were tested to find out their change regulation and the influence on survival rates and metamorphic rates of shrimp larvae.

本文利用欧开牌微胶囊饲料、微粒饲料和博尚牌系列微型饲料作为对虾育苗饲料，分别以70％、80％、90％和100％的比例与卤虫活饵料配合来培育凡纳对虾幼体，通过对凡纳对虾幼体有关生长发育指标的对比以及对育苗期间水中总氨氮(NH_3-N_t)、非离子氨氮(NH_3-Nm)、亚硝酸盐氮(NP_2~--N)、化学耗氧量和主要浮游生物等水质因子进行检测，找出它们的变化规律并比较上述饲料对幼体生长发育、成活率、变态率和育苗效果的影响。

In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

。但是，在否定句或疑问句里，这种带有"do"的方法表达的效果却没有什么强调的意思。

Go down on one's knees;kneel down

屈膝跪下。。。下跪祈祷