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Using manganous sulfate solution as precursor, Mn2+ was converted to Mn2 by the addition of ammoni, then Mn2 was oxidized to Mn3O4 with microwave irradiation.The rea-brown Mn3O4 powder was obtained.

论文在微波辅助加热条件下,向净化后的硫酸锰溶液中滴加氨水,使溶液中的Mn2+沉淀为Mn2,利用空气氧化Mn2得到Mn3O4沉淀,过滤,洗涤,干燥后得到棕红色四氧化三锰固体。

First take the administration team group first forIM model making by given ranitidine 0.06g and the 5%hyperhaline typical finemixtured powder with the 50ug/ml MNNG, 0.1%ammonia water,2g sodiumsalicylate added into 100ml 30%alcoholic solution for intragastric administration 6weeks and the nomal control group by given the ordinary feeds and commonwater;After 9 weeks administration,the model groups rats was put to death for modelmaking detection.

从实验第一天起正常对照组给予普通饲料和正常饮水;模型组大鼠则食用含0.06雷尼替丁和5%的高盐的标准粉末状混合饲料,给予含有浓度为50μg/ml的甲基硝基亚硝基胍溶液每日自由饮用,MNNG溶液装入涂有黑漆的避光饮水瓶内,每24 h更换1次药液,每周饮5天,周2和周5则给予浓度0.1%的氨水饮用;同时将2g水杨酸钠放入100ml 30%的酒精溶液中,配置成2%的水杨酸钠和30%的酒精的混合溶液,从第4周起每天早上9点灌胃。

The method comprises the steps that the molybdenum bearing spent catalyst is roasted and comminuted, then the molybdenum bearing spent catalyst is leach and filter by adopting alkaline solution bearing ammonia, ammonium bicarbonate and oxyful, and the secondary roasting and leaching are performed to the solids after filtration, the twice leaching solution is acidified and the aluminum is precipitated out, then is acidified continuously to precipitate out the molybdenum in the form of molybdic acid, the molybdic acid is dissolved by using ammonia water further, the pH value is adjusted again to obtain ammonium molybdate deposition, and the ammonium molybdate product is obtained after dryness.

将含钼废催化剂进行焙烧、粉碎,然后采用含氨、碳酸氢铵和双氧水的碱性溶液浸取并过滤,过滤后的固体物进行二次焙烧和浸取,两次浸取液酸化沉淀出铝,然后继续酸化将钼以钼酸形式沉淀出来,钼酸进一步用氨水溶解,再次调节pH值获得钼酸铵沉淀,干燥后得到钼酸铵产品。

In order to recover Mo and Cu,the acidic from the production process of molybdic ammonium was disposed by DK macropous cation exchange resin,AH compex resin and general cation exchange resin,respectively.Other heavy metals in wastewater were deposited by adding ammonia liquor in the proess.

钼酸铵[分子式为(NH4)2Mo4O13·2H2O或(NH4)6Mo7O24·4H2O]是石油化学工业和高分子合成工业催化剂、陶瓷彩釉和颜料、特殊分析试剂和药物以及生产金属钼丝、片等的重要原料[1],工业上通常采用将精钼砂焙烧、硝酸浸洗、氨水浸出、净化和加酸沉淀等一系列工艺流程。

Then obtain heavy magnesium water solution, add interfacial active agent and ammonia to solution, via hydrothermal treatment and filtration washing, dry to gain nemaline magnesium hydroxide.

得到重镁水溶液,向溶液中加入表面活性剂和氨水,经过水热处理,过滤洗涤后、干燥得到纤维状氢氧化镁。

The peaks intensity of Zr-MCM-41 mesoporous molecular sieves had a tendency to weak and the catalytic activities of them as catalysts in catalizing octadecanol to corresponding octadecanoic acid decreased with addition of zirconium ions.

水热环境下可加速反应物质的迁移运动,氨水缓慢释放OH-离子,促进了TEOS水解、缩聚反应及有机-无机组装过程更好地进行。

In the experiments, some facters such as the proportion of tetraethyl orthosilicate to coupling agents and distilled water to tetraethyl orthosilicate,the concentration of ammonia,reaction time and reaction temperature were controlled.

研究了正硅酸乙酯与偶联剂的比例、水硅比、氨水用量、反应温度与反应时间等因素对包覆效果的影响,其中重点讨论了偶联剂的添加方式对成膜效果的影响。

This investigation was prepared MCM-41 catalyst films on silicon wafer in ammonia media, using tetraethyl orthosilicate as a precursor and cetyltrimethylammonium bromide as a surfactant.

中文摘要本研究以四乙基氧矽溶液为矽酸盐的来源,溴化十六烷基三甲基铵盐为界面活性剂,在氨水的环境下,制备MCM-41触媒薄膜於矽晶片上。

A modified γ-Al〓O〓 was prepared by a special precipitation method with aluminum nitrate solution containing a certain amounts of orthosilicic acid and ammonia aqueous solution. Compared with commercial γ-Al〓O〓, the modified γ-Al〓O〓 was an effecient catalyst for dehydration of tetrahydrofurfuryl alcohol to dihydropyran. The results revealed that the strong acid sites on the surface of the catalyst may play a crucial role in this reaction.

并以硝酸铝和氨水为原料,用沉淀法制备出一种高比表面和拥有较多强酸中心的γ-Al〓O〓,它在四氢糠醇开环脱水制备二氢吡喃的反应中有优良的催化活性,通过比较此γ-Al〓O〓和普通商业γ-Al〓O〓的Py-TPD图,发现强酸中心在制备二氢吡喃的反应中可能具有关键的作用。

Ammonium Copper Quaternary is a novel wood preservative. DDAC, copper sulfate pentahydrate, ammonium hydroxide or ethanolamine were used to synthesize three different kinds of ACQ.

利用二甲基二癸基氯化铵、五水合硫酸铜、氨水或乙醇胺合成3种不同的氨溶烷基铜铵(ACQ,包括A型、B型、D型)。

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