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In the third part of this paper, a facile method is presented for synthesis of malonaldehyde dianil from propargyl alcohol by oxidizing using chromium trioxide and addition reaction with aniline.

对肼基苯磺酸是由对氨基苯磺酸经亚硝酸钠重氮化得到的重氮盐用亚硫酸氢钠还原、水解、硫酸酸化制得,本文经多次实验确定了反应原料、用量及反应条件,得到的产品纯度好,产率高。

We found that under acid condition, selenite radical combined with active hydroxide radical and amino-group of chitooligosaccharides to form chitooligosaccharides - Se compound molecule, the remaining group complex interacted with the negative sodium tripolyphosphate via electrostatical interactation to form nanoparticles with the size about 100nm.

通过透射电镜、粒径分析仪等方法表征,发现壳寡糖-硒纳米颗粒平均粒径为100nm左右,在酸性条件下,亚硒酸根与壳寡糖单元上活性羟基和氨基化合,形成壳寡糖-硒复合分子,剩余的基团与带负电的多聚磷酸钠复凝聚,在4℃下能够稳定保存,25℃以上壳寡糖溶胀而致纳米颗粒发生分解。

The long wave ultraviolet grass green fluorescence function material is synthesized with the p-toluensulfonyl chloride and o-amino benzoic acid as raw materials,pyridine as solvent,and sodium ethoxide as activator.

缑卫军,刘新奇,紫外长波草绿荧光功能材料的合成研究以对甲苯磺酰氯和邻氨基苯甲酸为原料,吡啶为溶剂,乙醇钠为催化剂,合成紫外长波草绿荧光功能材料。

The extremities were titanic, and there was no response to touch stimulations.Our results suggested that Pentobarbital sodium inhibited neuronal firing through GABA_A receptors, therefore the local field potentials and neural firing rates were inhibited; Urethane acted on many kinds of receptors including inhibitory and excitory ones, so the local field potentials did not change significantly; however, because of the multiform receptors on the neurons, the changing of firing rates to different neurons were not the same; Ketamine mainly acted on the NMDA receptors, therefore the local field potentials and neural firing rates were enhanced, and most neural firing rates would be increased.

从这三种麻醉剂的底层作用机制来看,戊巴比妥钠通过作用于GABAA受体对神经细胞发挥抑制性作用,因此表现为场电位和神经元放电的降低;氨基甲酸乙酯同时作用于多种受体通道,既有兴奋性受体,也有抑制性受体,因此,对场电位的影响不大,但对单个神经元来说,每个神经细胞上的受体通道分布差异较大,因此,单个神经元的放电频率变化会有所不同;盐酸氯胺酮主要作用于兴奋性的NMDA受体,故整体场电位活性增加,多数神经元的放电频率也会有所升高。

The key intermediate 3-methylaminopiperidine was synthesized from 3-methylaminopyridine by two methods,formylation and lithium aluminium hydride reduction or condensation with triethyl orthoformate and sodium borohydride reduction,and then hydr...

以3-氨基吡啶为原料,分别通过甲酰化反应、氢化铝锂还原和原甲酸三乙酯缩合、硼氢化钠还原两种方法得到3-甲胺基吡啶,最后经催化氢化得到中间体3-甲胺基哌啶。

The key intermediate 3- methylaminopiperidine was synthesized from 3-methylaminopyridine by two methods, formylation and lithium aluminium hydride reduction or condensation with triethyl orthoformate and sodium borohydride reduction, and then hydrolysis.

以3-氨基吡啶为原料,分别通过甲酰化反应、氢化铝锂还原和原甲酸三乙酯缩合、硼氢化钠还原两种方法得到3-甲胺基吡啶,最后经催化氢化得到中间体3-甲胺基哌啶。

He sample is dissolved in a mixture of nitric acid and potassium chlorate.The determinations of Te,Bi,Fe and Cu are performed on a flame atomic absorption spectrophotometer.The selenium is determined photormetrically with 3,3'-diaminobenzidine,and the sulfur is determined gravimetrically as barium sulfate,precipitated frorm an EDTA-citric acid medium.

辉碲铋矿物经HNO_3-KCIO_3溶解,用火焰原子吸收法或乙二胺四乙酸二钠络合滴定法测定Bi,火焰原子吸收法测定Te、Fe、Cu,3,3'二氨基联苯胺光度法测定Se,硫酸钡重量法测定S。

Results CsA clearly decreased creatinine clearance and increased urinary excretion of N-acetyl-β-D-glucosaminidase in rats as compared with those in the vehicle group. Morphologic changes consisted of vacuolization of tubular cell, expansion of the interstitium and interstitial fibrosis, hyalinization of afferent arterioles. Severity of the injury was related to the dosage of CsA. Striped interstitial fibrosis and arteriolopathy were more severe in the rats treated with CsA and low-salt diet than with CsA and normal diet.

结果 用CsA的大鼠出现尿量增多、内生肌酐清除率下降、尿N-乙酰-β-D-氨基葡萄糖苷酶排泄增多等;病理上表现为不同程度的细胞浊肿、空泡变性及灶性分布的间质纤维化和小动脉病变,随CsA剂量的增加,病变呈加重趋势;结合低钠饮食,CsA慢性肾毒性病变明显加重。

With the increase in CO(NH2)2 concentration,the molecular weight significantly increased,and the best concentration scope of DMAEMA was 0.06%-0.10%.Inaddition,the agents for preventing cross-linking were used to prevent the cross-linking reaction and it content was not allowed too high,and the best concentration scope of sodium acetate(the regulator of molecula weight)was

在此中和度下,AMPS的适宜用量范围为AM的75%~16.25%;AA的适宜用量范围44%~55%;(NH4)2S2O8的适宜用量范围为AM/AA/AMPS总量的0.07%~0.12%;分子量随CO(NH2)2的增加而明显升高;甲基丙烯酸N,N-二甲氨基乙酯的适宜用量范围为0.06 %~0.10%;使用抗交联剂可以解决产品交联造成的难溶问题,但加入量不宜过多,否则分子量会下降;分子量调节剂醋酸钠的用量在1.24 %~1.54%范围内可以使产品的分子量达最佳值。

Paraacetaminophenyl-β-hydroxyethylsulfone can be used as raw material to produce the target product 2-sulfonic-4-(β-sulphatoethyl-sulphone) phenylamine through sulfonationating and hydrolytic reactions.

本文研究了以对乙酰氨基苯基-β-羟乙基砜为原料,经磺化和水解反应,制得产品2-磺酸-4-苯胺的合成工艺,以及2-磺酸-4-乙基砜基硫酸酯苯胺钠盐后处理的最佳操作工艺。

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