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Similarly, 5TPS-AVB〓 or 5-TPS-IVB〓 reacted with carbamino chloride or phosphoryl chloride in IM/DMAP system to produce six new 4"-carbamates or 4"-phosphorylates in good yields.

LA-47与氨基甲酰氯和磷酰氯反应,得到3个对应的5-4-TPS-AVB〓氨基甲酸酯或膦酸酯衍生物,产率良好。

The copolycondensation type polyamic acid was synthesized by using 3,3', 4,4'-Benzophenonetetracarboxylic dianhydride as the dianhydride monomer, 4,4'-Diamino diphenylmethane and 4,4'-Oxydianiline as the diamine monomer under microwave irradiation in Dimethylformamide.

在微波辐射条件下,采用3,3',4,4'-二苯酮四羧酸二酐、4,4'-二氨基二苯甲烷和4,4'-二氨基二苯醚为单体,N,N'-二甲基甲酰胺为溶剂,低温合成一种共缩聚聚酰亚胺的前驱体聚酰胺酸,化学亚胺化脱水环化生成BTDA型共缩聚聚酰亚胺。

The experimental results showed that when AcO-or other anion s were added to a solution consisting of 1,5-(di-benzaldehyde) dithiocarbohydrazone and Hg2+(at a ratio of 1∶2),a hypsochromic shift took place on the maximum ultraviolet absorption peak of the ligand.

设计合成了配体1,5-二双缩二氨基硫脲及其金属配合物,探讨了不同金属阳离子对1,5-二双缩二氨基硫脲紫外吸收光谱的影响,并将标题化合物应用于阴离子识别。

This project mainly exploratorily studied that polyurethane was produced via condensation reaction between polyhydroxylated compounds and methyl carbamate, which was firstly synthesized by dimethyl carbonate and amines. The process is a green route because it turns away the synthesis and the utilization of toxical isocyanic acid ester.

本项目主要探索性地研究了碳酸二甲酯和胺类化合物反应生成氨基甲酸甲酯,然后氨基甲酸甲酯再和多羟基化合物直接反应得到聚氨酯材料,从而避免了异氰酸酯的合成和使用。

Three series of donor-acceptorπ-conjugated molecules 1, 2, and 3 have been designed and synthesized with a N, N-dimethylamino, Julolidine group (2,3,6,7-tetrahydro-1H, 5H-pyrido[3, 2, 1-ij]quinolinyl), or N, N-diphenylamino group as the donor moiety, a phenylvinyl or thienylvinyl unit as the bridge, and a bromide or aldehyde group as the acceptor moiety.

本文设计并合成了1、2、3三个系列的D-π-A型化合物(Donor-Acceptorπ-conjugated compounds),在化合物分子中引入久洛尼啶基团(2,3,6,7-tetrahydro-1H,5H-pyrido-[3,2,1-ij]quinolinyl),N,N-二甲基氨基,或N,N-二苯基氨基为供电子基团,以苯乙烯基或噻吩乙烯基为桥链,以溴原子或醛基为吸电子基团。

In the second section, with ketone and hydroxylamine hydrochloride as the starting materials, 3-aminopropanol is prepared via three steps including reaction of ketone and hydroxylamine hydrochloride , condensation of ketoxime and acrylonitrile, and hydrogenation cracking of condensation product.

第二是3-氨基丙醇的制备,由酮肟丙烯睛缩合物催化氢化裂解制得:即先以酮、盐酸羟胺为起始原料在碱性条件下合成酮肟,再与丙烯腈反应生成酮肟丙烯腈缩合物后经催化氢化裂解制得3-氨基丙醇。

A key intermediate of abacavir, named N-(2-amino-4,6-dichloro-5-pyrimidinyl) formamide was synthesized from diethyl malonate and guanidine hydrochloride. This method suits to industry for large scale. The materials are easy to get and very cheap.

2-氨基-4,6-二氯-5-甲酰氨基嘧啶是合成阿巴卡韦的关键中间体,本文拟以丙二酸二乙酯和盐酸胍为起始原料合成这一关键中间体,具有原料来源广,适合大规模生产等优点。

Amino 5 nitrophenol was synthesized using o aminophenol and urea as raw materials through cyclocondensation ,nitration and alkaline hydrolysis in turn.

以邻氨基苯酚和尿素为原料,对环合、硝化、碱性水解的传统工艺进行改进,合成了 2 氨基 5 硝基苯酚。

The levels of blood glutamate-pyruvate transaminase, glutamic oxalacetic transaminase were measured and compared.

测定各血标本丙氨酸氨基转移酶、门冬氨酸氨基转移酶的变化并予以比较分析。

The yield reached 67.0% The medicinal and pesticidal activities of a part of the compounds have been measured .

在进行氨基酰化时,论文克服了该类嘧啶环上4位氨基在常规条件下不与芳香类和带有强吸电子基如三氯乙酰基酰化试剂发生反应的困难,通过采用在强碱性条件下进行酰化,得以成功。

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