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氨基甲酸酯

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Additionally LC-MS was also used in qualitative analysis of the reactionsystem for the synthesis of dipropyl toluene-2,4-dicarbamate TDC(Pr. The main side-reactions were condensation reactions between 3-amino-4-methyl N-propylphenylcarbamate with TU or toluene 2,4-bisurea.

同样,运用液质联用技术对甲苯-2,4-二氨基甲酸丙酯TDC合成反应进行了定性分析,确定了副产物并推测其主要副反应是中间产物3-氨基-4甲基苯氨基甲酸丙酯与TU和甲苯-2,4-二脲之间的缩合反应。

Two new kind of energy transfer donor-acceptor dyads consisting of α-naphthoic acid moiety and 9-aminoacridine units linked by tetraethylene glycol or triethylene glycol flexible chain have been synthesized.

本工作分别用聚三乙二醇及聚四乙二醇柔性链将α-萘甲酸酯与9-氨基吖啶连接起来,合成了两种新型二元发色团分子体系,在两个体系中,选择激发α-萘甲酸酯,都可以发生从α-萘甲酸酯到9-氨基吖啶的高效率的单重态-单重态能量传递。

Pyrethroids used in mixture with Organophosphates or Carbamates could effectively control insecticide resistance mosquito.

结论当淡色库蚊产生抗药性后,采用有机磷或氨基甲酸酯类杀虫剂与拟除虫菊酯类混用的方法,能取得较好效果。

Methods The sample pro-treatment method was optimized by oscillators and sample concentration instrument, and the carbamates pesticide in vegetable were tested by gas chromatography-mass spectrometry.

方法用振荡器和样品浓缩仪优化样品前提取方法,以气质联用仪分析氨基甲酸酯农药。

The four carbamates were hydrolyzed in alkalescent aqueous solutions, resulting in the formation of 2-sec-butylphenol, 2-isopropylphenol, m-cresol and α-naphthol, which could be determined by amperometry after capillary electrophoretic separation.

用毛细管电泳-安培检测法测得酚类化合物的量,然后分别换算为等当量的氨基甲酸酯类农药的量,从而建立了用毛细管电泳-安培检测法检测所选四种农药残留的方法。

The nano-ionic liquid containing metal complex could be an effective catalyst for oxidative carbonylation of amines to carbamates and disubstituted ureas and for synthesis of unsymmetric ureas from amines and nitrobenzene, in which turn over frequencies exceeded 10000mol/mol/h.

以该系列纳米离子液体为催化剂高效的实现了胺类化合物催化氧化羰化制备氨基甲酸酯和二取代脲(转化频率>10000mol/mol/h)以及胺与硝基苯通过一氧化碳羰化制备不对称脲的过程。

In this test, metabolites and enzyme activities involved in energy metabolism in Cysticercus cellulosae were determined systematicly in vivo and in vitro and under action of drugs.The principles of variation of energy metabolism in Cysticercus cellulosae and mechanism of action of the benzimidazol carbamate drugs were illustrated so as to select an effective drug against immature and mature cysticerci and to provide a theoretical and experimental chemotherapy.

本研究首次系统地测定了体内发育过程中、体外培养条件下及抗囊药物作用下猪囊尾蚴能量代谢的有关物质含量和酶活性的变化,阐明了猪囊尾蚴的能量代谢变化规律和苯并咪唑氨基甲酸酯类药物作用机理,为筛选有效的抗囊药物以及为药物治疗提供了重要的实验和理论依据。

Inhabition of NX0 and NX1 on the activities of fumaric reductase in tissue homogenate of cysticerci was tested. The results showed that the two kinds of benzimidazol carbamate drugs could inhabite the activity of fumaric reductase complex noncompetently.

测试了NX0和NX1对猪囊尾蚴组织匀浆延胡索酸还原酶活性的抑制作用,结果表明两种苯并咪唑氨基甲酸酯类药物非竞争性抑制延胡索酸还原酶复合体活性。

Two carbonyl triruthenium metal clusters were separated with cellulose tris (3, 5-dimethylphenyl-carbamate) as chiral stationary phase. The effects of the optimal conditions were determined according to the effects of the mobile phase composition, the flow rate of the mobile phase and the solvents of the samples etc on the chiral separation of the metal clusters.

应用纤维素三(3, 5-二甲基苯基氨基甲酸酯)手性固定相对2种羰基钌金属簇合物进行了拆分,通过流动相组成、流速和样品溶剂等条件对拆分影响的考察对拆分条件进行了优化。

The cellulose pulp with α-cellulose higher than 90% and polymerisation degree of range of 450~625 was treated with 14%~16% sodium hydroxide solution for 30~40 min under temperature of 40~50°C, and blended with urea in the ratio of 1:2~3. The product was reacted in xylene as solvent at 137°C for 2~3 h.

指出:选用聚合度为450~625、α-纤维素含量大于90%的纤维素桨粕,用14%~16%的氢氧化钠溶液,于40~50℃条件下活化处理30~40min后,与尿素以1:2~3的比例混合,在137℃的二甲苯体系中反应2~3h,便可得到含氮量为2.4%~3.5%的纤维素氨基甲酸酯产物。

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