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With the occurrence of H2/Pd-C and ethyl formic ester,the reduction of the nitro group and the formylation of the amino group could be finished in one step.

但是在甲酸乙酯存在下,用H2/Pd-C对Ⅶ的硝基进行还原,得到的Ⅷ中的氨基可当即被甲酰化,使由Ⅶ到Ⅳ的两步反应一步完成。

Moreover, the effects of the molar ratios of the reagents on the yield are examined. The best molar ratios are a 2.0 molar equivalence of thionyl chloride and a 3.0 molar equivalence of paminophenol to retinoic acid, and the total yield is 80.7%.

此外,研究了反应试剂的摩尔比对反应收率的影响,最佳摩尔比为二氯亚砜和对氨基苯酚物质的量分别是维甲酸物质的量的2倍和3倍,总收率为80.7%。

Part two: Using chloroformic ester reacted with potassuim thiocyanate to get thiocyanic esters. Then reacted with biological substituted pyrimidinamine to synthesize forty two thiourea compounds, thirty eight of them are new compounds. Their structures have been charactered by IR, 1H NMR and elemental analysis.

第二部分:先以氯甲酸酯和硫氰酸钾为原料合成异硫氰酸酯,再与有生物活性的取代氨基嘧啶反应,合成了一系列新的取代嘧啶基硫脲类化合物,合成的42个化合物中有38个为首次合成的新化合物,结构经元素分析、IR及~1H NMR得到确证。

Aim To study the relationship between the structures of a series of 4,4-diaryl-3-butenyl derivatives of nipecotic acid and guvacine and their inhibition activity of the γ-aminobutyric aciduptake.

目的研究3-哌啶甲酸和四氢烟酸的4,4-二芳基-3-丁烯衍生物结构和对γ-氨基丁酸摄取抑制活性之间的关系。

The effects of imidization method,coagulation bath and temperature were studied on the structure and separation performance of polyimide membrane,prepared by using pyromellitic dianhidride and 4,4′-oxydianiline as raw materials.

针对以均苯四甲酸二酐和4, 4′-二氨基二苯醚为原料合成聚酰亚胺的过程,研究了亚胺化方法、凝胶浴组成与温度等条件对膜的结构和分离性能的影响。

A high temperature resistant polyimide adhesive agent was synthesized by pyromellitic dianhydride and 4,4-diamino diphenyl ether in order for the self-adhesion of aero dynamo magnetic steel plates.

为解决国内无法生产航空电机用自粘磁钢片的难题,用均苯四甲酸二酐和二氨基二苯醚合成一种耐高温聚酰亚胺粘合剂,配合相应的处理工艺,制成一种耐250℃的自粘性磁钢片,成功应用于航空、航天等高科技领域。

A silver ion selective electrode was prepared and characterized with trimethylene bis (N-ethyl-N-phenyldithiocarbamate) as ionophore.

制备并考察了以双(N-乙基-N-苯基氨基二硫代甲酸)1,3-丙二醇酯为载体的银离子选择电极的性能。

The good results can be obtained with the newalgorithm; the local minimal can be avoided in some degree. In this paper, neural networks also were applied to quantitativestructure-property relationships analysis:1Studies on the toxicity of aniline, nitrobenzene and phenol derivatives and their structures.2 Studies on HEPT compounds for their anti-aids.3 Studies on nitrogen mustards and 2-formylpyridine thiosemicarbazone compounds for their anti-cancer.4 Studies on phenol and aniline derivatives for their gas chromatographic retention values.5 Studies on discrimination of tea by Self-organizing feature map network.

本论文还利用上述方法进行了一些定量结构活性相关性研究,主要内容: 1环境中有毒有害有机物的定量结构活性相关性研究。2抗艾滋病类药物定量结构活性相关性研究。3抗肿瘤类药物(氮芥子气类化合物和2-甲酸吡啶缩氨基硫脲类化合物)定量结构活性相关性研究。4苯酚和苯胺类衍生物色谱比移值预测。5将神经网络用于茶叶的分类。

Three composites of the different fibers with epoxy resin matrix are prepared and the corresponding unilateral fiber reinforced winding ring specimens are fabricated. The mechanical poperties of the composites including tensile strength, modulus and three point interlaminar shear strength are tested.

据文献 [2 ]介绍,PBO(聚对亚苯基苯并双口恶唑)是含杂环的苯氮聚合物的一种,它是采用二氨基间苯二酚和对苯二甲酸在多磷酸中聚合、采用空气间隙湿法纺丝法进行纺丝而制得的。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口,替代木托盘,免薰蒸,符合欧盟、北美各国对出口货物包装材料的法令要求;喷涂钢托盘适用于重载上货架之用,托盘表面根据需要制作成平板状、波纹状及间隔形式,满足不同的使用要求。

A single payment file can be uploaded from an ERP system to effect all pan-China RMB payments and overseas payments in all currencies.

付款指令文件可从您的 ERP 系统上传到我们的电子银行系统来只是国内及对海外各种币种付款。