氨基甲酸乙酯

Two new kind of energy transfer donor-acceptor dyads consisting of α-naphthoic acid moiety and 9-aminoacridine units linked by tetraethylene glycol or triethylene glycol flexible chain have been synthesized.

本工作分别用聚三乙二醇及聚四乙二醇柔性链将α-萘甲酸酯与9-氨基吖啶连接起来，合成了两种新型二元发色团分子体系，在两个体系中，选择激发α-萘甲酸酯，都可以发生从α-萘甲酸酯到9-氨基吖啶的高效率的单重态-单重态能量传递。

For the determination of five carbamate pesticide residues by high performance liquid chromatography with gel permeation chromatography purification, sample was extracted with acetonitrile and purified with gel permeation chromatography. Methanol-water was used as the mobile phase by gradient elution, flow rate of 1.0mL/min, using a fluorescence detector and quantitating with external standard method.

凝胶渗透色谱-液相色谱法测定5种氨基甲酸酯类农药残留中，实验采用乙腈提取，凝胶渗透色谱柱对样品进行净化，以甲醇-水为流动相，进行梯度洗脱，流速1.0mL／min，荧光检测器检测，外标定量测定。

Methods The amino acids in the injections were pretreated with 6-aminoquinolyl-N-hydroxysuccinimdyl separately and their derivatives were analyzed on Waters 2695 HPLC using AccQ-Tag column. Gradient eluents consisted of sodium acetate solution (pH 4.95), acetonitrile and water. The Detection wavelength was 248 nm and column temperature 37℃.

采用AccQ-Tag法，以6-氨基喹啉－N-羟基琥珀酰亚胺基甲酸酯为衍生试剂，与复方氨基酸注射液(18AA-V)中17种氨基酸柱前衍生，用Waters 2695 HPLC仪器，AccQ-Tag柱，以醋酸钠(pH 4.95)缓冲液为流动相A，乙腈为流动相B，水为流动相C进行梯度洗脱，检测波长为248 nm，柱温为37℃，进样量为5μL。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。