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氨基甲酸乙酯

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Urethane adduct was synthesized from decarboxylated cashew nut shell liquid,hexamethylenediisocynate and polyethylglycol,which was then reacted with melamineformaldehyde resin to form aqueous coating material.

采用天然植物油、己二异氰酸酯和聚乙二醇在较温和的条件下反应,制得了水溶性的氨基甲酸酯加成物,以此和低醚化度甲醚化三聚氰氨甲醚甲醛树脂制备了水性涂料。

Clinicians should be able to recognize and treat significant toxidromes resulting from acetaminophen; anticholinergic agents including antihistamines and psychoactive drugs; anticoagulants such as warfarin or rat poison; cardiac medications including calcium channel blockers, beta-blockers, and digoxin; muscarinic cholinergic agents including carbamates, some mushrooms, and organophosphates; nicotinic cholinergic agents such as insecticides and nicotine; cyanide; ethylene glycol or methanol from antifreeze or rubbing alcohol; iron-containing products such as deferoxamine; opioids such as morphine, hydrocodone, or methadone; salicylate (aspirin-containing products); sulfonylurea; and sympathomimetic agents such as amphetamines, caffeine, cocaine, or ephedrine.

医师必须可以辨识与治疗乙醯胺酚;抗胆碱剂,如抗组织胺与精神作用药物;抗凝血剂,如warfarin或杀鼠剂;钙离子阻断剂、乙型阻断剂、毛地黄等心脏药物;蕈毒胆碱剂,如氨基甲酸酯盐、某些有毒蘑菇、有机磷农药;菸碱性胆碱剂,如杀虫剂与尼古丁;氰化物;抗冻剂或外用酒精的乙二醇或者甲醇;含铁产品,如 deferoxamine;鸦片类,如吗啡、hydrocodone、美沙冬;水阳酸;硫醯基尿素类降血糖药;拟交感神经药物,如安非他命、咖啡因、古柯碱或麻黄素等造成的明显中毒症候群。

The target compound was synthesized from clarithromycin via hydrolyzation,acetylation,cyclic carbonatation,oxidation,decarbonatation,acylation,cyclic carbamatation and cyclization.

方法以克拉霉素为起始原料,经水解、乙酰化、环碳酸酯化、氧化、脱碳酸酯化、酰化、环氨基甲酸酯化和环合等反应合成目标化合物。

N-Carbobenzoxy-L-homoserinelactone was prepared via N-alkylation reaction of L-methionine and iodoacetamide with benzyl chloroformate as amino protecting agent.

以L-蛋氨酸为原料,氯甲酸苄酯为氨基保护试剂,与碘乙酰胺(I2微量)内酯化反应,合成N-苄氧羰基-L-高丝氨酸内酯。

Omeprazole racemate was resolved respectively by simulated moving bed chromatography and batch chromatography with the coated cellulose triphenylcarbamate as chiral stationary phase and ethanol containing 0.1% diethylamine as mobile phase.

用纤维素三苯基氨基甲酸酯涂敷型手性固定相和含0.1%二乙胺的乙醇溶液,研究了模拟移动床色谱和间歇色谱对奥美拉唑对映体的拆分。

The key intermediate 3-methylaminopiperidine was synthesized from 3-methylaminopyridine by two methods,formylation and lithium aluminium hydride reduction or condensation with triethyl orthoformate and sodium borohydride reduction,and then hydr...

以3-氨基吡啶为原料,分别通过甲酰化反应、氢化铝锂还原和原甲酸三乙酯缩合、硼氢化钠还原两种方法得到3-甲胺基吡啶,最后经催化氢化得到中间体3-甲胺基哌啶。

The key intermediate 3- methylaminopiperidine was synthesized from 3-methylaminopyridine by two methods, formylation and lithium aluminium hydride reduction or condensation with triethyl orthoformate and sodium borohydride reduction, and then hydrolysis.

以3-氨基吡啶为原料,分别通过甲酰化反应、氢化铝锂还原和原甲酸三乙酯缩合、硼氢化钠还原两种方法得到3-甲胺基吡啶,最后经催化氢化得到中间体3-甲胺基哌啶。

Polyimide/silica (PI/SiO2) nano-hybrid films of different solid content were prepared based on pyromellitic dianhydride and 4, 4'-oxydianiline using tetraethoxysilane as the inorganic precursors.

以均苯四甲酸二酐和4,4'-二氨基二苯醚为有机单体,正硅酸乙酯为无机前驱体,制备了SiO2含量一定,PAA杂化胶液固体含量不同的PI/SiO2纳米杂化薄膜。

The determination of amino acids in blood clam antianaemia oral liquid using HPLC-AccQ-Tag method is reported. The oral liquid reacted with 6-aminoquinolyl-N-hydroxysuccini-mdyl carbamate. Then, the corresponding derivatives were analyzed with an HPLC. The chromatographic conditions were AccQ-TagTM C18 column for amino acids analysis (3.9mm×15cm); mobile phase of program elution sodium acetate solution(pH5.02), acetonitrile, Milli-Q water. The amino acids'AQC deriatives were detected at 248nm with a UV-detector. Eighteen kinds of amino acids were completely determined in 35 minutes.

以6-氨基喹啉-N-羟基琥珀酰亚胺基氨基甲酸酯为衍生剂,与毛蚶抗贫血口服液中的氨基酸柱前定量衍生,用WatersHPLC仪,AccQ-TagTM专用C18柱(3.9mm×15cm),以140mmol·L-1的醋酸钠溶液(pH5.02)为溶剂A,乙腈为溶剂B,超纯水为溶剂C,进行梯度洗脱,检测波长为248nm,35min测试完毕。

Methyl-l, 3-oxazine-2,4-dione are prepared from ethyl acetoacetate and ethyl carbamate at 140 for 6h, catalysted by zinc acetate, giving to 48.8% yields which is 33% more than the literature value.

选用醋酸锌作催化剂,使乙酰乙酸乙酯与氨基甲酸酯在140℃反应6h,合成6-甲基-1,3-噁嗪-2,4-二酮,产率达48.8%,较文献报道值高出了33%。

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