氨基甲酸乙酯

With the occurrence of H2/Pd-C and ethyl formic ester,the reduction of the nitro group and the formylation of the amino group could be finished in one step.

但是在甲酸乙酯存在下，用H2/Pd-C对Ⅶ的硝基进行还原，得到的Ⅷ中的氨基可当即被甲酰化，使由Ⅶ到Ⅳ的两步反应一步完成。

Two kinds of ashless and non-phosphorus additives, hydroxyl-containing dithiocarbamate derivatives were prepared.

合成了2-乙羟基-吗啡啉二硫代氨基甲酸酯和2-乙羟基-二正丁胺基二硫代氨基甲酸酯两种添加剂。

In order to find biologically active urea compounds,seven new N-[5-(3-pyridyl)-1,3,4-thiadiazol-2-yl]-N'- urea derivatives were synthesized by the reaction of 2-amino-5-(3-pyridyl)-1,3,4-thiadiazole with aroylazides,which were prepared starting from carboxylic acids,ethyl chloroformate and sodium azide by one-pot procedure.

为了寻找高生物活性的脲类化合物，通过2-氨基-5-(3-吡啶基)-1，3，4-噻二唑与酰基叠氮化物反应，设计合成了7个新的N-[5-(3-吡啶基)-1，3，4-噻二唑-2-基]-N'-取代苯基脲，其中芳酰基叠氮化物是以芳酸、氯甲酸乙酯、叠氮化钠为起始原料采用&一锅法&所制得。

METHODS 5-amino-1-hydroxyethyl pyrazole-4-carboylic acid was synthesized through condensation of ethyl cyanoacetate and triethyl orthoformate followed by one-pot methodology of cyclization,hydolysis.

方法原甲酸三乙酯与氰乙酸乙酯缩合，然后和羟乙基肼经环合、水解等一锅法合成5-氨基吡唑-4-甲酸，然后在亚硫酸钠存在条件下加热脱羧得到5-氨基-1-羟乙基吡唑。

Bezaldehyde was used as protective agent in first method.S-Epichloeohydrin was aminated and acidulated to give(2S)-1-Amino-3-chloro-propanol Salts.The acetylation of (2S)-1-Amino-3-chloro-propanol by acetic anhydride produced the intermediate-N-[2--3-chloropropyl]acetamide.And then at 20℃,in the presence of lithium tert-butoxide,benzyl 3-fluoro-4-morpholinophenyl carbamate react with-N-[2--3-chloropropyl]acetamide to give linezolid in total yield of 43.6%.

路线一采用苯甲醛作保护剂，使S-环氧氯丙烷氨解、酸化生成S-1-氨基-3-氯-2-丙醇盐酸盐，然后经乙酰化反应后，生成中间体-N-[2-乙酰氧基-3-氯丙基]乙酰胺，再用N-(3-氟-4-吗啉苯基)氨基甲酸苄酯和中间体在催化剂叔丁醇锂存在下25℃反应生成利奈唑酮，总产率达到43.6%。

Structures of glycosyl ester of 13-cis-4-restinoic acid(5) and 6 were characterized by 1H NMR,13C NMR,IR and MS and confirmed to be β-configuration.

13-顺维甲酸与溴代-2，3，4，6-四-O-乙酰基-α-D-吡喃葡萄糖在4-二甲氨基吡啶催化下合成了13-顺维甲酸葡萄糖酯(5)，以二氧化锰为氧化剂，5经氧化成功地合成了新化合物13-顺-4-羰基维甲酸葡萄糖酯(6)。

Ethyl carbamate,a known genotoxic compound,is mainly found as a natural trace constituent in wine and other alcoholic beverages.

氨基甲酸乙酯(Ethyl Carbamate，EC)是一种基因致癌物，葡萄酒及其它酒精饮料中含有微量的EC。

METHODS: Rats in each group were anesthetized with intraperitoneal injection of ethyl carbamate at dosage of 1mg/kg; then in intestinal IR group and shenfu injection group rats' superior mesenteric artery was occluded with vascular clamp for 1 hour before 2-hour reperfusion,which was not conducted in blank control group.

各组大鼠给予氨基甲酸乙酯1 mg/kg腹腔注射麻醉，肠缺血再灌注组和参附注射液组用血管钳夹闭肠系膜上动脉1 h然后再灌注2 h，空白对照组不用血管钳夹闭肠系膜上动脉。

In metabolizing argine, there had no obvious difference among three strains and the control 3 1 DH. Thus, three selected strains had better characters of degrading argininc that they couldn"t over-degrade arginine to produce large numbers" precursors of carcinogenic ethyl carbamate as citrulline, etc.

分析表明，精氨酸分解代谢方面，三个菌株与对照31DH没有明显差异，由此说明，三个优选菌株精氨酸代谢特性良好，不会过多降解精氨酸、代谢产生瓜氨酸等前体物质，从而不会导致致癌物质——氨基甲酸乙酯的大量合成。

It's a quick-drying, zinc phosphate primer, based on long oil alkyd resin and urethane alkyd resin.

长油醇酸树脂和氨基甲酸乙酯醇酸树脂配制而成的快干磷酸锌底漆。

What would he tell Judith and the children?

他将怎样告诉朱迪丝和孩子们呢？

I this is at that time, the opinion with peacockish true girl is full of in a heart.

这就是当时的我，一个心中布满虚荣的女孩子真实的想法。