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Omeprazole racemate was resolved respectively by simulated moving bed chromatography and batch chromatography with the coated cellulose triphenylcarbamate as chiral stationary phase and ethanol containing 0.1% diethylamine as mobile phase.

用纤维素三苯基氨基甲酸酯涂敷型手性固定相和含0.1%二乙胺的乙醇溶液,研究了模拟移动床色谱和间歇色谱对奥美拉唑对映体的拆分。

A method for the preparation of microcellular elastomeric polyurethane foams from a reaction mixture comprising a polyisocyanate component containing at least 85% by weight of 4,4'-diphenylmethane diisocyanate or a variant thereof, a polyol composition comprising at least one polyoxyalkylene polyol having an average nominal hydroxyl functionality of from 2 to 6, an average hydroxyl equivalent weight of at least 1300 and an average oxyethylene content of between 50 and 85% by weight, water, a chain extender having an average hydroxyl equivalent weight of from 15 to 250 and optionally a crosslinking agent, the hardblock-content being more than 45% by weight.

本发明是有关一种制备微孔弹性聚氨基甲酸酯泡沫体的方法,其反应混合物包括:一种含至少85重量%的4,4′-二苯甲烷二异氰酸酯或其变体的聚异氰酸酯组分,一种多元醇组合物,其包含至少一种平均标称羟基官能度从2至6、平均羟基当量至少1300且平均氧乙烯含量介于50至85重量%之间的聚氧亚烷基多元醇,水,一种平均羟基当量为15至250之增链剂,以及视需要使用的交联剂,该硬性嵌段-含量(hardblock-content)大于45重量%。

The isocyanate-terminated polyurethane prepolymer was also synthesized form polytetramethylene glycol and 4,4'-diphenylmethane diisocyanate in N,N-Dimethylformamide.

另外,将聚醚双醇与量之4,4'-二苯甲基二异氰酸酯行预聚合反应,形成具-NCO末端基之聚氨基甲酸酯预聚合体。

In this article, we have been investigated that synthesizing and properties of shape memory polyurethane. The shape memory polyurethane was synthesized from PCL diol, MDI(4, 4'-diphenylmethane diisocyanate) and BDO (1,4-butanediol) in this experiment. We analyzed that the effect of differential mole ratio of monomers to synthesized SMPU. Besides, the various concentrations of Nano-silver were mixed with SMPU. Mechanical properties and shape memory behavior of SMPU nanocomposite films were investigated.

本研究目的为藉由改变4,4'-二苯甲基二异氰酸盐(4,4'-diphenylmethane diisocyanate, MDI)/聚己内酯二元醇(polycaprolactone diol, PCL diol)/1,4-丁二醇(1,4-butanediol, BDO)等不同莫耳比制备形状记忆型聚氨基甲酸酯(Shape Memory Polyurethane, SMPU);并探讨改变不同单体莫耳比及添加不同浓度奈米银溶液对其物性及形状记忆性的影响。

N,N- bisdithiocarbamate nickel have been synthesized in good yield by electrochemical oxidation of sacrificial anodes in one - chamber cell with a mixture of carbon disulphide plus dibutylamine.

烷基硫代氨基甲酸类及其与金属离子的配合物一直是无机化学中研究的热点领域之一1工】,该类物质可作为液一液萃取剂且具有一些药物的功能。

The extremities were titanic, and there was no response to touch stimulations.Our results suggested that Pentobarbital sodium inhibited neuronal firing through GABA_A receptors, therefore the local field potentials and neural firing rates were inhibited; Urethane acted on many kinds of receptors including inhibitory and excitory ones, so the local field potentials did not change significantly; however, because of the multiform receptors on the neurons, the changing of firing rates to different neurons were not the same; Ketamine mainly acted on the NMDA receptors, therefore the local field potentials and neural firing rates were enhanced, and most neural firing rates would be increased.

从这三种麻醉剂的底层作用机制来看,戊巴比妥钠通过作用于GABAA受体对神经细胞发挥抑制性作用,因此表现为场电位和神经元放电的降低;氨基甲酸乙酯同时作用于多种受体通道,既有兴奋性受体,也有抑制性受体,因此,对场电位的影响不大,但对单个神经元来说,每个神经细胞上的受体通道分布差异较大,因此,单个神经元的放电频率变化会有所不同;盐酸氯胺酮主要作用于兴奋性的NMDA受体,故整体场电位活性增加,多数神经元的放电频率也会有所升高。

Spontaneous discharges of the rostral ventrolateral medulla neurons were extracellularly recorded by multi-barrelled microelectrodes in urethane-anesthetized rats.

实验用多管微电极细胞外记录氨基甲酸乙酯麻醉的SD大鼠延髓头端腹外侧区神经元的活动。

The unit discharge of auditory neuron in the cortical AⅠ area was recorded with the extracellularly recording method. The character of ON-OFF responses induced by short pure tone and the influence of stimulating lateral amygdaloid nucleus on these responses and the tuning curves of the recorded neurons were examined.

在30只氨基甲酸乙酯麻醉的SD大鼠上记录神经元单位放电,观察短纯音诱发的皮层AⅠ区神经元ON-OFF反应的特性及电刺激杏仁外侧核(lateral amygdaloid nucleus, LA)对ON-OFF反应以及调谐曲线的影响。

The effects of electrical and chemical stimulation of the vertral medial area of nucleus facialis on the myoelectric activities of genioglossus were observed in 26 urethane-anaesthetized and vagotomized rabbits.

本研究在26只氨基甲酸乙酯麻醉、断双侧迷走神经的健康成年家兔上观察了电、化学刺激面神经核腹内侧区对颏舌肌肌电活动的影响。

Effects of electrical and chemical stimulation of the dorsal and ventral medial area of nucleus facialis on myoelectric activities of genioglossus and phrenic muscle were observed in 44 urethane-anaesthetized and vagotomized rabbits.

在44只氨基甲酸乙酯麻醉、断双侧迷走神经的健康成年家兔上,观察电、化学刺激面神经核背内侧区和腹内侧区对颏舌肌和膈肌肌电活动的影响。

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