氨基化

In order to provide some scientific data for judging biological toxicity and bioavailability caused by heavy metals in sediments in Guilin, China, for the first time, the authors sampled sediments in different water areas in Guilin, and determined AVS by P-Amino dimethyl aniline dihydro chloride photometry through a set of acidification-ventilation-absorption AVS reaction unit, determined copper, lead, zinc, cadmium and nickel with tomic absorption spectrophotometry, mercury and arsenium with atomic fluorescence, and cipangopaludina cathayensis was selected as the tested species for bioavailability experiment.

首次以桂林水系沉积物为研究对象，通过酸化－吹气－吸收装置，用对氨基二甲基苯胺光度法测定沉积物中AVS含量，用原子吸收分光光度法测定SEM和间隙水中Cu、Pb、Zn、Cd、Ni含量，用原子荧光法测定Hg、As含量。

The synthesis of l-(4-acetylaminophenyl)-2-bromo-1-propanone was discussed, and the mechanism and possible factors were analyzed. Hence the routine was determined, in which l-(4-acetylaminophenyl)- 1-propanone was reacted with Bromine dissolved in ethanol, so that the a -bromination can be carried on, resulted in the yield of up to 70.4%.

探讨了1-(4-乙酰胺基苯基)-2-溴代-1-丙酮的合成方法，分析了反应机理和影响因素，确定将1-(4-乙酰氨基苯基)-1-丙酮溶解在乙醇中以溴的乙醇溶液进行α-溴化的合成路线，产率可达70.4％。

Universal indicator paper,special indicator paper,ammonium fluoride,ammonium hydrogen difluoride,nbenzyldimethylamine,disinfectant paper,nacetylphenylhydrazine,mcresol purple,bromocresol green,fluorescein,eosin Y,ninhydrin,phenedons,potassium phthalate,pamimobenzene sulphonic acid anhydrous.

广泛试纸，精密试纸，氟化铵，氟化氢铵，N苄基二甲胺，消毒试纸，N乙酰苯肼，间甲酚紫，溴甲酚绿，荧光素，曙红Y，水合茚三酮，菲尼酮S，苯甲酸氢钾，无水对氨基苯磺酸。

We also studied the enantioselective conjugate addition of chalcone in the presents of chiral Ni2 aminoalcohol complexes.

我们还研究了手性氨基醇配体/镍盐催化的a，β-不饱和酮的不对称迈克尔加成反应，以及酰腙的不对称烯丙基化反应。

In order to find biologically active urea compounds,seven new N-[5-(3-pyridyl)-1,3,4-thiadiazol-2-yl]-N'- urea derivatives were synthesized by the reaction of 2-amino-5-(3-pyridyl)-1,3,4-thiadiazole with aroylazides,which were prepared starting from carboxylic acids,ethyl chloroformate and sodium azide by one-pot procedure.

为了寻找高生物活性的脲类化合物，通过2-氨基-5-(3-吡啶基)-1，3，4-噻二唑与酰基叠氮化物反应，设计合成了7个新的N-[5-(3-吡啶基)-1，3，4-噻二唑-2-基]-N'-取代苯基脲，其中芳酰基叠氮化物是以芳酸、氯甲酸乙酯、叠氮化钠为起始原料采用&一锅法&所制得。

N-Carbobenzoxy-L-homoserinelactone was prepared via N-alkylation reaction of L-methionine and iodoacetamide with benzyl chloroformate as amino protecting agent.

以L-蛋氨酸为原料，氯甲酸苄酯为氨基保护试剂，与碘乙酰胺(I2微量)内酯化反应，合成N-苄氧羰基-L-高丝氨酸内酯。

Polyether modified polysiloxane was synthesized by the hydrosilation reaction of hydrogen containing silicone fluidand allyl polyether, using chloroplatinic acid as the catalyst.

以氯铂酸为催化剂，利用含氢硅油与烯丙基聚醚的硅氢加成反应，合成出聚醚改性硅油；然后用乙醇胺进行胺化反应，制成纸张用氨基改性聚醚硅油柔软剂。

Copolymerize methacrylic acid 3(4′-N,N-dimethylamino) ketone xanthate and acrylamide were copolymerized with N,N-methylene bisacrylamide,and then combined with silane ethylene group in the form of covalent bond on the quartz glass shee t to be made into a sensor,to determine ethanol.

将甲基丙烯酸3-(4′-N，N-二甲氨基)黄酮酯和丙烯酰胺、N，N′-亚甲基双丙烯酰胺共聚并共价键合在硅烷化的含乙烯基团的石英玻片上，制成了可测定乙醇的传感器。

Starting with two reactive methylene compounds, ethyl cyanoacetate and malononitrile, two 5-amino-1H-pyrazoles were prepared through the intermediates ketene dithioacetal.

从两个活泼亚甲基化合物开始，经过乙烯酮二硫代缩醛中间体，合成了两个5-氨基-1H-吡唑，以这个两个化合物为中间体，与芳香族和脂肪族α-溴代酮反应，而后经酸催化亚胺化互变异构后得到含咪唑并[1，2-b]吡唑甲硫醚类化合物6a-6g。

To increase the leaching efficiency, diastatic power and Alpha- N content of wort of the raw barley malt during bear production is crucial to increase materials usage rate.

啤酒生产过程中提高原料大麦麦芽的浸出率、糖化力和麦汁α-氨基氮是提高啤酒原料利用率的关键问题。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。