氨基

The study sum up a synthesized route which synthesize (2E,4E)-1,6-bis(3-aminopiperidin-1-yl)hexa -2-4-diene-1,6-dione easily.

总结出了一条反，反-1，6-（R-3-氨基哌啶基）粘糠酰氨的一条合成路线，为国内外同行在合成反，反-1，6-（R-3-氨基哌啶基）粘糠酰氨及其性能研究方面提供了大量得数据，为同行们在合成和更深入的研究反，反-1，6-（R-3-氨基哌啶基）粘糠酰氨提供有限的参考，以互相学习交流。

Five of their single crystals were obtained and their structures were determined by X-ray diffraction. By comparison, it was found that dithiocabamate complexes often formed an exactly planar MS4 unit, such as [Mo(R2dtc)2]; and also formed a special MS 5 unit, such as [Cu2(R2dtc)4], the copper atom lies in a distorted square-pyramidal environment.Four kinds of heteropoly acids were prepared and characterized; a series of solid superacid catalyst of supported heteropoly acid were prepared and characterized; regioselectivites of chlorobenzene mononitration with nitric acid with different heteropoly acid on different supports and reaction conditions have been investigated.

培养并解析了5个该类配合物的单晶结构，通过比较，发现二硫代氨基甲酸盐与过渡金属容易形成四配位结构，金属原子与4个硫原子共平面，比如二乙基二硫代氨基甲酸钼；也能形成比较特殊的五配位结构，比如二乙基二硫代氨基甲酸双核铜，Cu原子与5个S原子相连，处于一个变形的四方锥结构的配位环境。

The main research now is focused on the polymerization of difluoramino substituted oxetane monomers, the preparation of neopentyl difluoramino nitrato plasticizers, and the molecular design and synthesis of cyclic N2 nitramino geminal difluoramino oxidizers.

目前该领域的研究工作主要集中在二氟氨基取代环氧丁烷聚合物合成，新戊基二氟氨基硝酸酯增塑剂制备，以及环N2硝胺基偕二氟氨基氧化剂的分子设计与合成上。

The intermediate which obtained from oximation of 7a-e reacted withmethyl N-(2-bromomethylphenyl)-N-methoxycarbamate to synthesize oxime ether methyl carbamate 3a-e.

以邻位卤代苯甲醛和3-丁烯-2-醇为原料通过钯催化&一锅法&反应合成了2-乙酰基茚7a-e，7a-e 肟化之后和N-(2-溴甲基苯基)-N-甲氧基氨基甲酸甲酯反应合成了肟醚类氨基甲酸甲酯3a-e，进一步胺解之后得到了肟醚类氨基甲酰甲胺3f-j。

The colon temperatures were measured by a thermistor and the cytosolic free calcium concentration ([Ca2+]i) in dissociated brain cells was measured by Fura 2-AM. The results demonstrated that the pyretic action of egtazic acid (0.6 μmol, icv) was markedly inhibited by DEX (5 mg/kg,iv), but DEX (60-120 μmol/L) did′t affect [Ca2+]i in dissociated hypothalamus cells. Actinomycin D, which interferes with gene transcription (3 nmol, icv), completely abolished the antipyretic action of DEX on egtazic acid-induced fever.

结果发现：脑室灌注乙二醇双(2-氨基乙醚)四乙酸(0.6 nmol)引起家兔结肠温度明显升高，静脉注射地塞米松(5 mg/kg)显著抑制家兔乙二醇双(2-氨基乙醚)四乙酸性发热，地塞米松(60-120 μmol/L)并不影响下丘脑细胞内[Ca2+]i，而事先脑室灌注抑制基因转录的放线菌素D(3 nmol)则完全取消了地塞米松对乙二醇双(2-氨基乙醚)四乙酸性发热的解热作用。

The obtained terephthalaldhydic acid semicarbazone has such advantages as simple process and high purity (above 99% after post treatment), and can be used as standard in enzymoimmunoassay of semicarbazide.

本发明成功合成了呋喃西林代谢物氨基脲的衍生物氨基脲缩对醛基苯甲酸，合成步骤简洁，经过后处理，纯度高达99％以上，完全可以用作标准品，为以后人们对氨基脲的酶联免疫检测研究提供了方便的途径，可以满足国内对其研究的需要。

We also introduced spectrophotometer into the analysis of sulfamate type electrolete to measure the content of nickel sulfamate for the first time. This method is much easier than the conventional chemistry titration, it can be accomplished within one minute. Furthermore, it enhances significantly the precision of the measurement.

在电铸液分析中，我们首次将分光光度法应用于氨基磺酸盐型镍电铸液中氨基磺酸镍的测定，该方法较传统的化学滴定法操作更简单，它可以在1分钟内完成氨基磺酸镍浓度的测定，且大幅提高了分析结果的精确度，样品的消耗量仅为原来的千分之一。

The anodic behavior of electrolytic nickel anode in nickel sulfamate plating Solution was investigated,using anodic polarization curves,metallographic observation of cross-sections of nickel deposits,Hull Cell tests with solutions with and without Cl-,F-,bending tests with five solutions of different compositions,and sulfur content analysis in nickel deposit with mass spectrometry.

采用极化曲线、金相观察、赫尔槽电镀试验、弯曲试验和质谱分析方法，研究了氨基磺酸盐镀镍的阳极行为，证明了当在氨基磺酸盐镀液中使用电解镍阳极时，其活化峰值电流和镀液组成有很大的相关性，当镀液中不含F-和Cl-时其阳极活化峰值电流小，阳极处于极化状态，或相当大面积处于极化状态，使氨基磺酸根在极化的阳极表面氧化，从而使含硫化合物夹附于镀镍层，形成镀层内应力，并使镀层成为层状结构，并出现半光亮的外观。

Synthesis and structural characterization of novel cycioplatinated complexes with 2-aryl imidazolines 2-arylimidazoline ligands 2a-2d were synthesized from benzoyl chloride or p-methoxybenzoyl chloride with aminoethanol or valinol and 2e was synthesized from 2-phenylimidazoline.

新型2-芳基咪唑啉环铂化合物的合成与结构表征以苯甲酰氯或4-甲氧基苯甲酰氯和氨基醇(2-氨基乙醇或外消旋的缬氨基醇)为原料，合成了四种2-芳基咪唑啉配体2a-2d，以2-苯基咪唑啉为原料合成了配体2e，其中2d为新化合物。

The main contents and conclusions are as follows:(1) Synthesis of 1,6-hexamethylenedicarbamate catalyzed by yttrium nitrate Yttrium nitrate was employed as the catalyst in the synthesis of 1,6-hexamethylenedicarbamate from alkyl carbamates.

主要内容和结论如下：(1)硝酸钇为催化剂合成1，6-己二氨基甲酸酯采用硝酸钇作为小分子氨基甲酸烷基酯和1，6-己二胺合成1，6-己二氨基甲酸酯的催化剂。

But we don't care about Battlegrounds.

但我们并不在乎沙场中的显露。

Ah! don't mention it, the butcher's shop is a horror.

啊！不用提了。提到肉，真是糟透了。