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Firstly, the 10-methoxy-5H-dibenzazepine is synthesized through brominating and methoxylation and hydrolyzation from 5H-dibenzb, fJazepine-5-carbonyl chloride.

首先,研究了以5-氯甲酰基亚氨基芪为原料,经溴化、甲氧基化、水解合成了10-甲氧基亚氨基芪。

The intermediate 2-amino-4-nitrophenol was diazotized and coupled with sodium 2,4-diaminobenzenesulfonate to form the high-strength leather brown RHM C.

制得的2-氨基-4-硝基苯酚经重氮化、与2,4-二氨基苯磺酸偶合,合成出高强度的皮革棕 RHM C.I。

To overcome the shortcomings of traditional chemical hydrogenating, this paper studied a new synthesizing way for preparation of o-phenetidine .

本文针对传统合成邻氨基苯乙醚工艺方法中的缺点,对催化氢化法制备邻氨基苯乙醚的工艺进行了研究。

Four main saccharifying technical conditions of wheat beer influencing α-amino nitrogen content of wort including wheat malt proportiong, the ratio of water and raw materials, holding time at 52 ℃, and holding time at 65 ℃ were optimized by response surface method and the mathematical model of each factor incluencing α-amino nitrogen content was established.

采用响应曲面分析法对影响小麦啤酒麦汁α-氨基氮含量的4个主要糖化工艺参数即小麦芽比例、水料比、52 ℃保温时间和65 ℃保温时间进行优化,建立了各因素对麦汁α-氨基氮含量影响的数学模型。

A four-ball tester was used to evaluate the load carrying and antiwear properties of bismuth dibutyldithiocarbamate,bis-dibutyldithiocarbamates(V7723),sulfurized isobutylene,molybdenum ester non sulfur and phosphorus in a mineral oil respectively and their synergistic effects.

利用四球试验机评价了二丁基二硫代氨基甲酸铋与二丁基二硫代氨基甲酸酯(V7723)、硫化异丁烯和非硫磷钼酸酯添加剂的极压和抗磨性能,以及它们之间的极压和抗磨协同作用。

The character amino group vibration absorption bands were displayed in FTIR/ATR spectrum at 3352 and 1613 cm^(-1), respectively.

傅里叶变换红外光谱图谱在3352和1613 cm^(-1)处出现了新的氨基吸收峰,证实了表面接枝了氨基

Serum alt, ast, bile acid and albumin levels were measured with automatic biochemistry analysator during the procedure.

采用ccl4造模,全自动生化分析仪检测血清丙氨酸氨基转移酶、天门冬氨酸氨基转移酶、胆汁酸及白蛋白水平;he染色和vg染色观察肝脏病理及纤维化面积的变化,分析黄芪对肝功能及肝纤维化形成的影响。

Diamino-dipenylamine-2-sulfonicacid was used as an alternative of benzidine,and reacted withl-hy droxy-8-aminonaphthalene-3,6-dusuifonicacid,m-benzioc-diamine and aniline to synthesize eco-friendly black direct dye s.

报道了以4,4'-酸(4,4'-二氨基-二苯胺-2-磺酸)代替联苯胺,与H酸(1-羟基-8-氨基-3,6-二萘磺酸)、间苯二胺、苯胺等合成无致癌作用的环保型黑色直接染料。

The determination of amino acids in blood clam antianaemia oral liquid using HPLC-AccQ-Tag method is reported. The oral liquid reacted with 6-aminoquinolyl-N-hydroxysuccini-mdyl carbamate. Then, the corresponding derivatives were analyzed with an HPLC. The chromatographic conditions were AccQ-TagTM C18 column for amino acids analysis (3.9mm×15cm); mobile phase of program elution sodium acetate solution(pH5.02), acetonitrile, Milli-Q water. The amino acids'AQC deriatives were detected at 248nm with a UV-detector. Eighteen kinds of amino acids were completely determined in 35 minutes.

以6-氨基喹啉-N-羟基琥珀酰亚胺基氨基甲酸酯为衍生剂,与毛蚶抗贫血口服液中的氨基酸柱前定量衍生,用WatersHPLC仪,AccQ-TagTM专用C18柱(3.9mm×15cm),以140mmol·L-1的醋酸钠溶液(pH5.02)为溶剂A,乙腈为溶剂B,超纯水为溶剂C,进行梯度洗脱,检测波长为248nm,35min测试完毕。

To dye the different types of fibers by the same dye, universal dyes based on naphthalene ring system are prepared by the diazo coupling reaction of 7-acetamide-4-hydroxy-2-oaphtialene-β-(N,N-dimethylaminoethyl)solfonamide and m-aminobenzene-β-hydroxyethyl sulfone sulfunate.

为了实现用同一支染料对不同类型的纤维进行染色的目的,通过间氨基苯基-β-羟乙基砜硫酸酯与7-乙酰氨基-4-羟基-2-萘-β磺酰胺的重氮化偶合反应合成了含萘环的通用染料,其结构通过质谱分析进行了表征。

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