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A surface-initiated ring-opening polymerization approach was used to functionalize multiwalled carbon nanotubes with linear poly.

通过化学改性,在碳纳米管表面引入氨基,然后引发N~5-苄氧羰基赖氨酸的N~2-羧基-α-氨基酸酐单体的开环聚合,成功将聚赖氨酸接枝到碳纳米管表面。

The relationship between the structures and the fungicidal activities of the compounds has been discussed.

一以氨基胍碳酸盐为原料,首先与草酸、甲酸反应合成了3-氨基-1,2,4。

Laboratory evaluation consists of hematocrit (hemoconcentration suggests preeclampsia), platelet count, protein excretion, serum creatinine, serum uric acid, serum alanine and aspartate aminotransferase concentrations, and lactic acid dehydrogenase concentration.

实验室评估包括红细胞压积,血小板计数,蛋白排泄,血肌酐,血尿酸,血清丙氨酸氨基转化酶和天门冬氨酸氨基转化酶,和乳酸脱氢酶浓度

The invention relates to a synthesis method of N-acetylaminoglucose, which comprises dissolving D-glucosamine hydrochlorate and alcohol at the mass ratio of 2-2.5:100, adjusting the pH value of the solution to 9-10, filtering, taking the filter liquor, mixing and adding acetic anhydride at the 50-60wt% amount of D-glucosamine hydrochlorate, mixing and reacting for 2h, using absolute ethyl alcohol to recrystallizing, filtering and recrystallizing via water, to obtain rod-shape food grade N-acetylaminoglucose.

本发明涉及一种N-乙酰氨基葡萄糖的合成方法。该方法的具体步骤为:将D-葡萄糖胺盐酸盐和乙醇按2~2.5∶100的质量比溶于水中,调节该溶液的pH值为9~10;过滤,取滤液,搅拌下加入乙酸酐,其加入量为原料D-葡萄糖胺盐酸盐量的50~60wt%;搅拌反应2小时后,用无水乙醇进行重结晶;过滤,晶体再用水重结晶,得棒状食品级N-乙酰氨基葡萄糖。

It is shown by Infrared spectra that relative concentration of amino formic acid ester has prominent relationship with compressive stress at 10% strain in the process of accelerated hygrothermal tests, which means that hydrolysis of amino formic acid ester is main factor resulting in decrease of compressive properties.

经红外光谱测定,在人工加速湿热老化试验过程中,材料的活性基团氨基甲酸酯的相对浓度与10%定应变压缩应力的相关性显著,氨基甲酸酯水解是材料室内贮存过程中力学性能下降的主要原因。

The experimental results showed that when AcO-or other anion s were added to a solution consisting of 1,5-(di-benzaldehyde) dithiocarbohydrazone and Hg2+(at a ratio of 1∶2),a hypsochromic shift took place on the maximum ultraviolet absorption peak of the ligand.

设计合成了配体1,5-二双缩二氨基硫脲及其金属配合物,探讨了不同金属阳离子对1,5-二双缩二氨基硫脲紫外吸收光谱的影响,并将标题化合物应用于阴离子识别。

After basal anesthesia, ilioinguinal/iliohypogastric nerve blockades was administed in nerve block group, paracetamol group received rectal paracetamol, control group had not any medication.

各组患儿行基础麻醉后,神经阻滞组行患侧髂腹股沟/髂腹下神经阻滞;对乙酰氨基酚组经肛门塞人直肠对乙酰氨基酚栓剂;对照组未予任何药物镇痛。

After extraction by ethanol and purification by cationic ion-exchange column, a method of using reversed-phase high-performance liquid chromatography and precolumn derivatization with o-phthalaldehyde and 9-fiuorenylmethylchloroformate is employed for determination of free amino acids in tobacco . This method assures that amino acids with amino and imino groups can be determined simultaneously. The results of duplication experiment and recovery experiment are acceptable.

本试验用乙醇提取烟叶中的游离氨基酸,并用阳离子交换树脂纯化,再用邻苯二甲醛、氯甲酸芴甲酯联合柱前衍生、反相高效液相色谱分析测定了烟叶中的游离氨基酸,该方法能同时测定烟叶中的带氨基和亚氨基基团的氨基酸,并且分析方法的重现性和回收率均令人满意。

Among the six polyetherimdes, ODPA-IPDA with the largest free-volume and larger intrasegmental mobility has the highest permeability and the lowest permselectivity, ODPA-DABP with the smallest free- volume and the smallest intrasegmental mobility has the lowest permeability and the lowest permselectivity, ODPA-DMMDA with the larger free-volume and smaller intrasegmental mobility has higher permeability and higher permselectivity.

二苯醚四酸二酐(ODPA-4.4'-二J氨基二苯异丙烷具有很大的自由体积和较小的链段活动性、很大的透气性和较小的透气选择性,ODPA—4,4'-二氨基二苯酮具有很小的自由体积和较小的链段活动性、很小的透气性和较大的透气选择性,ODPA—3,3'-二甲基二苯甲烷二胶具有较大的自由体积和较小的链段活动性、很大的透气性和很大的透气选择性。

Xinquan HuTwo new chiral backbones R-- and S--2-amino-2"-hydroxy-4,4",6,6"-tetra methyl-1,1"-biphenyl were synthesized via nitration, diazotation/iodination, Ulhnann coupling, selective reduction, diazotation/hydrolysis, hydrogenation and resolution from 2,4-dimethyl-aniline in seven steps.

以2,4-二甲基苯胺为起始原料,经过硝化反应、重氮化碘代反应、Ullmann缩合反应、选择性双硝基单还原反应、重氮化水解反应、催化氢化反应和拆分,首次合成了--2-氨基-2'-羟基-4,4',6,6'-四甲基-1,1'-联苯和--2-氨基-2'-羟基-4,4',6,6'-四甲基-1,1'-联苯两个对映体。

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