氨基

The cis novel bisoxazoline ligands L1-L4 have been synthesized through the treatment of new cis dihydroxy diamide with p-toluenesulfonyl chloride in the presence of catalytic quantity of 4--pyridine, and the cis dihydroxy diamide could be achieved from the condensation of the amino alcohols and cis cyclopropane dicarbonyl chloride prepared via oxidation and halogenation from cis-2,2-dimethyl-3-formylcyclopropanecarboxylate with DCC.

我们以蒈醛酸内酯为起始原料，经过氧化反应、酰氯化反应得到顺式环丙烷二酰氯，然后在二环己基碳二亚胺的催化下与相应的氨基醇反应合成了顺式二羟基酰胺，再用对甲苯磺酰氯将羟基活化，最后在二甲氨基吡啶的催化下关环合成顺式双噁唑啉配体L1～L4。

The resultant was hydrogenised to remove protective group of amino group, then the product was reacted with NaNO2 to give diazonium salt, which was conjugated with salicylic acid, hydroxybenzene, N-salicyloyl glycine acid to get azo derivatives of 4-ASA.

本文首先对4-ASA的氨基和羟基进行了选择性保护，通过氢化还原法选择性脱除氨基的保护基，然后将氢化产物制成重氮盐，通过与水杨酸、苯酚和水杨酰甘氨酸发生反应生成4-ASA的偶氮衍生物，最后在碱性条件下水解得到最终产物。

The influence of each condition on the reaction speed and yield was studied, and the optimal conditions were: the ratio of the amount of substance of aromatic amine and heptafluoro-isopropyl iodine was 1:1.1~1.5, the amount of substance of sodium dithionite, sodium bicarbonate, aniline compounds were respectively 1.1~1.3, the amount of substance of phase transfer catalyst TBAB and aniline compounds was 0.05~0.1, the concentration of aniline compound was 0.5~1.0 mol/L, reaction temperature was 10~20 ℃, and the solvent was aether.

最佳结果为：芳胺与七氟异丙基碘的物质的量比1：1.1~1.5，连二亚硫酸钠、碳酸氢钠与苯胺的物质的量分别为1.1~1.3，相转移催化剂四丁基溴化铵与苯胺的物质的量比在0.05~0.1，溶剂总用量使苯胺浓度在0.5~1.0 mol/L；反应温度10~20℃；溶剂采用乙醚。取代基供电子性越强，反应时间越短，产率越高；氨基的对位优先反应，氨基的邻位较难发生反应；且七氟异丙基总是优先取代在芳环电子云密度较高的位置上。

The results show that the iminodiacetic acid wastewater can be treated effectively by electrodialysis method.

实验结果表明，采用电渗析法能够有政处理亚氨基二乙酸废水，电渗析脱盐率＞96％，亚氨基二乙酸损失率＜0.6%。

Using nickel aminosulfonic bath as a study system of electroform ing and by adding cobalt aminosulfonic,the internal stress,composition,hardness and tensile strength of the electroform ed nickel-cobalt deposit were tested.

采用氨基磺酸镍镀液作为电铸的研究体系，并在镀液中加入氨基磺酸钴，对镍钴合金电铸层的内应力、组成、硬度、抗拉强度等进行了测试。

In some cases, its epimer 4 was also obtained. 22 compounds were synthesized, among them 18 were new.3. Using the intramolecular Pictet-Spengler reaction to form the pentacyclic skeleton of Et-743, the byproducts 25 were obtained under various conditions. The structures of them were determined to be 1, 2-dihydro-isoquinoline compounds, and the mechanism of the reaction was proposed.B. The synthesis of the analogs of Et-743Because of the failure of removing the protective groups in compounds 14, the synthetic strategy was adjusted.

对于苄基保护的羟基化合物13a，顺利得到化合物30，然后与不同的羧酸反应得到18个酯化合物33-50；对于苄氧羰基保护的氨基化合物13b，由于脱除保护基的化合物31在空气中不稳定，所以我们采取不经分离纯化，直接与羧酸反应得到酰胺化合物53-62，然后再分别对其C-21位的羰基进行还原氰基化，得到10个酰胺目标化合物63-72，另外，我们还对羟基转化为氨基的反应进行了探索。3。

In this section, we study the reactions of both potassium ferricyanide and hexaammineruthenium chloride at a 4-aminobenzoic acid modified glassy carbon electrode by SECM in different pH solutions.

应用扫描电化学显微镜对4-氨基苯甲酸修饰的玻碳电极进行了电化学表征，研究了酸度对电极表面修饰的4-氨基苯甲酸解离形态的影响，及不同的荷电中介体在此修饰电极表面的电化学行为。

Results show that treating the pear juice with FPC-21 resin can reduced pH value, formol index and browning index. Reduction of pH value enhence the decolor ability of XAD-16 resin on pear juice. Reduction of pH value and formol index can control the browning rate of PJC during storage.

结果显示，阳离子树脂处理可降低酥梨汁的pH值、氨基态氮和褐变指数；降低pH值可提高吸附树脂对酥梨汁的脱色能力；降低pH值、氨基态氮可控制70 °Brix浓缩酥梨汁贮存中褐变速度。

In this dissertation, two derivatives of aniline containing polyoxyethylene substituent m-phenylene diamino formyl alkylenediamine poly acetate and poly-3-aminobenzoate were designed and synthesized. And then, comb-shaped polyaniline grafted by PEO were prepared by chemical oxidation copolymerization. The structure of copolymers were characterized by FTIR, ultraviolet-visible spectrum, elemental analysis and TEM etc..

本文在设计并合成两种含聚氧乙烯取代基的苯胺衍生物——间苯二氨基甲酰己二氨基甲酸聚氧乙烯乙酸酯和3-聚氧化乙烯单甲醚基苯胺的基础上，采用化学氧化法将它们与苯胺进行共聚，制备出了聚氧乙烯接枝聚苯胺的梳型共聚物。

Fucose composed of 40% the total carbohydrate with lesser but approximately equal amount of galactose, glucosamine, and galactosamine present.

对糖萼的糖化学组份分析表明糖萼是由40％的岩藻及大致等量的半乳糖，氨基葡萄糖和氨基半乳糖组成。

But we don't care about Battlegrounds.

但我们并不在乎沙场中的显露。

Ah! don't mention it, the butcher's shop is a horror.

啊！不用提了。提到肉，真是糟透了。